Full-Beam X-Ray Scatterometry for Low-Correlation 3D Metrology

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Solution Overview

Problem

Current x-ray scatterometry systems face challenges in accurately measuring complex, three-dimensional semiconductor structures due to penetration issues and parameter correlation, especially with the increasing use of opaque materials and smaller feature sizes.

Innovation Solution

The implementation of full beam x-ray scatterometry systems that simultaneously measure the zero diffraction order and higher diffraction orders, using photon counting detectors with high dynamic range and thick, highly absorptive crystal substrates to absorb the direct beam without damage, thereby improving measurement accuracy and reducing parameter correlation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If traditional scatterometry measures only higher diffraction orders while blocking zero order, then measurement dynamic range is reduced, but direct beam information is lost

Engineering Contradiction:
Improvemeasurement accuracyVSAvoiddirect beam information
Core Design Contradiction:
Measurement precisionVSLoss of information

Solution Approach 1:

The patent combines the measurement of both zero order (direct beam) and higher diffraction orders into a single unified measurement process. The detector simultaneously captures both the direct beam and scattered radiation, merging previously separate measurement channels into one comprehensive system that preserves all beam information.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The patent extends the measurement from traditional single-dimension (higher orders only) to multi-dimension by incorporating zero order measurements alongside higher diffraction orders. This dimensional expansion in measurement space allows simultaneous capture of direct beam and scattered radiation intensities, providing more complete structural information.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Length of stationary object

If longer wavelengths are used to penetrate deep into 3D FLASH structures, then depth penetration is improved, but light intensity decreases and sensitivity is lost

Engineering Contradiction:
Improvepenetration depthVSAvoidlight intensity
Core Design Contradiction:
Length of stationary objectVSIllumination intensity

Solution Approach 1:

The patent changes the illumination wavelength parameter to X-ray range, which fundamentally alters the penetration characteristics. X-rays provide both deep penetration capability and sufficient interaction strength with the material, resolving the trade-off between penetration depth and measurement sensitivity that plagues longer wavelength optical methods.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent substitutes optical radiation with X-ray radiation, replacing the optical measurement mechanism with an X-ray scattering mechanism. This substitution enables deep penetration into opaque and high-aspect-ratio structures while maintaining measurement sensitivity through the detection of X-ray diffraction patterns.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Loss of information

If multiple angles of illumination and shorter wavelengths are used, then measurement information is increased, but device complexity increases

Engineering Contradiction:
Improvemeasurement informationVSAvoidsystem complexity
Core Design Contradiction:
Loss of informationVSDevice complexity

Solution Approach 1:

The patent creates a universal X-ray scatterometry system that can measure multiple parameters (critical dimensions, material composition, layer thicknesses) simultaneously through a single measurement configuration. The system uses fixed-angle X-ray illumination with detection of both zero and higher orders, providing multi-functional measurement capability without requiring complex multi-angle scanning mechanisms.

Inventive Principle:
Principle #6Universality (Multi-functionality)

4Device complexity

If conventional optical metrology is used on opaque high-k materials, then measurement simplicity is maintained, but measurement capability is lost

Engineering Contradiction:
Improvemeasurement simplicityVSAvoidmeasurement capability
Core Design Contradiction:
Device complexityVSReliability

Solution Approach 1:

The patent changes the fundamental measurement parameter from optical wavelength to X-ray wavelength, enabling penetration through and scattering from opaque high-k materials. This parameter change transforms the measurement capability to handle previously inaccessible materials while maintaining a relatively simple scatterometry measurement configuration.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables high throughput measurements with improved accuracy, allowing for the characterization of dimensions and material properties of semiconductor devices, including those with high aspect ratios and opaque materials, while reducing measurement uncertainty and parameter correlation.

Implementation Method 1

photon counting detectors with high dynamic range and thick, highly absorptive crystal substrates that absorb the direct beam without damage

Methodology Applied
Scientific EffectAbsorption (EM radiation): Absorption (EM radiation)

Implementation Method 2

scatterometry and reflectometry implementations and associated analysis algorithms are commonly used to characterize critical dimensions, film thicknesses, composition and other parameters of nanoscale structures

Methodology Applied
Scientific EffectX-ray scattering: Scattering

Implementation Method 3

detecting the intensities of the resulting zero diffraction order and higher diffraction orders

Methodology Applied
Scientific EffectDiffraction: Diffraction

Data Source

PatentUS12320763B2Full beam metrology for x-ray scatterometry systems
Publication Date: 2025.06.03 KLA CORP
  • US12320763B2 patent drawing
  • US12320763B2 patent drawing
  • US12320763B2 patent drawing

AI summary

Methods and systems for characterizing dimensions and material properties of semiconductor devices by full beam x-ray scatterometry are described herein. A full beam x-ray scatterometry measurement involves illuminating a sample with an X-ray beam and detecting the intensities of the resulting zero diffraction order and higher diffraction orders simultaneously for one or more angles of incidence relative to the sample. The simultaneous measurement of the direct beam and the scattered orders enables high throughput measurements with improved accuracy. The full beam x-ray scatterometry system includes one or more photon counting detectors with high dynamic range and thick, highly absorptive crystal substrates that absorb the direct beam with minimal parasitic backscattering. In other aspects, model based measurements are performed based on the zero diffraction order beam, and measurement performance of the full beam x-ray scatterometry system is estimated and controlled based on properties of the measured zero order beam.