Fibrillated Cellulose Non-ionic Ether Composite High Dry Matter

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing fibrillated cellulose (FC) products face challenges in achieving high dry matter content for economic commercialization due to aggregation and hornification issues, making them difficult to redisperse and maintain rheological properties, especially when dried, and current solutions require expensive equipment or additives.

Innovation Solution

Co-processing FC with non-ionic cellulose ethers to create concentrated, easily dispersible powders that retain rheological performance even in aqueous media with salts, using a process involving mechanical treatment, concentration, and controlled drying to achieve high dry matter content without hornification.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If fibrillated cellulose is concentrated to high dry matter content for economic commercialization, then production costs and transport costs are reduced, but aggregation and hornification occur making the material difficult to redisperse and maintain rheological properties

Engineering Contradiction:
Improvedry matter contentVSAvoidrheological properties
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The patent introduces non-ionic cellulose ethers as intermediary substances that act as dispersing agents and rheology modifiers. These cellulose ethers prevent aggregation and hornification of fibrillated cellulose at high dry matter contents, enabling easy redispersion while maintaining rheological properties. The cellulose ethers serve as a mediator between the fibrillated cellulose and the aqueous environment, allowing stable suspension even in the presence of salts.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent creates a composite material system combining fibrillated cellulose with non-ionic cellulose ethers. This composite approach leverages the high surface area and rheological activity of fibrillated cellulose while using the cellulose ethers to provide stability, prevent aggregation, and maintain properties under various conditions including high concentration and salinity. The synergistic combination resolves the contradiction between concentration and stability.

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If fibrillated cellulose is dried to high dry matter content for economic commercialization, then storage and transport costs are reduced, but the material becomes difficult to redisperse without expensive equipment or additives

Engineering Contradiction:
Improvedry matter contentVSAvoidredispersibility
Core Design Contradiction:
Quantity of substanceVSEase of manufacture

Solution Approach 1:

Non-ionic cellulose ethers serve as intermediary substances that facilitate redispersion of concentrated fibrillated cellulose. These cellulose ethers act as wetting agents and dispersing agents that enable easy mixing with water without requiring expensive high-shear equipment. The cellulose ethers mediate between the concentrated dry material and the aqueous environment, allowing simple redispersion processes.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent utilizes parameter changes in the cellulose ether structure (such as degree of etherification, molecular weight, and hydrophobicity) to optimize performance. By adjusting these parameters, the cellulose ethers can be tuned to provide optimal dispersibility and rheological modification at different concentrations, enabling easy redispersion of high dry matter content products without additional additives or expensive equipment.

Inventive Principle:
Principle #35Parameter changes

3Adaptability or versatility

If fibrillated cellulose products are used in aqueous media with salts for practical applications, then commercial viability is improved, but aggregation increases making redispersion difficult

Engineering Contradiction:
Improveapplicability in saline mediaVSAvoiddispersibility
Core Design Contradiction:
Adaptability or versatilityVSStability of the object's composition

Solution Approach 1:

Non-ionic cellulose ethers act as intermediary protective agents that shield fibrillated cellulose from salt-induced aggregation. These cellulose ethers form protective interfaces around the cellulose fibrils, preventing direct interaction with salts that would cause aggregation. This intermediary action maintains dispersibility and rheological properties even in saline aqueous media, enabling practical commercial applications.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent employs parameter changes in cellulose ether characteristics (such as hydrophobicity, molecular weight, and etherification degree) to optimize performance in saline environments. By adjusting these parameters, the cellulose ethers can be tailored to provide optimal protection against salt-induced aggregation, maintaining product stability and dispersibility in various aqueous applications including food, personal care, and industrial formulations.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method allows for the production of FC products with high dry matter content that are easily dispersible and maintain desired rheological properties, including thixotropic behavior, without the need for expensive equipment or additives, enabling economic commercial-scale production and use in various applications.

Implementation Method 1

the compositions of the invention... provide thixotropic compositions when dissolved in an aqueous medium

Methodology Applied
Scientific EffectThixotropy: Thixotropy

Data Source

PatentUS20220213297A1Compositions comprising fibrillated cellulose and non-ionic cellulose ethers
Publication Date: 2022.07.07 AKZO NOBEL CHEMICALS INTERNATIONAL BV

AI summary

The present invention relates to compositions comprising fibrillated cellulose and one or more nonionic cellulose ethers. Such compositions were found to be able to modify the rheology of an aqueous medium, also when the aqueous medium comprises salts and surfactants, whereby specific formulations shows desirable thixotropic thickening of the aqueous medium.