Fireproof Glass Unit with Quantum Dot Gel Matrix

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Solution Overview

Problem

There is a lack of technical solutions for glass units that combine fire resistance with the ability to absorb and convert electromagnetic radiation, particularly in the UV, VIS, and IR ranges, while ensuring high fire resistance and transparency.

Innovation Solution

A method is developed to create a selective fireproof matrix modified with semiconductor nanoparticles, specifically CdSe/CdS quantum dots, dispersed in a gel matrix composed of sodium and potassium silicates, sorbitol, xylitol, and colloidal silica, which is filled into the chambers of glass units, providing fire resistance and electromagnetic wave conversion.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If glass units are filled with conventional fireproof materials, then fire resistance is improved, but transparency and electromagnetic radiation conversion ability deteriorate

Engineering Contradiction:
Improvefire resistanceVSAvoidtransparency
Core Design Contradiction:
ReliabilityVSIllumination intensity

Solution Approach 1:

The patent uses a composite material consisting of a gel matrix (water, glycerol, colloidal silica) combined with semiconductor quantum dots (CdSe/CdS nanoparticles). This composite provides both fire resistance from the gel matrix and electromagnetic radiation conversion with maintained transparency from the quantum dots, resolving the contradiction between fire resistance and transparency.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent changes the physical and chemical parameters of the fireproof layer by using a gel-based composition with specific ratios of water (50-70%), glycerol (5-20%), and colloidal silica (10-30%), along with quantum dots at controlled concentrations. This allows the material to maintain transparency while achieving fire resistance through parameter optimization.

Inventive Principle:
Principle #35Parameter changes

2Adaptability or versatility

If quantum dots are added to the fireproof matrix, then electromagnetic radiation conversion ability is improved, but manufacturing complexity increases

Engineering Contradiction:
Improveelectromagnetic radiation conversionVSAvoidmanufacturing complexity
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The patent merges the fireproof matrix and quantum dots into a single integrated gel composition that can be applied in one step. The quantum dots are dispersed directly into the gel matrix during preparation, combining the fireproofing and electromagnetic conversion functions into a single material system, thereby reducing manufacturing complexity.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The gel matrix itself serves as the dispersion medium for quantum dots, eliminating the need for separate application processes. The composition is self-assembling during the gelation process, where quantum dots automatically disperse and stabilize within the gel network, reducing manual intervention and manufacturing complexity.

Inventive Principle:
Principle #25Self-service

3Reliability

If semiconductor nanoparticles are dispersed in the gel matrix, then optoelectronic properties are maintained at high temperatures, but even dispersion becomes difficult

Engineering Contradiction:
Improveoptoelectronic properties stabilityVSAvoideven dispersion
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent uses colloidal silica particles as an intermediary medium that facilitates even dispersion of quantum dots within the gel matrix. The colloidal silica acts as a spacer and stabilizing agent, preventing quantum dot aggregation and ensuring uniform distribution throughout the fireproof layer, thereby maintaining optoelectronic properties at high temperatures.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent optimizes the concentration parameters of quantum dots (0.1-5 mg/L) and colloidal silica (10-30%) in the gel matrix to achieve even dispersion. By carefully controlling these parameters during preparation, the system maintains stable quantum dot distribution that preserves optoelectronic properties even under high temperature conditions.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution achieves high fire resistance and transparency in glass units by ensuring even dispersion of quantum dots, maintaining optoelectronic properties at high temperatures, and preventing toxic substance release during combustion, while being environmentally friendly and easy to dispose of.

Implementation Method 1

The smaller the diameter of particles, the emission spectrum shifts towards shorter wavelengths, and this phenomenon has been called the quantum size effect

Methodology Applied
Scientific EffectQuantum size effect:

Implementation Method 2

low-dimensional structures of semiconductors called quantum dots absorb electromagnetic radiation waves in a wide range, from UV to IR, as a result of which they emit waves of a strictly defined length

Methodology Applied
Scientific EffectPhotoluminescence: Photoluminescence

Implementation Method 3

which, in turn, are transferred to the edge of the system where the photovoltaic effect and electricity generation take place

Methodology Applied
Scientific EffectPhotovoltaic effect: Photovoltaic Effect

Implementation Method 4

A commonly used multi-functional glass unit consists of at least two panes forming an inter-pane chamber or chambers filled with air or other gas. A single-chamber glass unit usually has an outer tempered pane and an inner pane with an emissive coating

Methodology Applied
Scientific EffectFire resistance:

Data Source

PatentEP3816125B1Method of obtaining a selective fireproof layer modified with semiconductor nanoparticles and filling the chamber or chambers of a glass unit with this active layer as well as a glass unit containing this or those layers
Publication Date: 2023.07.05 ML SYST SPOLKA AKCYJNA
  • EP3816125B1 patent drawingFigure 1

AI summary

The subject of the invention is a method of obtaining a selective fireproof layer modified with semiconductor nanoparticles and filling with this active layer the chambers or chambers of an insulating glass unit and an insulating glass unit containing one or these layers, which consists in the fact that it is carried out in five successive technological stages, whereby in in the first stage, a glycerine dispersion of quantum dots is made at a concentration ranging from 20 mg / 1 to 50 mg / 1, in the second stage, a matrix for quantum dots (QDS) is prepared by homogenizing the mixture in the reactor by introducing into it successively: - 32.2 - 32.4% by weight of an aqueous sodium silicate solution, and - 32.2 - 32.4% by weight of an aqueous potassium silicate solution, and then in the third step to the thus obtained homogeneous mixture the following are added dropwise: - 0.75% by weight of sorbitol - 0.85% by weight of xylitol, and - 2 % - 3.00% by weight of glycerine dispersion of quantum dots and the whole is subjected to mixing, and then in the fourth step, 30.60% - 32.00% by weight of the aqueous solution of colloidal silica are introduced into this reactor and the whole is subjected to mixing and then cooling to obtain a liquid selective fireproof matrix modified with semiconductor nanoparticles, and then, in the fifth step, the matrix obtained in this way is filled in the chambers between panes of the glass unit and the entire system is subjected to a temperature of 60 ° - 70 °C for 6 - 8 hours, as a result of which the required transparency and fire resistance of the entire system, of each of these glass units, is obtained.