Flame-Zone Soot Capture for Consistent Optical Article Composition

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Solution Overview

Problem

Existing methods for capturing soot during the production of optical articles result in inefficient deposition and contamination, leading to variations in soot composition and concentration, which affects the quality of the produced articles.

Innovation Solution

A method involving the combustion of silicon- and titanium-containing precursors to produce a soot stream, followed by the use of a capture medium and condensate to form a slurry, which is recirculated and mixed with additional slurry to achieve the desired soot concentration and composition, utilizing dispersants and turbulence to enhance soot capture.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If scrubber type pollution abatement systems are used to capture soot particles, then soot capture is achieved, but the collected particles become contaminated and have limited uses

Engineering Contradiction:
Improvesoot capture efficiencyVSAvoidparticle contamination
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The patent extracts soot particles from the gas stream directly at the combustion source using a capture medium introduced into the flame zone, separating the soot collection function from traditional downstream scrubber systems. This extraction approach captures particles before they become contaminated by subsequent processing equipment

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent introduces a capture medium (liquid or gas) as an intermediary substance that directly contacts and captures soot particles in the flame zone. This intermediary approach allows selective capture of soot while leaving other combustion products to follow normal exhaust paths, avoiding contamination from contact with scrubber materials

Inventive Principle:
Principle #24Intermediary (Mediator)

2Quantity of substance

If soot is captured using conventional methods, then some soot is recovered, but deposition efficiency remains less than desirable

Engineering Contradiction:
Improvesoot recovery amountVSAvoiddeposition efficiency
Core Design Contradiction:
Quantity of substanceVSProductivity

Solution Approach 1:

The patent performs preliminary action by introducing the capture medium into the flame zone where soot particles are freshly formed and highly reactive. This timing allows maximum capture efficiency before particles settle, aggregate, or escape the combustion region

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent employs fluid dynamics by introducing a capture medium (liquid or gas) that flows through the flame zone, utilizing pneumatic and hydraulic principles to entrain and transport soot particles. The fluid flow patterns enhance particle-capture medium contact and improve overall deposition efficiency

Inventive Principle:
Principle #29Pneumatics and hydraulics

3Adaptability or versatility

If soot concentration or composition varies, then production flexibility is maintained, but article quality consistency deteriorates

Engineering Contradiction:
Improveproduction flexibilityVSAvoidarticle quality consistency
Core Design Contradiction:
Adaptability or versatilityVSManufacturing precision

Solution Approach 1:

The patent implements feedback control by monitoring soot particle characteristics and adjusting precursor delivery rates or capture medium flow to maintain consistent soot composition and concentration. This closed-loop approach ensures article quality consistency while allowing flexibility in production parameters

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The patent controls soot composition and concentration by precisely adjusting input parameters such as precursor delivery rates, oxygen availability, and capture medium flow rates. These parameter changes allow flexible production while maintaining consistent soot quality for high-quality optical articles

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method achieves high soot capture efficiency with minimal contamination, resulting in consistent soot composition and reduced waste, enabling the production of high-quality optical articles.

Implementation Method 1

combusting a first precursor comprising a silicon-containing compound and a second precursor in a burner to produce a soot stream comprising soot

Methodology Applied
Scientific EffectCombustion: Combustion

Implementation Method 2

passing water as a vapor and aerosol into the soot stream proximate the burner such that the soot is captured in the water and forms a slurry

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 3

passing water as a vapor and aerosol into the soot stream proximate the burner such that the soot is captured in the water

Methodology Applied
Scientific EffectAerosol: Aerosol

Implementation Method 4

recirculating the slurry through the soot stream such that the slurry is from about 20 wt% to about 80 wt% soot

Methodology Applied
Scientific EffectSedimentation: Sedimentation

Data Source

PatentEP3830044B1Methods of capturing soot
Publication Date: 2025.09.03 CORNING INC
  • EP3830044B1 patent drawingFigure 1
  • EP3830044B1 patent drawingFigure 2
  • EP3830044B1 patent drawingFigure 3A

AI summary

A method of capturing soot includes the steps: combusting a first precursor in a burner 32 to produce a soot stream 36, the soot stream 36 comprising soot 40 and exiting the burner 32 at an outlet 33; and directing a capture medium 48 to the soot stream 36, the capture medium 48 contacting the soot in an impact region 50, the soot having a temperature greater than 50° C in the impact region. The capture medium 48 may be sprayed via a slurry nozzle 44 and the soot may form a slurry 60.