Flash Vaporization System for Uniform OLED Deposition

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Solution Overview

Problem

Conventional vapor deposition methods face challenges in maintaining a uniform vaporization rate due to variations in material feed rate, leading to non-uniform film thickness and low throughput in OLED manufacturing, especially with organic materials that degrade at high temperatures and require precise temperature control.

Innovation Solution

A flash vaporization system with a low thermal mass heating element is used, where a constant current is applied to maintain a constant heat flux, allowing the heating element temperature to vary, and the vaporizable material is fed from a temperature-controlled region below its vaporization temperature, ensuring uniform vaporization despite variations in feed rate.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Stability of the object's composition

If conventional vapor deposition sources use large thermal mass to minimize temperature fluctuations, then temperature stability is improved, but the time to reach equilibrium temperature and stable vapor deposition rate increases significantly

Engineering Contradiction:
Improvetemperature stabilityVSAvoidtime to reach equilibrium
Core Design Contradiction:
Stability of the object's compositionVSLoss of time

Solution Approach 1:

The patent changes the thermal mass parameter of the heating element from large to small, fundamentally altering the thermal response characteristics. This allows the system to reach equilibrium rapidly while maintaining temperature stability through feedback control, resolving the contradiction between speed and stability

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent implements feedback control by monitoring the actual vapor deposition rate and adjusting the heating power accordingly. This closed-loop control maintains temperature stability despite the small thermal mass, enabling rapid equilibrium while preserving deposition rate consistency

Inventive Principle:
Principle #23Feedback

2Object-affected harmful factors

If small quantities of organic material are loaded into the source to minimize temperature exposure, then material degradation is reduced, but the operation time and throughput are limited

Engineering Contradiction:
Improvematerial degradationVSAvoidthroughput
Core Design Contradiction:
Object-affected harmful factorsVSProductivity

Solution Approach 1:

The patent extracts the material from the heating zone and delivers it directly to the substrate. The material remains in the cold storage region until needed, then is rapidly vaporized and deposited. This separation allows large quantities of material to be stored without degradation while maintaining high throughput

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent uses rapid flash vaporization to quickly convert material from solid to vapor and deposit it onto the substrate. This rapid process minimizes the time material spends at elevated temperatures, reducing degradation while enabling high deposition rates for improved throughput

Inventive Principle:
Principle #21Skipping (Rushing through)

3Adaptability or versatility

If flash vaporization is used with variable feed rate, then material delivery flexibility is improved, but vaporization rate uniformity deteriorates

Engineering Contradiction:
Improvefeed rate flexibilityVSAvoidvaporization rate uniformity
Core Design Contradiction:
Adaptability or versatilityVSManufacturing precision

Solution Approach 1:

The patent employs feedback control where the vapor deposition rate is continuously monitored and the heating power is adjusted in response. This maintains uniform vaporization rate despite variations in material feed rate, resolving the contradiction between flexibility and precision

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The patent makes the heating power dynamic rather than static. The heating element's power input is continuously adjusted based on feedback signals, allowing the system to adapt to feed rate variations while maintaining constant vaporization rate and film uniformity

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach achieves stable and uniform vapor deposition rates without the need for complex closed-loop control systems, minimizing material degradation and enabling continuous operation with high uniformity, even with varying feed rates, and is effective for both organic materials that vaporize directly and those that melt before vaporizing.

Implementation Method 1

heating it to a temperature so as to cause vaporization and create a vapor plume

Methodology Applied
Scientific EffectVaporization: Evaporation

Implementation Method 2

a flash vaporization system with a low thermal mass heating element is used

Methodology Applied
Scientific EffectFlash vaporization: Flash Evaporation

Implementation Method 3

a constant current is applied to maintain a constant heat flux

Methodology Applied
Scientific EffectJoule heating: Joule Heating

Implementation Method 4

Physical vapor deposition in a vacuum environment is the principal means of depositing thin films of material

Methodology Applied
Scientific EffectPhysical vapor deposition: Physical Vapour Deposition

Implementation Method 5

vaporizing material at a uniform rate for forming a layer on a substrate

Methodology Applied
Scientific EffectCondensation: Condensation

Data Source

PatentEP1924721B1Method for vaporizing material at a uniform rate
Publication Date: 2014.07.02 GLOBAL OLED TECHNOLOGY LLC
  • EP1924721B1 patent drawingFigure 1
  • EP1924721B1 patent drawingFigure 2
  • EP1924721B1 patent drawingFigure 3

AI summary

A method of vaporizing material at a uniform rate for forming a layer on a substrate includes feeding a column of vaporizable material from a temperature controlled region maintained below the vaporizable material's effective vaporization temperature to a source of vaporization energy, wherein the volume of the column can vary during vaporization; and providing a source of vaporization energy delivering a constant heat flux to the surface of the column so that a uniform volume per unit time of the vaporizable material is vaporized to form the layer on the substrate, irrespective of the feeding rate.