Flat Feed Hood Tube Bundle Reactor for Temperature Control

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Conventional tube bundle reactors face challenges in controlling reaction conditions, particularly temperature, for uncatalyzed and homogeneously catalyzed reactions, leading to low selectivity and potential reactor instability due to large-volume inlet and outlet hoods, which can result in uncontrolled reactions and product loss.

Innovation Solution

A tube bundle reactor design with a small internal volume feed hood that allows precise temperature control and efficient heat dissipation, featuring a flat shape with a significant increase in cross-sectional area along the longitudinal axis, ensuring homogeneous reaction conditions throughout the reactor.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If large-volume inlet and outlet hoods are used in conventional tube bundle reactors, then the reactor can handle high flow rates, but temperature control becomes difficult leading to hot spots and uncontrolled reactions

Engineering Contradiction:
Improveflow rateVSAvoidtemperature control
Core Design Contradiction:
ProductivityVSTemperature

Solution Approach 1:

The inlet hood is segmented into multiple inlet ports distributed across the hood surface, allowing the total flow to be divided into multiple smaller streams. This segmentation prevents any single location from becoming a hot spot while maintaining high overall flow rates through the reactor.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The hood design creates locally optimized flow conditions by distributing inlet ports across the hood surface rather than concentrating flow at a single point. Each local region receives a controlled portion of the total flow, ensuring uniform temperature distribution while maintaining high overall productivity.

Inventive Principle:
Principle #3Local quality

2Quantity of substance

If large-volume hoods are used in tube bundle reactors, then material handling capacity increases, but reaction selectivity decreases due to uncontrolled reactions and product loss

Engineering Contradiction:
Improvematerial handling capacityVSAvoidreaction selectivity
Core Design Contradiction:
Quantity of substanceVSManufacturing precision

Solution Approach 1:

The outlet hood is equipped with multiple outlet ports that segment the product stream into several controlled flows. This prevents uncontrolled reactions by ensuring that no single outlet region becomes a zone of excessive residence time or temperature, thereby maintaining high reaction selectivity while handling large quantities of material.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The distributed outlet port arrangement creates locally optimized exit conditions across the hood surface. Each local region maintains controlled residence time and temperature conditions, preventing product degradation and maintaining high selectivity even at high throughput levels.

Inventive Principle:
Principle #3Local quality

3Strength

If conventional tube bundle reactor design is used, then structural strength is adequate, but temperature uniformity and reaction stability are poor

Engineering Contradiction:
Improvestructural strengthVSAvoidtemperature uniformity
Core Design Contradiction:
StrengthVSStability of the object's composition

Solution Approach 1:

The hood design employs asymmetric port distribution and varying port sizes optimized for the specific reaction requirements. This asymmetric configuration creates more uniform flow patterns and temperature distribution compared to symmetric designs, while the overall structural strength is maintained through appropriate material selection and thickness.

Inventive Principle:
Principle #4Asymmetry

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This design enhances reaction selectivity and stability by maintaining uniform temperature and pressure conditions, preventing hot spots and uncontrolled reactions, even in critical situations, and is suitable for temperature-sensitive materials and reactions.

Implementation Method 1

featuring a flat shape with a significant increase in cross-sectional area along the longitudinal axis, ensuring homogeneous reaction conditions throughout the reactor

Methodology Applied
Scientific EffectHeat dissipation: Convection

Implementation Method 2

The reaction conditions are controlled via operating parameters such as temperature, pressure and flow rate within the reactor

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Data Source

PatentEP2389241B1Tube bundle reactor and process for non-catalyzed or homogenously catalyzed reactions
Publication Date: 2018.06.06 BASF SE
  • EP2389241B1 patent drawingFigure 1a~1b
  • EP2389241B1 patent drawingFigure 2
  • EP2389241B1 patent drawingFigure 3~4

AI summary

The invention relates to a tube bundle reactor having a flat feed dome. Alternatively, the discharge dome can also be designed flat. The flat design reduces the reaction heat developing in the hood in reaction types that take place not only in the tube bundle (non-catalyzed reactions and reactions with homogenously distributed catalyst). Undesired reactions that already take place in the dome due to accumulated heat are thus heavily suppressed, whereby greater selectivity in temperature-sensitive reactions is achieved. Additionally, the temperature distribution within the domes can be precisely controlled. The tube bundle reactor comprises a tube bundle that has a feed end connected to a feed dome of the tube bundle reactor, wherein the feed dome is designed in a flat shape having a cross-sectional surface at the feed end and an inner volume, and the ratio of the inner volume to the cross-sectional surface is less than 0.35 m. The invention is furthermore implemented by a method for operating a tube bundle reactor, comprising: introducing a reactant mixture into a tube bundle and converting at least a portion of the reactant mixture into a product inside the tube bundle. The introduction step comprises: feeding the reactant mixture into an inner space of a feed dome of the tube bundle reactor and forwarding the reactant mixture into a feed end of the tube bundle in the form of a fluid flow. The fluid flow has a cross-sectional surface upon entering the feed end and the inner space of the feed dome through which the fluid flows has an inner volume; wherein the ratio of the inner volume to the cross-sectional surface is less than 0.35 m.