Fluidic Assay Supports for Time-Domain Multiplex Decoding

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Solution Overview

Problem

Existing bead-based multiplexed diagnostics methods face limitations in the number of multiplexing levels due to the need for well-resolved spectral properties of encoding dyes, requiring costly equipment and limiting detection speed.

Innovation Solution

Employ time-domain decoding methods that utilize encoding agents with similar spectral properties but different stabilities, allowing for physical and chemical changes in response to defined events to distinguish populations, without the need for additional optical filters or costly equipment.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If traditional spectral decoding methods are used with multiple dyes at different intensity levels, then multiple analytes can be detected, but the number of multiplexing levels is limited and costly equipment is required

Engineering Contradiction:
Improvemultiplexing capabilitiesVSAvoidequipment complexity
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The patent changes the decoding parameter from spectral properties to temporal stability. Encoding agents with different photostabilities are used, and decoding is achieved by measuring fluorescence intensity changes over time during photobleaching. This allows multiple multiplexing levels to be distinguished using a single optical filter, dramatically reducing equipment complexity while increasing adaptability for multiplexed detection

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent transitions from spectral dimension decoding (different wavelengths) to temporal dimension decoding (different time behaviors during photobleaching). By measuring fluorescence intensity as a function of time during controlled photobleaching, the system extracts multiple encoding states from encoding agents that would appear identical in static spectral measurements, effectively adding a temporal dimension to the decoding process

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Adaptability or versatility

If multiple encoding dyes with different spectral properties are used, then multiplexing can be achieved, but detection speed is reduced and equipment cost increases

Engineering Contradiction:
Improvemultiplexing levelsVSAvoiddetection speed
Core Design Contradiction:
Adaptability or versatilityVSProductivity

Solution Approach 1:

The patent employs periodic illumination to induce controlled photobleaching of encoding agents. By applying light in periodic pulses and measuring fluorescence intensity changes during each pulse cycle, the system rapidly decodes multiple multiplexing levels through temporal analysis of photobleaching kinetics, significantly increasing detection speed compared to static spectral measurements

Inventive Principle:
Principle #19Periodic action

Solution Approach 2:

The patent maintains continuous monitoring of fluorescence intensity during the photobleaching process, extracting decoding information from the entire temporal trajectory of intensity changes rather than relying on discrete spectral snapshots. This continuous measurement approach maximizes information extraction from each encoding agent, improving detection speed and efficiency

Inventive Principle:
Principle #20Continuity of useful action

3Measurement precision

If encoding agents with different intensity levels are used, then bead populations can be distinguished, but spectral resolution requirements increase and practical upper limits are reached

Engineering Contradiction:
Improvebead population distinctionVSAvoidspectral resolution difficulty
Core Design Contradiction:
Measurement precisionVSDifficulty of detecting and measuring

Solution Approach 1:

The patent changes the measurement parameter from static fluorescence intensity to dynamic photobleaching rate. By monitoring how fluorescence intensity changes over time during controlled photobleaching, the system can distinguish encoding agents with similar initial intensities based on their different decay kinetics, eliminating the need for high spectral resolution while maintaining precise bead population distinction

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent transitions from static intensity measurement to dynamic temporal analysis. Encoding agents are differentiated by their time-dependent fluorescence decay characteristics during photobleaching rather than by their steady-state intensity levels. This dynamic approach allows precise distinction of multiple bead populations without requiring high spectral resolution, as the temporal evolution of fluorescence provides additional discriminatory information

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Increases multiplexing capabilities by resolving more distinct encoding states, enhancing detection speed and efficiency with a low-cost analytical platform.

Implementation Method 1

encoding agents with similar spectral properties but different stabilities, allowing for physical and chemical changes in response to defined events

Methodology Applied
Scientific EffectFluorescence: Fluorescence

Implementation Method 2

encoding agents with similar spectral properties but different stabilities, allowing for physical and chemical changes in response to defined events

Methodology Applied
Scientific EffectPhotobleaching: Photo-oxidation

Implementation Method 3

beads functionalized with biorecognition elements (such as antibodies, oligonucleotides, etc.)

Methodology Applied
Scientific EffectMolecular recognition: Adsorption

Data Source

PatentEP3957996B1Fluidic devices, kits, and solid supports for decoding methods for multiplexing assays
Publication Date: 2025.09.17 THE UNIV OF NORTH CAROLINA AT CHAPEL HILL
  • EP3957996B1 patent drawingFigure 1A
  • EP3957996B1 patent drawingFigure 1B
  • EP3957996B1 patent drawingFigure 1C

AI summary

Decoding methods are provided for identifying populations in assays, particularly multiplexing assays and those associated with fluidic devices.