Syntactically Foamed Adhesive Mixing via Inhomogeneous Temperature Control

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing methods for producing syntactically foamed polymer compositions, such as pressure-sensitive adhesives, face challenges in maintaining homogeneity and reducing mechanical and thermal stress on matrix polymers, leading to microballoon destruction and uneven expansion, which affects the quality and consistency of the final product.

Innovation Solution

The method involves introducing expandable microballoons into a matrix material and controlling the temperature distribution in the mixing unit to create an inhomogeneous temperature field, with one surface heated to initiate expansion and the other surface kept cooler, allowing for gentle expansion and mixing in a planetary roller extruder, thereby reducing microballoon destruction and enhancing homogeneity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If uniform temperature distribution is used in the mixing unit, then the expansion of microballoons is controlled, but the mixing homogeneity deteriorates and microballoon destruction increases

Engineering Contradiction:
Improvemicroballoon expansion controlVSAvoidmixture homogeneity
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent applies local quality by creating different temperature zones within the mixing unit: a first region with temperature T1 that promotes microballoon expansion and a second region with temperature T2 that maintains mixture homogeneity. This spatial differentiation of temperature allows simultaneous achievement of controlled expansion and uniform mixing, resolving the contradiction between reliability of expansion control and stability of composition.

Inventive Principle:
Principle #3Local quality

2Productivity

If high temperature is applied to expand microballoons, then the expansion capacity increases, but the mechanical and thermal stress on matrix polymers increases leading to degradation

Engineering Contradiction:
Improvemicroballoon expansion capacityVSAvoidpolymer degradation
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The patent implements local quality by concentrating high temperature (T1) only in the first region where microballoon expansion occurs, while maintaining lower temperature (T2) in the second region where matrix polymers are processed. This localized thermal application enables high expansion capacity without subjecting the entire matrix to excessive thermal stress, thus reducing polymer degradation.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The mixing unit is segmented into two distinct temperature regions: a first region for microballoon expansion and a second region for homogeneous mixing at lower temperature. This segmentation allows the expansion process to occur at high temperature in a controlled zone while protecting the bulk matrix material from thermal degradation, resolving the contradiction between productivity and harmful effects.

Inventive Principle:
Principle #1Segmentation

3Productivity

If rapid mixing is performed, then the productivity increases, but the mechanical stress on microballoons increases causing destruction

Engineering Contradiction:
Improvemixing speedVSAvoidmicroballoon integrity
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent applies local quality by creating a specific thermal environment in the first region with temperature T1 that facilitates gentle microballoon expansion, while the second region with temperature T2 provides a protective environment for the matrix. This spatial differentiation allows rapid mixing to occur without subjecting microballoons to excessive mechanical stress, maintaining their integrity while improving productivity.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach results in a highly homogeneous mixture with early and controlled expansion of microballoons, reducing polymer degradation, achieving smoother surfaces, and improving the mechanical properties of the final product with reduced roughness and increased fatigue resistance.

Implementation Method 1

the expansion of the expandable microballoons takes place after they have been introduced into the matrix material... the temperature distribution in the mixing aggregate (1) is inhomogeneous in a sectional plane transverse to the conveying direction of this unit (1)... a first surface (3) of the mixing chamber (2) delimiting the mixing space (2) is heated to such a high temperature that the temperature (T E ), which is sufficient for the start and progress of the expansion, is reached in the polymer mass containing microballoons, insofar as it comes into contact with this first limiting surface (3)

Methodology Applied
Scientific EffectThermal expansion: Thermal Expansion

Implementation Method 2

the temperature distribution in the mixing aggregate (1) is inhomogeneous in a sectional plane transverse to the conveying direction of this unit (1)... a first surface (3) of the mixing chamber (2) delimiting the mixing space (2) is heated to such a high temperature that the temperature (T E ), which is sufficient for the start and progress of the expansion, is reached in the polymer mass containing microballoons, insofar as it comes into contact with this first limiting surface (3), while in the same section transverse to the conveying direction of the mixing aggregate (1), a second surface (4) of the mixing aggregate (1) delimiting the mixing space (2) is at such a low temperature that in the polymer mass containing microballoons, insofar as it is in contact with this second limiting surface (4), the temperature (T E ), which is sufficient to start and progress the expansion, is not reached

Methodology Applied
Scientific EffectTemperature gradient: Temperature Gradient

Data Source

PatentEP2801461B1Method for producing a syntactically foamed polymer composition, preferably a pressure-sensitive adhesive mass
Publication Date: 2019.07.10 TESA SE
  • EP2801461B1 patent drawingFigure 1

AI summary

Method and apparatus for producing a syntactically foamed polymer mass, preferably a pressure-sensitive adhesive, wherein at least the majority of the enclosed foam cavities are achieved by introducing expandable microballoons into a matrix material and subsequent mixing, and the expansion of the expandable microballoons takes place after their introduction into the matrix material, wherein the temperature distribution in the mixing unit (1) is inhomogeneous in a cross-sectional plane transverse to the conveying direction of this unit, wherein in a cross-sectional plane transverse to the conveying direction of the mixing unit, a first surface (3) of the mixing unit bounding the mixing chamber (2) is heated to such a high temperature that a temperature sufficient for the start and progression of expansion is reached in the polymer mass containing the microballoons, while in the same cross-sectional plane, a second surface (4) of the mixing unit bounding the mixing chamber is heated to such a low temperature,that the polymer mass containing the microballoons does not reach a temperature sufficient to initiate and continue the expansion.