Self-supporting foam-geometry structures for adsorption

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Solution Overview

Problem

Conventional structures used in separation and catalysis processes, such as packed beds and monoliths, suffer from high pressure drops and inefficient mass transfer rates due to their physical limitations, leading to suboptimal performance in gas separation and catalytic reactions.

Innovation Solution

The development of self-supporting foam-geometry structures with greater than 50% active material by weight, featuring tortuous channels and varying pore densities, which enhance fluid flow paths and volumetric efficiency while reducing weight and size.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If packed beds are used with conventional extrusions of small sphere-like active materials, then the structures can be easily manufactured, but large pressure drops occur and mass transfer rates are inefficient

Engineering Contradiction:
Improveease of manufactureVSAvoidmass transfer rate
Core Design Contradiction:
Ease of manufactureVSProductivity

Solution Approach 1:

The patent applies porous foam-geometry structures with interconnected voids and struts to replace conventional packed beds. The porous architecture provides tortuous flow paths that enhance mass transfer rates while maintaining ease of manufacture through direct formation processes. The interconnected pore structure allows efficient fluid distribution and contact with active material surfaces.

Inventive Principle:
Principle #31Porous materials

Solution Approach 2:

The invention transitions from zero-dimensional packed spheres to three-dimensional foam-geometry structures with complex internal architectures. This dimensional transformation creates tortuous channels and interconnected voids that improve fluid flow patterns and mass transfer efficiency while maintaining structural integrity and manufacturability.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Productivity

If monolith substrates are used as engineered structures with active material coatings, then pressure drops are reduced, but the majority of weight is inactive structural material

Engineering Contradiction:
Improvepressure dropVSAvoidweight
Core Design Contradiction:
ProductivityVSWeight of moving object

Solution Approach 1:

The patent employs porous foam-geometry structures where the entire structure consists of active material distributed throughout the porous matrix. This eliminates the need for heavy inactive structural substrates while maintaining the low pressure drop characteristics of engineered structures through the open-cell foam architecture and tortuous flow paths.

Inventive Principle:
Principle #31Porous materials

Solution Approach 2:

The invention creates composite foam structures combining active material with binder materials in a porous matrix. This composite approach provides both structural support and catalytic/adsorptive functionality throughout the entire volume, eliminating the separation between structural and active components found in coated monoliths.

Inventive Principle:
Principle #40Composite materials

3Ease of manufacture

If conventional extrusions of small sphere-like active materials are used in packed beds, then the structures can be easily manufactured, but the equipment size and weight increase

Engineering Contradiction:
Improveease of manufactureVSAvoidequipment size
Core Design Contradiction:
Ease of manufactureVSVolume of stationary object

Solution Approach 1:

The patent uses porous foam-geometry structures that provide high surface area to volume ratios, enabling compact equipment design. The interconnected porous network allows efficient fluid distribution and contact with active material, achieving high productivity in smaller equipment volumes while maintaining ease of manufacture through direct formation processes.

Inventive Principle:
Principle #31Porous materials

Solution Approach 2:

The foam-geometry structure with its hierarchical porous architecture creates nested voids and channels at multiple scales. This nested structure maximizes the utilization of available volume for active material and fluid flow, reducing the overall equipment size required for a given processing capacity.

Inventive Principle:
Principle #7Nested doll (Nesting)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

These structures provide improved interaction between the active material and fluid streams, increasing working capacity and volumetric efficiency, reducing equipment size and weight, and minimizing pressure drops, thus enhancing the efficiency of separation and catalysis processes.

Implementation Method 1

the self-supporting structure is a foam-geometry structure configured to provide one or more tortuous channels for fluid flow paths through the self-supporting structure

Methodology Applied
Scientific EffectAdvection: Advection

Implementation Method 2

For adsorption process, the adsorbent materials preferentially adsorbs one or more gas components, while not adsorbing one or more other gas components. The non-adsorbed components are recovered as a separate product.

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 3

When the pressure is reduced, the adsorbed component is released, or desorbed from the adsorbent material.

Methodology Applied
Scientific EffectDesorption: Desorption

Data Source

PatentEP3558490B1Self-supporting structures having foam-geometry structure and active materials
Publication Date: 2022.06.29 EXXONMOBIL TECHNOLOGY & ENGINEERING CO
  • EP3558490B1 patent drawingFigure 1
  • EP3558490B1 patent drawingFigure 2~3B
  • EP3558490B1 patent drawingFigure 3C~4

AI summary

A method and system for manufacturing and using a self-supporting structure in processing unit for adsorption or catalytic processes. The self-supporting structure has greater than 50% by weight of the active material in the self-supporting structure to provide a foam- geometry structure providing access to the active material. The self-supporting structures, which may be disposed in a processing unit, may be used in swing adsorption processes and other processes to enhance the recovery of hydrocarbons.