Flotation Contactor with Throttling Duct for Bubble Size Control

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Solution Overview

Problem

Current flotation technologies face inefficiencies in separating fine and coarse particles due to limitations in bubble size control, shear intensity, and turbulence, leading to reduced recovery rates, especially for particles outside the intermediate size range.

Innovation Solution

An apparatus and method that generate fine bubbles and increase shear intensity by using a contactor with a throttling duct and flow manipulator to create a high-energy dissipation rate environment, ensuring intimate contact between bubbles and particles, and a draft tube to assist coarse particles in rising to the froth.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If conventional aeration devices are used to distribute bubbles uniformly across the column cross-section, then bubble distribution is improved, but bubble size becomes too large (1-5 mm) for effective fine particle capture

Engineering Contradiction:
Improvebubble distribution uniformityVSAvoidbubble size control
Core Design Contradiction:
Ease of operationVSManufacturing precision

Solution Approach 1:

The aeration system is segmented into multiple independent porous sparger elements distributed across the column cross-section. Each sparger generates bubbles locally, allowing precise control of bubble size while maintaining uniform distribution through the segmented arrangement rather than a single large aeration device

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Porous sparger materials are used to generate fine bubbles through the porous structure. The porous nature of the sparger elements creates numerous small bubble nucleation sites, producing bubble sizes suitable for fine particle capture while maintaining uniform distribution across the column

Inventive Principle:
Principle #31Porous materials

2Loss of time

If tall column cells (height-to-diameter ratio 2:1 to 10:1) are used to provide sufficient contact time, then particle-bubble contact time is improved, but device complexity and space requirements increase

Engineering Contradiction:
Improvecontact timeVSAvoidcolumn height
Core Design Contradiction:
Loss of timeVSDevice complexity

Solution Approach 1:

Particle-bubble contact occurs preliminarily in a dedicated contactor device before the particles enter the main separation column. This preliminary contact action allows most particle capture to occur in a compact volume, reducing the required height of the separation column while maintaining adequate contact time

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

A separate contactor device acts as an intermediary between the aeration system and the separation column. This intermediary component provides a dedicated zone for intensive particle-bubble contact, decoupling the contact time requirement from the overall column height and allowing the column to be more compact

Inventive Principle:
Principle #24Intermediary (Mediator)

3Productivity

If high gas fractions are used to improve fine particle flotation, then fine particle recovery is improved, but coarse particle separation efficiency deteriorates due to excessive turbulence

Engineering Contradiction:
Improvefine particle recoveryVSAvoidcoarse particle separation
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The flotation system is segmented into two distinct operational zones: a high gas fraction contactor zone for fine particle capture and a low gas fraction separation zone for coarse particle handling. This segmentation allows each zone to be optimized for its specific particle size range without the adverse effects of the other zone's operating conditions

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Different local conditions are provided in different zones of the system. The contactor zone has high gas fraction and intense turbulence optimized for fine particles, while the separation column has low gas fraction and calm conditions optimized for coarse particles. Each zone has locally optimized quality parameters matched to its function

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly improves the recovery of fine and coarse particles by reducing bubble size, increasing shear intensity, and controlling the gas-liquid mixture, resulting in enhanced flotation efficiency and reduced operational costs.

Implementation Method 1

a contactor arranged to receive under pressure a supply of feed slurry incorporating particles suspended in a liquid and a supply of gas, the contactor being arranged to mix the slurry with the air forming a gas-liquid bubbly two-phase mixture

Methodology Applied
Scientific EffectGas-liquid mixing:

Implementation Method 2

an outlet from the contactor configured to provide a restriction to the flow of mixture therethrough and maintain the mixture within the contactor under pressure

Methodology Applied
Scientific EffectThrottling:

Implementation Method 3

a flow manipulator downstream from the outlet configured to induce a high energy dissipation rate within the mixture passing therethrough

Methodology Applied
Scientific EffectEnergy dissipation:

Implementation Method 4

increase shear intensity by using a contactor with a throttling duct and flow manipulator to create a high-energy dissipation rate environment

Methodology Applied
Scientific EffectShear: Shear Stress

Implementation Method 5

a separation cell arranged to receive mixture from the flow manipulator and allow bubbles with attached particles to rise to the surface of liquid within the cell

Methodology Applied
Scientific EffectBuoyancy: Archimedes' Principle (Buoyancy)

Implementation Method 6

chemical reagents or collectors which have the effect of making the particles which it is desired to remove, water repellent or hydrophobic

Methodology Applied
Scientific EffectHydrophobicity: Hydrophobe

Implementation Method 7

The hydrophobic particles attach to the air bubbles and rise to the surface of the cell, from which they can be removed by flowing over a lip under the action of gravity

Methodology Applied
Scientific EffectGravity: Gravitation

Data Source

PatentUS9656273B2Method and apparatus for contacting bubbles and particles in a flotation separation system
Publication Date: 2017.05.23 UNIV OF NEWCASTLE RES ASSOCS
  • US9656273B2 patent drawing
  • US9656273B2 patent drawing
  • US9656273B2 patent drawing

AI summary

A flotation separation apparatus for separating particles in suspensions, feeds slurry containing the particles through an inlet into a contactor where gas is fed through an inlet to mix with the slurry, for example in a downwardly plunging jet, to form a gas-liquid bubbly two-phase mixture under pressure from an outlet restriction in a throttling duct. The mixture is passed through a flow manipulator configured to induce a high energy dissipation rate, for example by way of a Shockwave formed in a diverging section of the throttling duct reducing the size of the bubbles and brining those bubbles into intimate contact with particles in the mixture which is released into a separation cell where a flow manipulating draft tube is provided to reduce turbulence in the mixture. Alternative apparatus and methods for inducing the high energy dissipation rate and for reducing turbulence in the mixture are also described and claimed.