Furnace Access Port for Precise Moisture Sample Loading

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Solution Overview

Problem

Prior thermogravimetric analyzers expose samples to ambient environmental conditions during loading, leading to inaccurate moisture content determination due to changes in sample weight, especially for agricultural products.

Innovation Solution

An access port in the furnace cover allows for precise introduction of sample material into crucibles within a controlled environment, enabling the operator to add or remove material until the desired weight is reached, while maintaining the furnace in a closed and controlled atmosphere.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If the furnace cover is opened to allow sample loading, then the operator can easily load samples into crucibles, but the samples are exposed to ambient environmental conditions causing moisture content changes and inaccurate analytical results

Engineering Contradiction:
Improveease of sample loadingVSAvoidaccuracy of moisture content determination
Core Design Contradiction:
Ease of operationVSMeasurement precision

Solution Approach 1:

The furnace cover is segmented into a main cover body and a separate access port closure. The access port is a localized opening that can be opened and closed independently of the entire cover, allowing sample loading without exposing the entire furnace interior to ambient conditions. This segmentation enables selective access while maintaining the controlled environment for samples.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The access port acts as an intermediary mechanism between the operator and the crucibles. It provides a controlled interface for introducing samples while maintaining the sealed environment of the furnace. The access port closure serves as a mediator that isolates the sample chamber from ambient conditions during the loading process.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Measurement precision

If the furnace cover is kept closed to maintain controlled environment, then sample moisture content remains stable, but the operator cannot load or adjust samples in the crucibles

Engineering Contradiction:
Improveaccuracy of moisture content determinationVSAvoidability to load and adjust samples
Core Design Contradiction:
Measurement precisionVSEase of operation

Solution Approach 1:

The access port provides a localized opening in the otherwise sealed cover, enabling selective access to crucibles without compromising the overall sealed environment. This segmentation allows the cover to remain closed for maintaining controlled conditions while providing a specific access point for sample loading and adjustment.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The access port closure can be dynamically opened and closed as needed during the loading process. This dynamic capability allows the operator to access crucibles for sample loading or weight adjustment while minimizing the time the furnace environment is exposed to ambient conditions, thus maintaining measurement precision.

Inventive Principle:
Principle #15Dynamics

3Productivity

If samples are loaded in an open environment, then the loading process is quick and simple, but the sample weight changes due to moisture absorption or loss leading to inaccurate results

Engineering Contradiction:
Improvespeed of sample loadingVSAvoidaccuracy of sample weight measurement
Core Design Contradiction:
ProductivityVSMeasurement precision

Solution Approach 1:

The access port provides a focused, localized opening that enables rapid sample loading while maintaining the sealed furnace environment. This segmentation allows the loading process to be quick and simple like open loading, but without the harmful exposure to ambient conditions that cause weight changes.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The furnace maintains a controlled, inert atmosphere that prevents moisture exchange between samples and ambient air. The access port closure ensures this inert environment is maintained during sample loading, allowing fast loading without the weight changes that occur in open environmental loading.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

Data Source

PatentUS11899033B2Access port for a thermogravimetric analyzer furnace
Publication Date: 2024.02.13 LECO CORP
  • US11899033B2 patent drawing
  • US11899033B2 patent drawing
  • US11899033B2 patent drawing

AI summary

The analyzer of the present invention is specifically adapted to provide moisture determinations for foods and other agricultural material. It allows the operator to introduce a precise weight of sample into a crucible in a closed furnace in a controlled environment through an access port in the furnace cover. The access port in the cover can be tapered to allow easy access to an underlying aligned crucible and allow an operator to add and remove sample material from the crucible until a precise desired sample weight is reached as measured by a balance within the furnace. The access port is enclosed by an insulated cover after the samples are sequentially placed in the crucibles.