Flow-Enhanced Non-Linear Magnetophoresis for Particle Separation

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Solution Overview

Problem

Current bio-separation techniques, such as liquid chromatography, electrophoresis, and linear magnetophoresis, are slow and face challenges with particle coagulation, making them inefficient for multiple separations and complex sample analysis.

Innovation Solution

A flow-enhanced non-linear magnetophoretic (F-NLM) separator using a chip-based device with distinct fluid paths and magnetic arrays, where a rotating magnetic field and controlled flow rates selectively trap and transport particles based on their magnetic properties, allowing for efficient separation of different particle types.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If linear magnetophoresis is used with a very strong magnetic field and field gradient, then separation of particles can be achieved, but magnetic particles coagulate to form undetectable complexes such as chains

Engineering Contradiction:
Improveseparation resolutionVSAvoidparticle coagulation
Core Design Contradiction:
Measurement precisionVSStability of the object's composition

Solution Approach 1:

The patent applies a rotating magnetic field instead of a static strong magnetic field. The field rotates at a frequency that prevents particles from settling into fixed chains while still providing sufficient magnetic force for separation. This dynamic approach maintains particle dispersion while achieving separation based on magnetic moment differences.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The magnetic field is applied periodically through rotation at specific frequencies. By controlling the rotation frequency to match or exceed the particle response time, the system prevents coagulation while maintaining separation efficiency. The periodic reversal of field direction disrupts chain formation.

Inventive Principle:
Principle #19Periodic action

2Measurement precision

If conventional bio-separation techniques like liquid chromatography, electrophoresis, or centrifugation are used, then high resolution separation is achieved, but the process is slow and difficult to implement

Engineering Contradiction:
Improveseparation resolutionVSAvoidseparation speed
Core Design Contradiction:
Measurement precisionVSProductivity

Solution Approach 1:

The patent replaces mechanical separation mechanisms (chromatography columns, electrophoresis buffers, centrifugal force) with a magnetic field-based system. This substitution enables faster separation speeds while maintaining high resolution, as magnetic forces act directly on particles without requiring complex mechanical setups or long processing times.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Device complexity

If a single fluid path is used in the separation device, then device complexity is reduced, but the ability to separate multiple particle types simultaneously is limited

Engineering Contradiction:
Improvefluid path configurationVSAvoidmulti-particle type separation capability
Core Design Contradiction:
Device complexityVSAdaptability or versatility

Solution Approach 1:

The device divides the single fluid path into multiple parallel fluid paths, each equipped with its own magnetic array. This segmentation allows different particle types to be separated simultaneously in different channels based on their specific magnetic properties, while each individual channel remains relatively simple in design.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The magnetic array system is designed to be universally applicable across multiple fluid paths. The same basic magnetic array structure can be replicated and configured in different channels to handle various particle types, providing multi-functionality without significantly increasing overall device complexity.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables rapid and efficient separation of particles with high sensitivity to size and magnetic moment, improving the resolution and speed of bio-separation processes, particularly in complex mixtures like blood samples.

Implementation Method 1

a magnetic array provided proximal to the first fluid path such that particles within the sample operably experience an induced magnetic field causing a retention of particles of the first type within the first fluid path

Methodology Applied
Scientific EffectMagnetic field: Magnetic Field

Implementation Method 2

flow-enhanced non-linear magnetophoretic (F-NLM) separator... where a rotating magnetic field and controlled flow rates selectively trap and transport particles based on their magnetic properties

Methodology Applied
Scientific EffectMagnetophoresis:

Data Source

PatentEP2579988B1Non-linear magnetophoretic separation system and method
Publication Date: 2018.08.22 UNIV COLLEGE DUBLIN NAT UNIV OF IRELAND DUBLIN
  • EP2579988B1 patent drawingFigure 1(a)~1(c)
  • EP2579988B1 patent drawingFigure 2(a)
  • EP2579988B1 patent drawingFigure 2(b)

AI summary

A flow enhanced method and system for flow non-linear magnetophoresis (F-NLM) is described. By tuning an external field frequency and the flow rate the migration velocities of different bead types may be caused to differ by several orders of magnitude over an extended range of frequencies to allow for separation of particles. Use of such efficiency in separation in bio-separation and similar assays is described.