FTIR Condensation Testing Across Wide Temperature Ranges

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Solution Overview

Problem

Existing Fourier transform infrared spectrometers cannot perform online condensation research of volatile materials at different temperatures, limiting the ability to obtain continuous data on volatile matter released by materials at various condensation temperatures.

Innovation Solution

A real-time spectrum testing device comprising a testing module, vacuum module, temperature control module, and an FTIR spectrometer, which allows for the measurement of spectral characteristics of volatile condensable materials at different condensation temperatures across a wide temperature range.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If an existing Fourier transform infrared spectrometer is used, then the infrared spectrum of a normal-temperature sample can be tested, but it cannot implement online condensation research or obtain continuous data at different condensation temperatures

Engineering Contradiction:
Improvetemperature range adaptabilityVSAvoidmeasurement capability for condensation research
Core Design Contradiction:
Adaptability or versatilityVSReliability

Solution Approach 1:

The patent applies the dynamics principle by making the testing system adaptable to different temperature conditions. A temperature control system with heating and cooling capabilities is integrated into the testing cabin, allowing the environment to be dynamically adjusted. This enables the FTIR spectrometer to perform measurements across a wide temperature range from cryogenic to elevated temperatures, transforming a static normal-temperature testing device into a dynamic multi-temperature testing system that can conduct online condensation research

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent implements parameter changes by modifying the operating temperature parameter of the testing system. By integrating temperature control mechanisms (heating sheets, cooling systems) and vacuum control capabilities, the system can vary temperature and pressure parameters to simulate different space environment conditions. This allows continuous data collection at different condensation temperatures, enabling research on volatile matter behavior under varying thermal conditions

Inventive Principle:
Principle #35Parameter changes

2Reliability

If a vacuum environment is created for space simulation, then molecular pollution can be studied, but the complexity of the testing system increases with multiple control modules

Engineering Contradiction:
Improvevacuum environment simulation capabilityVSAvoidsystem structure complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent applies the merging principle by integrating multiple testing functions into a single unified vacuum testing cabin. The vacuum system, temperature control system (with heating and cooling), and FTIR spectrometer are combined within one enclosed chamber. This consolidation allows simultaneous control of vacuum conditions and temperature parameters while performing spectral measurements, reducing the need for multiple separate testing equipment and simplifying the overall system architecture

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The testing cabin is designed as a multi-functional universal platform that can perform multiple operations: creating vacuum environments for space simulation, controlling temperature across wide ranges, and conducting FTIR spectral measurements. This universal design allows a single system to replace multiple specialized devices, reducing overall system complexity while maintaining comprehensive testing capabilities for studying molecular pollution under various space-like conditions

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables continuous data collection on volatile matter release and condensation, providing essential reference data for preventing organic pollution in precision optical systems and informing effective protection measures.

Implementation Method 1

the vacuum module includes a vacuum inner cavity and a vacuum system; the vacuum inner cavity is installed in the testing cabin in a thermally insulated manner, and is connected to the vacuum system outside the testing cabin

Methodology Applied
Scientific EffectVacuum: Vacuum

Implementation Method 2

the temperature control module includes a refrigeration system and a temperature control system; the refrigeration system is connected to the standard testing lens by means of a refrigeration system interface installed on the cabin wall of the testing cabin

Methodology Applied
Scientific EffectCooling: Cooling

Implementation Method 3

the temperature control system is connected to the stage by means of a temperature control system interface installed on the cabin wall of the testing cabin

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 4

the FTIR spectrometer is configured to test infrared spectral characteristics of a volatile condensable material on the standard testing lens to obtain a spectral test result

Methodology Applied
Scientific EffectInfrared radiation: Infrared Radiation

Implementation Method 5

Molecules released at a high temperature condense at a low temperature range, which is referred to as molecular pollution

Methodology Applied
Scientific EffectCondensation: Condensation

Data Source

PatentUS12345630B2Real-time spectrum testing device for volatile condensable material in wide temperature range and testing method
Publication Date: 2025.07.01 SHANGHAI INSTITUTE OF TECHNICAL PHYSICS CHINESE ACADEMY OF SCIENCES
  • US12345630B2 patent drawing
  • US12345630B2 patent drawing
  • US12345630B2 patent drawing

AI summary

Provided are a real-time spectrum testing device for a volatile condensable material in a wide temperature range and a spectrum testing method by using the device. The device includes a testing module, a vacuum module, a temperature control module, and a spectrometer, where the testing module includes a testing cabin (5), a replaceable standard testing lens (2), and a stage (3); two infrared perspective windows (1) are symmetrically installed on two opposite side walls of the testing cabin (5); the vacuum module includes a vacuum inner cavity (8) and a vacuum system (4); the vacuum inner cavity (8) is installed in the testing cabin (5) in a thermally insulated manner and connected to the vacuum system (4); the stage (3) and the standard testing lens (2) are installed in the vacuum inner cavity (8); the temperature control module includes a refrigeration system (7) and a temperature control system (6).