Functional Oil Powder via Cyclodextrin and Microfluidic Emulsification

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Solution Overview

Problem

Existing methods for manufacturing edible oil powders involve high-temperature processes that degrade active substances and require food additives like magnesium stearate and silicon dioxide, leading to stability and encapsulation issues and negative customer perception.

Innovation Solution

A method using cyclodextrin and a microfluidic device to emulsify and lyophilize functional oils, forming a coating layer and achieving homogeneous solutions for stable oil powders without the need for additional dispersing agents.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If high-temperature heat treatment is performed in emulsifying and spray drying steps, then the emulsification and drying processes can be completed, but the active substances in the edible oil are destroyed and rancidity and oxidation are accelerated

Engineering Contradiction:
Improveemulsification and drying process completionVSAvoiddestruction of active substances and accelerated rancidity
Core Design Contradiction:
Ease of manufactureVSObject-affected harmful factors

Solution Approach 1:

The invention changes the temperature parameter from high-temperature heat treatment to low-temperature or ambient temperature processing. The spray drying process is replaced with a freeze-drying or low-temperature drying method, maintaining the drying function while eliminating the harmful thermal effects that destroy active substances and accelerate oxidation.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention utilizes phase transition of water from liquid to solid (freezing) and then sublimation from solid to gas (freeze-drying), replacing the traditional liquid-to-gas evaporation process. This phase transition approach enables drying without high-temperature exposure, preserving the integrity of active substances in the edible oil.

Inventive Principle:
Principle #36Phase transitions

2Reliability

If food additives such as dispersing agents are added to extend shelf life, then the encapsulation and stability properties are improved, but the number of additives increases leading to negative customer perception

Engineering Contradiction:
Improveencapsulation and stability propertiesVSAvoidnumber of food additives
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The invention extracts and removes the need for food additives such as dispersing agents from the formulation. By optimizing the emulsification process and using appropriate drying methods, the invention achieves stable oil powder without relying on additional additive substances, thereby reducing the quantity of substances added to the final product.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention enables the edible oil and emulsifier system to self-stabilize without external additives. The proper selection of emulsifier and control of processing parameters allow the system to maintain encapsulation and stability properties inherently, making additional dispersing agents unnecessary.

Inventive Principle:
Principle #25Self-service

3Duration of action of stationary object

If edible oils are processed into powders to extend shelf life and improve edibility, then the storage stability and direct consumption feasibility are improved, but the active substances are degraded due to heat treatment

Engineering Contradiction:
Improveshelf life extensionVSAvoiddegradation of active substances
Core Design Contradiction:
Duration of action of stationary objectVSObject-affected harmful factors

Solution Approach 1:

The invention changes the drying temperature parameter from high-temperature spray drying to low-temperature freeze-drying or similar low-temperature drying methods. This parameter change enables the powder form to be achieved while preserving active substances that would otherwise be degraded by thermal exposure.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention employs freeze-drying phase transitions (liquid→solid→gas) instead of thermal evaporation (liquid→gas). This allows water removal and powder formation to occur without high-temperature exposure, extending shelf life while protecting temperature-sensitive active substances from degradation.

Inventive Principle:
Principle #36Phase transitions

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method produces functional oil powders with excellent encapsulation and stability, extending shelf life and allowing direct consumption, while avoiding the use of additives that affect customer perception.

Implementation Method 1

cyclodextrin forms a coating layer on the surface of the functional oil contained in the emulsified solution

Methodology Applied
Scientific EffectMolecular encapsulation: Absorption (physical)

Implementation Method 2

secondary emulsification is performed with a microfluidic device by passing the modified emulsified solution through the microfluidic device

Methodology Applied
Scientific EffectMicrofluidic emulsification: Hydrodynamic Cavitation

Implementation Method 3

the homogeneous solution is lyophilized to obtain the functional oil powder

Methodology Applied
Scientific EffectFreeze-drying: Freeze Drying

Data Source

PatentUS20250204571A1Method of manufacturing a functional oil powder
Publication Date: 2025.06.26 METAL INDS RES & DEV CENT
  • US20250204571A1 patent drawing

AI summary

The present invention is related to a method of manufacturing a functional oil powder. By using cyclodextrin and a microfluidic device, not only can the required temperature and time of an emulsification step decrease, but the obtained functional oil powder also can have excellent properties of encapsulation and stability. After a storage period, the functional oil powder hardly becomes wet. Moreover, there is no grease discharge and the microorganisms can hardly grow therein. Therefore, the present invention can be applied to make the product of the functional oil.