Fluoropolymer Film Adhesion to Rubber Substrates

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Solution Overview

Problem

Existing fluoropolymer films fail to adhere firmly to rubber substrates and withstand the necessary baking temperature, leading to substrate deterioration and inadequate heat resistance in applications like copier and printer rolls.

Innovation Solution

A laminate comprising a substrate with a metal oxide and a functional group-containing fluoropolymer coating layer, specifically a phosphate group-containing fluoropolymer copolymerized with tetrafluoroethylene and perfluoro(alkyl vinyl ether), which provides adequate adhesion and heat resistance when baked at temperatures tolerable by the substrate.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional fluoropolymer paint or PFA coating is applied to rubber rollers, then non-stickiness and heat resistance are improved, but adhesion to the rubber substrate deteriorates

Engineering Contradiction:
Improveheat resistanceVSAvoidadhesion
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The patent introduces a silane-coupling agent as an intermediary substance between the rubber substrate and the fluoropolymer coating. This coupling agent contains both silicone groups that bond with the rubber substrate and fluoropolymer-compatible groups that bond with the coating, thereby resolving the adhesion problem while maintaining heat resistance and non-stick properties

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent creates a composite coating system consisting of rubber substrate, silane-coupling agent layer, and fluoropolymer coating layer. This multi-layer composite structure allows each layer to perform its specific function: the rubber provides flexibility, the silane layer provides adhesion, and the fluoropolymer provides non-stickiness and heat resistance

Inventive Principle:
Principle #40Composite materials

2Strength

If fluoropolymer is coated using silicone-based adhesive, then adhesion is improved, but heat resistance deteriorates due to poor heat resistance of the silicone adhesive

Engineering Contradiction:
ImproveadhesionVSAvoidheat resistance
Core Design Contradiction:
StrengthVSReliability

Solution Approach 1:

The silane-coupling agent layer acts as a thin, sacrificial intermediary that provides sufficient adhesion during the coating process and under operating conditions, but does not compromise the overall heat resistance of the fluoropolymer coating system. The coupling agent layer is designed to be thin enough to not interfere with the heat resistance properties of the main fluoropolymer coating

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Manufacturing precision

If high baking temperature is used to form fluoropolymer film, then film formation and adhesion are improved, but substrate deterioration occurs

Engineering Contradiction:
Improvefilm formationVSAvoidsubstrate deterioration
Core Design Contradiction:
Manufacturing precisionVSObject-affected harmful factors

Solution Approach 1:

The silane-coupling agent layer serves as a heat-resistant intermediary that allows the fluoropolymer coating to be formed at reduced temperatures. This coupling layer protects the rubber substrate from direct exposure to high baking temperatures while still enabling proper film formation and adhesion of the fluoropolymer coating

Inventive Principle:
Principle #24Intermediary (Mediator)

4Adaptability or versatility

If rubber rollers are used for fusing systems, then flexibility is maintained, but durability deteriorates due to coating degradation

Engineering Contradiction:
ImproveflexibilityVSAvoiddurability
Core Design Contradiction:
Adaptability or versatilityVSDuration of action of stationary object

Solution Approach 1:

The patent creates a durable composite structure where the rubber substrate maintains flexibility while the fluoropolymer coating layer provides long-term durability, non-stickiness, and heat resistance. The silane-coupling agent layer ensures strong bonding between these two components, preventing coating degradation and extending the service life of the roller

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution enables the formation of a flexible, heat-resistant fluoropolymer film that adheres firmly to elastomer substrates, maintaining heat resistance during use and extending the lifespan of components like fuser and pressure rolls in copiers and printers.

Implementation Method 1

a laminate, comprising a substrate containing a metal oxide, and a functional group-containing fluoropolymer coating layer formed thereon

Methodology Applied
Scientific EffectChemical bonding: Chemical Bonding

Data Source

PatentUS7544406B2Laminate with fluoropolymer film and film-forming fluoropolymer
Publication Date: 2009.06.09 THE CHEMOURS CO FC LLC

AI summary

A functionalized fluoropolymer, preferably with phosphate functionality, can be coated on a metal oxide containing rubber substrate, which coating, after heating, results in a fluoropolymer-rubber substrate laminate without degradation of the rubber, and with good adhesion between the fluoropolymer and the rubber.