Fluorescence Spectral Shape Analysis for Oil Species Identification

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Solution Overview

Problem

Existing fluorometers are unable to accurately measure the concentration of different oil species in a liquid due to variations in fluorescence amplitude, leading to inaccurate results when calibrated for one species and encountering another.

Innovation Solution

An apparatus with a full scan UV to IR spectrometer and a microprocessor that analyzes the shape of the fluorescent response spectrum to identify the oil species and apply a calibration factor for precise concentration measurement, using a 3mW laser diode module as the excitation source.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If a fluorometer is calibrated for one oil species, then it can accurately measure that species, but it produces inaccurate results when a different species is present

Engineering Contradiction:
Improveconcentration measurement accuracyVSAvoidoil species compatibility
Core Design Contradiction:
Measurement precisionVSAdaptability or versatility

Solution Approach 1:

The patent uses fluorescence spectral shape analysis instead of amplitude-based measurement. Different oil species produce distinct fluorescence spectral shapes, allowing the system to identify and accurately measure various species without recalibration. The microprocessor compares the measured spectral shape against stored reference shapes to determine both species identity and concentration.

Inventive Principle:
Principle #32Color changes

Solution Approach 2:

The invention transitions from measuring fluorescence amplitude (single parameter) to analyzing fluorescence spectral shape (multiple parameters across different wavelengths). This parameter expansion allows differentiation between oil species that may have similar amplitudes but distinct spectral characteristics, resolving the contradiction between measurement accuracy and species adaptability.

Inventive Principle:
Principle #35Parameter changes

2Device complexity

If a fluorometer uses a single wavelength detection, then the device is simple, but it cannot distinguish between different oil species

Engineering Contradiction:
Improvedetection system simplicityVSAvoidoil species identification capability
Core Design Contradiction:
Device complexityVSLoss of information

Solution Approach 1:

The patent adds a spectral dimension to the detection system by measuring fluorescence across multiple wavelengths rather than at a single wavelength. This dimensional expansion provides sufficient information to distinguish between different oil species while maintaining relative device simplicity through the use of a spectrometer and computational analysis.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables automatic identification of oil species and accurate concentration determination by comparing the measured spectrum to known references, providing reliable measurements across various oil species.

Implementation Method 1

Many oils have a natural fluorescence and so, commonly, such measurement apparatus measure the amount or concentration of oil by the detection of fluorescence

Methodology Applied
Scientific EffectFluorescence: Fluorescence

Implementation Method 2

a detector for detecting the fluorescent response of a target material over a range of frequencies to produce a response spectrum for the material

Methodology Applied
Scientific EffectSpectroscopy: Absorption Spectroscopy

Data Source

PatentEP2433117B1Method and apparatus for measuring fluorescent material in a liquid
Publication Date: 2016.10.26 ADVANCED SENSORS
  • EP2433117B1 patent drawingFigure 1
  • EP2433117B1 patent drawingFigure 2

AI summary

A method of measuring the amount of a fluorescent material in a liquid, said method comprising the steps of exciting said fluorescent material and measuring the fluorescent response of the material over a range of wavelengths to determine a response spectrum, identifying the material from said response spectrum and determining the amount of said material as a function of the amplitude of the fluorescent response and a calibration factor based upon said identification of the material.