Fluidized-Bed Reactor Gas Inlet Nozzle Segmentation

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Solution Overview

Problem

Fluidized-bed reactors for gas-phase polymerization of olefins have inefficiencies due to the large volume below the gas distribution grid, which increases construction costs and allows polymer particles to be deposited in non-productive areas, reducing production efficiency.

Innovation Solution

The reactor design includes a gas recycle line that splits into two horizontal branches tangentially connected below the gas distribution grid, an inverted cone-shaped grid with annular modules, and a polymer discharge pipe integrated with the grid, along with a non-pressure-resistant divider plate to maintain pressure equality and prevent particle deposition.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If a large gas inlet nozzle is used to introduce high amounts of fluidization gas, then the gas distribution is improved, but the volume below the gas distribution grid increases, leading to larger reactor size and higher construction costs

Engineering Contradiction:
Improvegas distributionVSAvoidreactor volume
Core Design Contradiction:
Ease of operationVSVolume of stationary object

Solution Approach 1:

The gas inlet nozzle is divided into multiple smaller nozzles arranged in a specific pattern below the gas distribution grid. This segmentation allows the same total gas flow to be distributed through multiple entry points, improving gas distribution uniformity while reducing the required volume below the grid compared to a single large nozzle

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The gas inlet system transitions from a single large-dimensional nozzle to multiple smaller nozzles distributed in a two-dimensional arrangement below the grid. This dimensional change maintains the necessary gas introduction capacity while minimizing the vertical space requirement below the distribution grid

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Ease of operation

If a large volume is provided below the gas distribution grid for gas inlet, then gas introduction is facilitated, but polymer particles can be deposited in this non-productive area, reducing production efficiency

Engineering Contradiction:
Improvegas introductionVSAvoidproduction efficiency
Core Design Contradiction:
Ease of operationVSProductivity

Solution Approach 1:

The gas introduction function is segmented into multiple small nozzles rather than one large opening, which reduces the surface area where polymer particles could deposit while maintaining effective gas distribution into the fluidized bed

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The harmful function of the large volume below the grid (particle deposition zone) is eliminated by minimizing this space through the use of multiple small nozzles, extracting only the necessary gas introduction capability while removing the non-productive deposition area

Inventive Principle:
Principle #2Taking out (Extraction)

3Volume of stationary object

If the gas recycle line is connected directly below the gas distribution grid, then the reactor volume is reduced, but polymer particles may be carried into the recycle line and deposited

Engineering Contradiction:
Improvereactor volumeVSAvoidparticle deposition
Core Design Contradiction:
Volume of stationary objectVSObject-affected harmful factors

Solution Approach 1:

The gas recycle line connection is positioned in a horizontal dimension below the gas distribution grid rather than vertically, creating a spatial separation that minimizes particle carry-over while maintaining compact reactor volume

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

Solution Approach 2:

The connection point of the gas recycle line is specifically positioned at a location below the gas distribution grid where gas velocity is lower and particle suspension is minimal, creating a local zone that is less prone to particle deposition while still achieving compact reactor design

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration reduces the non-productive volume below the gas distribution grid, enhances gas distribution for efficient polymerization, and prevents polymer particle deposition, thereby improving production efficiency and reducing construction costs.

Implementation Method 1

fluidized-bed reactors are used for carrying out such gas-phase polymerization processes and contain a bed of polymer particles which is maintained in a fluidized state by an upward flow of a fluidizing gas

Methodology Applied
Scientific EffectFluidization: Fluidisation

Implementation Method 2

a recycle gas line in which coolers for removing the heat of polymerization

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Implementation Method 3

a recycle gas compressor

Methodology Applied
Scientific EffectCompression: Compression

Data Source

PatentUS11400428B2Fluidized-bed reactor having multiple recycle gas inlet nozzles
Publication Date: 2022.08.02 BASELL POLYOLEFINE GMBH
  • US11400428B2 patent drawing
  • US11400428B2 patent drawing

AI summary

Fluidized-bed reactor for the gas-phase polymerization of olefins including a gas distribution grid installed in a lower part of the fluidized-bed reactor and a gas recycle line, which is equipped with a compressor and a heat exchanger and which is connected at the upper end with the top of the fluidized-bed reactor, wherein the gas recycle line splits at the lower end in at least two horizontal branches which are connected tangentially with the fluidized-bed reactor below the gas distribution grid and a process for preparing an olefin polymer carried out in the fluidized-bed reactor.