Fullerene Electron Blocking Layer for Thermal Stability in Organic Photoelectric Devices

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Solution Overview

Problem

Conventional organic photoelectric conversion devices suffer from reduced sensitivity and increased dark current when exposed to heat, lacking sufficient heat resistance and high-speed response properties.

Innovation Solution

Incorporating a pair of electrodes with a photoelectric conversion layer sandwiched between them, and at least one electron blocking layer containing fullerene or fullerene derivatives, specifically with a mixed layer configuration that includes a first electron blocking layer with 0-10% fullerene volume ratio and a second layer with an electron donating organic material, enhancing thermal stability and charge transportability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If fullerene is used in the electric charge blocking layer to improve electron transport, then electron transport efficiency is improved, but heat resistance deteriorates when exposed to temperatures of 200°C or more

Engineering Contradiction:
Improveelectron transport efficiencyVSAvoidheat resistance
Core Design Contradiction:
ReliabilityVSTemperature

Solution Approach 1:

The patent uses composite materials by combining fullerene (C60) with electron-donating organic materials (such as TPD, TCTA, or mCP) in the electron blocking layer. This composite structure allows the layer to maintain electron transport capabilities while gaining thermal stability from the organic materials that can withstand temperatures of 200°C or more.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent changes the compositional parameters of the electron blocking layer by controlling the mixing ratio of fullerene and electron-donating organic materials. By optimizing these parameters, the layer achieves both sufficient electron transport performance and adequate heat resistance for manufacturing processes.

Inventive Principle:
Principle #35Parameter changes

2Reliability

If mixed layers of electron acceptor and electron donor are used throughout the photoelectric conversion layer to increase photoelectric conversion efficiency, then photoelectric conversion efficiency is improved, but heat resistance deteriorates

Engineering Contradiction:
Improvephotoelectric conversion efficiencyVSAvoidheat resistance
Core Design Contradiction:
ReliabilityVSTemperature

Solution Approach 1:

The patent applies local quality by differentiating the composition of different layers. The photoelectric conversion layer uses mixed layers of electron acceptor and donor for high efficiency, while the electron blocking layer uses a specific composite of fullerene and electron-donating materials for heat resistance. Each layer has optimized local composition suitable for its function.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent segments the device into functionally distinct layers with different material compositions. The photoelectric conversion layer is separated from the electron blocking layer, allowing each to be optimized independently - one for efficiency and one for heat resistance.

Inventive Principle:
Principle #1Segmentation

3Reliability

If conventional organic photoelectric conversion films are used to achieve high photoelectric conversion efficiency and low dark current, then sensitivity is improved, but heat resistance deteriorates when exposed to manufacturing process temperatures

Engineering Contradiction:
ImprovesensitivityVSAvoidheat resistance
Core Design Contradiction:
ReliabilityVSTemperature

Solution Approach 1:

The patent introduces electron-donating organic materials as intermediary substances in the electron blocking layer. These materials act as mediators that protect the sensitive photoelectric conversion layer from thermal degradation during manufacturing while allowing the device to maintain its sensitivity and photoelectric conversion efficiency.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration achieves high sensitivity, low dark current, and rapid response properties while maintaining heat resistance, suitable for applications requiring high photoelectric conversion efficiency and stability.

Implementation Method 1

fullerene is used for transporting electrons using a characteristic of an n-type organic semiconductor

Methodology Applied
Scientific EffectElectron transport: Conduction (electrical)

Implementation Method 2

a photoelectric conversion layer generating an electric charge by absorbing light

Methodology Applied
Scientific EffectPhotoelectric conversion: Photoelectric Effect

Data Source

PatentEP2448031B1Photoelectric conversion device and solid-state imaging device
Publication Date: 2014.07.23 FUJIFILM CORP
  • EP2448031B1 patent drawingFigure 1A~1B
  • EP2448031B1 patent drawingFigure 2
  • EP2448031B1 patent drawing

AI summary

A photoelectric conversion device having: a pair of electrodes (11;15); a photoelectric conversion layer (12) sandwiched between the pair of electrodes; and at least one electron blocking layer (16Ab) provided between one electrode of the pair of electrodes and the photoelectric conversion layer, wherein the photoelectric conversion layer contains at least one organic material, and the at least one electron blocking layer has a mixed layer (16Aa) containing fullerene or fullerene derivatives.