Flat-Ended Indenter Punch for Stress-Strain Curve Measurement

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Solution Overview

Problem

Current instrumented indentation techniques struggle to accurately determine the stress-strain curve of small-scale materials due to limitations in indenter geometry, such as the Berkovich indenter imposing only one effective strain and spherical indenters facing challenges in detecting initial plasticity and managing concurrent strain and material volume changes, especially in heterogeneous materials.

Innovation Solution

An instrumented indentation apparatus with a flat-ended indenter punch and a controller that calculates stress and strain using specific equations, allowing for controlled displacement and force application to construct a stress-strain curve, enabling precise measurement of mechanical properties without the need for expensive sample preparation like micro-pillar fabrication.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If a Berkovich indenter is used, then the indentation test can be performed with a standard geometry, but only one effective strain can be imposed and the stress-strain relationship beyond yield cannot be determined

Engineering Contradiction:
Improvestandard indenter geometryVSAvoidstrain range measurement capability
Core Design Contradiction:
Ease of manufactureVSAdaptability or versatility

Solution Approach 1:

The patent changes the geometric parameter of the indenter from a self-similar pyramidal shape (Berkovich) to a flat-ended cylindrical shape with a specific radius. This geometric parameter change enables the indenter to impose varying strains on the material during indentation, allowing measurement of the complete stress-strain curve including post-yield behavior, while maintaining a standardized indenter design.

Inventive Principle:
Principle #35Parameter changes

2Adaptability or versatility

If a spherical indenter is used, then the strain can increase with indentation force, but the initial onset of plasticity is difficult to detect and both strain and material volume change concurrently

Engineering Contradiction:
Improvestrain rangeVSAvoidplasticity detection accuracy
Core Design Contradiction:
Adaptability or versatilityVSMeasurement precision

Solution Approach 1:

The patent changes the indenter geometry from spherical to flat-ended cylindrical with a defined radius. This parameter change creates a stress distribution pattern where the maximum shear stress occurs at the surface rather than below the surface, enabling accurate detection of the initial onset of plasticity. The flat end surface maintains constant contact area, decoupling strain measurement from material volume changes.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The flat end surface of the indenter creates a uniform stress distribution across the contact area, establishing an equipotential stress field. This uniformity ensures that plasticity initiates simultaneously across the contact zone, making the onset of plasticity easily detectable and eliminating the detection difficulties associated with spherical indenters where stress concentrates at subsurface points.

Inventive Principle:
Principle #12Equipotentiality

3Measurement precision

If micro-pillar compression tests are performed, then the complete stress-strain curve can be obtained, but expensive equipment and time-consuming sample preparation are required

Engineering Contradiction:
Improvestress-strain curve accuracyVSAvoidsample preparation complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent extracts the essential measurement capability of micro-pillar compression tests (obtaining complete stress-strain curves) and transfers it to a standard instrumented indentation platform. By using a flat-ended cylindrical indenter, the method eliminates the need for complex micro-pillar fabrication while achieving the same measurement objectives through a simplified, widely available testing apparatus.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent creates a simplified copy of the micro-pillar compression test functionality using standard indentation equipment. The flat-ended cylindrical indenter replicates the uniaxial compression stress state of micro-pillars without requiring actual micro-pillar fabrication, thereby copying the measurement capability while eliminating the complex sample preparation and expensive equipment requirements.

Inventive Principle:
Principle #26Copying

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach allows for efficient and economical determination of the entire stress-strain curve on a nanoscale, improving accuracy and reducing complexity in measuring mechanical properties of small-scale materials by maintaining a constant contact area and easily detecting the onset of plasticity.

Implementation Method 1

When the spherical surface of the indenter punch first contacts the surface of the test material, the strain is small, and the deformation is elastic

Methodology Applied
Scientific EffectElastic deformation: Elasticity

Implementation Method 2

The imposed strain increases as the indenter punch is pressed further into the test material, and eventually causes plastic yield in the test material

Methodology Applied
Scientific EffectPlastic deformation: Plasticity

Implementation Method 3

a force detector that outputs data representative of an applied force corresponding to mechanical response of the sample as a reaction to being indented by the punch

Methodology Applied
Scientific EffectForce measurement: Force

Implementation Method 4

a displacement detector that outputs data representative of a depth to which the sample is indented by the punch

Methodology Applied
Scientific EffectDisplacement measurement: Displacement

Data Source

PatentUS10288540B1Instrumented indentation apparatus having indenter punch with flat end surface and instrumented indentation method using the same
Publication Date: 2019.05.14 KLA CORP
  • US10288540B1 patent drawing
  • US10288540B1 patent drawing
  • US10288540B1 patent drawing

AI summary

An instrumented indentation apparatus and instrumented indentation method, for use in instrumented indentation, employ a flat-ended indenter (punch). Force-displacement data of a loading operation, in which a sample is indented using the indenter, and the known value of the effective radius of the end surface of the indenter, are used to calculate values of stress and strain. The entire stress-strain curve for the sample may be produced from these values.