Fluorinated Ether Lubricant Solubility in HCFO

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Solution Overview

Problem

Hydrochlorofluoroolefins have insufficient solubility for fluorinated ether compounds with perfluoropolyether chains and CF3 groups at both terminals, particularly when the perfluoropolyether chain lacks a branched structure, limiting their use in forming uniform lubricant coating films with minimal environmental impact.

Innovation Solution

A lubricant solution comprising a hydrochlorofluoroolefin and specific solvents like 1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorohexane, nonafluorobutyl methyl ether, and 3-methoxy-4-trifluoromethyl-1,1,2,2,3,4,5,5-decafluoropentane, combined with a fluorinated ether compound having a perfluoropolyether chain without a branched structure, enhances solubility and allows for the formation of a uniform coating film.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Object-affected harmful factors

If hydrochlorofluoroolefin is used as solvent, then environmental impact is reduced, but solubility of fluorinated ether compound deteriorates

Engineering Contradiction:
Improveenvironmental impactVSAvoidsolubility
Core Design Contradiction:
Object-affected harmful factorsVSReliability

Solution Approach 1:

The patent introduces a co-solvent system where hydrofluorocarbon acts as an intermediary substance that bridges the solubility gap. The hydrofluorocarbon component specifically interacts with the fluorinated ether compound to enhance solubility, while the hydrochlorofluoroolefin maintains the environmentally friendly profile, thus mediating between environmental requirements and solubility needs

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent creates a composite solvent system combining hydrochlorofluoroolefin and hydrofluorocarbon in specific proportions. This composite approach leverages the environmental benefits of hydrochlorofluoroolefin while incorporating the superior solubility properties of hydrofluorocarbon, achieving a synergistic effect that resolves the contradiction between environmental impact and solubility

Inventive Principle:
Principle #40Composite materials

2Object-affected harmful factors

If hydrochlorofluoroolefin is used as solvent, then environmental impact is reduced, but uniformity of coating film deteriorates

Engineering Contradiction:
Improveenvironmental impactVSAvoiduniformity of coating film
Core Design Contradiction:
Object-affected harmful factorsVSManufacturing precision

Solution Approach 1:

The hydrofluorocarbon co-solvent acts as a mediator that ensures uniform distribution and evaporation characteristics. It facilitates the formation of a homogeneous coating solution that dries uniformly, while the hydrochlorofluoroolefin maintains the environmentally friendly profile, thus mediating between environmental requirements and coating uniformity

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent optimizes the compositional parameters of the solvent system, specifically the ratio of hydrochlorofluoroolefin to hydrofluorocarbon, to achieve optimal coating uniformity. By adjusting these parameters within specified ranges, the patent ensures both environmental benefits and manufacturing precision of uniform coating films

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution achieves excellent solubility and forms a uniform lubricant coating film with a small environmental impact, using hydrochlorofluoroolefins and specific solvents to dissolve fluorinated ether compounds, thereby addressing the solubility issues and environmental concerns.

Implementation Method 1

a lubricant solution comprising a solvent composition which comprises a hydrochlorofluoroolefin and at least one member selected from the group consisting of 1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorohexane, 1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorooctane, nonafluorobutyl methyl ether, nonafluorobutyl ethyl ether and 3-methoxy-4-trifluoromethyl-1,1,1,2,2,3,4,5,5,5-decafluoropentane, and a fluorinated ether compound

Methodology Applied
Scientific EffectSolubility: Solvation

Implementation Method 2

a method for producing a substrate provided with a lubricant coating film, which comprises applying the lubricant solution as defined in any one of [1] to 6] to a substrate, and then evaporating the solvent composition to form a coating film of the fluorinated ether compound on the surface of the substrate

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentUS11530363B2Lubricant solution, method for producing substrate provided with lubricant coating film
Publication Date: 2022.12.20 AGC INC

AI summary

To provide a lubricant solution capable of forming a uniform coating film by using a solvent composition which has a small impact on the global environment and which is excellent in solubility of the fluorinated ether compound, and a method for producing a substrate provided with a lubricant coating film.A lubricant solution comprising a solvent composition which comprises a HCFO and at least one member selected from the group consisting of 1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorohexane, 1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorooctane, nonafluorobutyl methyl ether, nonafluorobutyl ethyl ether and 3-methoxy-4-trifluoromethyl-1,1,1,2,2,3,4,5,5,5-decafluoropentane, and a fluorinated ether compound which is a fluorinated ether compound having a perfluoropolyether chain and CF3 groups at both terminals, wherein the perfluoropolyether chain does not have a branched structure.