Flow Rate Amplification Nozzle for Polysilicon Reactor Gas Circulation

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Solution Overview

Problem

Conventional reactors for manufacturing polycrystalline silicon rods using the Siemens method face issues with non-uniform gas circulation and reduced jetting efficiency, leading to surface unevenness, diameter inconsistencies, and increased impurity contamination due to insufficient gas flow rates and force.

Innovation Solution

The implementation of flow rate amplification nozzles that mix silicon deposition raw material gas with the reactor atmosphere, enhancing the gas flow rate and jetting force by utilizing a Venturi effect and Bernoulli's principle, ensuring better circulation and uniformity within the reactor.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Device complexity

If a straight barrel pipe type gas supply nozzle is used to supply silicon deposition raw material gas, then the nozzle structure is simple, but the gas flow rate decreases considerably before reaching the upper wall and raw material gas utilization efficiency becomes inferior

Engineering Contradiction:
Improvenozzle structureVSAvoidraw material gas utilization efficiency
Core Design Contradiction:
Device complexityVSProductivity

Solution Approach 1:

The nozzle structure is changed from a straight barrel pipe to a curved nozzle body that guides the gas flow dynamically along its length. The curved geometry allows the gas flow to adapt to the nozzle shape, maintaining higher flow rates and improving utilization efficiency while adding moderate structural complexity.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The nozzle design incorporates a curved three-dimensional path instead of a straight linear structure. This dimensional change allows the gas flow to traverse a more efficient path, maintaining higher velocities and improving gas utilization before reaching the upper wall of the reaction chamber.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Productivity

If the gas flow rate is increased to improve circulation, then raw material gas utilization efficiency improves, but surface unevenness and diameter non-uniformity occur in the polycrystalline silicon rod

Engineering Contradiction:
Improveraw material gas utilization efficiencyVSAvoidrod surface uniformity
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The curved nozzle structure creates localized flow patterns that distribute gas more uniformly across the reaction chamber. The curved geometry focuses the gas flow in specific regions, improving local gas utilization efficiency while maintaining overall rod surface uniformity through controlled flow distribution.

Inventive Principle:
Principle #3Local quality

3Ease of operation

If a side wall jetting port is added to form a hooking concave portion, then the hanging tool can be conveyed, but the jetting force of the raw material gas is reduced

Engineering Contradiction:
Improverod conveyanceVSAvoidgas jetting force
Core Design Contradiction:
Ease of operationVSForce

Solution Approach 1:

The nozzle function is segmented into two parts: the curved nozzle body that maintains high jetting force for gas delivery, and a separate hooking concave portion formed by controlled gas flow that provides conveyance functionality. This segmentation allows each function to be optimized independently.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The curved nozzle structure acts as an intermediary that guides and focuses the gas flow to create the hooking concave portion while maintaining the primary jetting function. The curved geometry serves as a mediator between the gas supply and the two functional requirements (jetting and hook formation).

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly improves the uniformity of polycrystalline silicon rod manufacturing by increasing gas flow rates and jetting force, reducing surface irregularities and impurity contamination, while enhancing the efficiency of raw material utilization and power intensity.

Implementation Method 1

flow rate amplification nozzles that mix silicon deposition raw material gas with the reactor atmosphere, enhancing the gas flow rate and jetting force by utilizing a Venturi effect and Bernoulli's principle

Methodology Applied
Scientific EffectVenturi effect: Venturi Effect

Implementation Method 2

flow rate amplification nozzles that mix silicon depositionraw material gas with the reactor atmosphere, enhancing the gas flow rate and jetting force by utilizing a Venturi effect and Bernoulli's principle

Methodology Applied
Scientific EffectBernoulli's principle: Bernoulli Effect

Implementation Method 3

the silicon core wires are heated to a silicon deposition temperature by energization, and in this state, a silicon deposition raw material gas composed of a silane compound such as trichlorosilane (SiHCl3) and monosilane (SiH4) and a reducing gas is supplied into an reaction chamber to deposit silicon on the silicon core wires by a chemical vapor deposition method

Methodology Applied
Scientific EffectChemical vapor deposition: Chemical Vapour Deposition

Data Source

PatentEP3763673B1Polycrystalline silicon rod manufacturing method, and reactor
Publication Date: 2023.04.19 TOKUYAMA CORP
  • EP3763673B1 patent drawingFigure 1(a)~1(b)
  • EP3763673B1 patent drawingFigure 2(a)~2(b)
  • EP3763673B1 patent drawingFigure 3(a)~3(b)

AI summary

[Problem] To develop a method for manufacturing a polycrystalline silicon rod using the Siemens process, wherein the jetting rate of a silicon deposition raw material gas from a gas supply nozzle is more greatly improved, thereby strengthening the force of the gas flow and achieving superior raw material gas circulation in an upper section and a lower section within a bell jar. [Solution] In a reactor for manufacturing a polycrystalline silicon rod, the polycrystalline silicon rod is manufactured by using, as at least one gas supply nozzle, a flow rate amplification nozzle provided with a function of amplifying the flow rate of the silicon deposition raw material gas supplied to the nozzle and jetting the gas.