Atomic Absorption Furnace Camera Image Storage

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Solution Overview

Problem

In atomic absorption spectrophotometers using a tube-like furnace, determining the optimal analysis conditions for unknown samples is challenging, leading to potential sample bumping or injection failures, which are difficult to diagnose and require labor-intensive re-investigation.

Innovation Solution

Incorporating a camera to capture images of the furnace before measurement, with associated image data storage and a data organization unit to delete unnecessary image data after normal measurement verification, allowing for ex-post verification of sample injection and temperature rise processes.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If all captured image data is stored for every measurement, then complete verification capability is achieved, but storage space is wasted on normal measurements

Engineering Contradiction:
Improveverification capabilityVSAvoidstorage space
Core Design Contradiction:
ReliabilityVSVolume of stationary object

Solution Approach 1:

The system changes the storage parameter dynamically based on measurement quality. Normal measurements (with adequate signal strength above threshold) have their image data deleted to save space, while abnormal measurements (with signal strength below threshold) retain their image data for verification. This parameter-based differentiation resolves the contradiction between complete verification capability and storage space efficiency.

Inventive Principle:
Principle #35Parameter changes

2Loss of information

If a camera is added to capture furnace images, then measurement verification is enabled, but device complexity increases

Engineering Contradiction:
Improvemeasurement process verificationVSAvoidsystem structure
Core Design Contradiction:
Loss of informationVSDevice complexity

Solution Approach 1:

The camera acts as an intermediary device that captures visual information of the measurement process without interfering with the core atomic absorption measurement. The image data serves as supplementary verification information, allowing users to confirm proper sample injection and furnace conditions without adding complex control mechanisms to the measurement system itself.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

Instead of modifying the measurement process or adding complex sensors inside the furnace, the system uses a camera to create a visual copy/image of the furnace interior and sample injection process. This optical copy provides verification capability with minimal intrusion into the measurement system, reducing overall complexity compared to direct sensing approaches.

Inventive Principle:
Principle #26Copying

3Volume of stationary object

If image data is automatically deleted for normal measurements, then storage space is secured, but verification of normal measurements becomes impossible

Engineering Contradiction:
Improvestorage space managementVSAvoidmeasurement verification
Core Design Contradiction:
Volume of stationary objectVSReliability

Solution Approach 1:

The system uses signal strength as feedback to determine whether to retain or delete image data. By continuously monitoring the signal strength during measurement and comparing it against a predetermined threshold, the system automatically makes informed decisions about data retention. This feedback mechanism ensures that only measurements meeting quality criteria have their images deleted, maintaining verification capability for problematic cases while managing storage efficiently.

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables efficient verification of sample injection and furnace state, reducing unnecessary data storage and labor, while securing storage space for other data by automatically determining normal measurement data based on signal strength thresholds.

Implementation Method 1

an atomization unit (4) provided with a tube-like furnace (6) and configured to atomize a sample injected into the furnace (6) by heating the sample

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 2

the furnace (6) is heated according to a predetermined temperature program to atomize the sample

Methodology Applied
Scientific EffectAtomization: Evaporation

Implementation Method 3

measurement light from a light source composed of a hollow cathode lamp is irradiated in the furnace

Methodology Applied
Scientific EffectLight emission from hollow cathode lamp: Luminescence

Implementation Method 4

the transmitted light is detected by a detector

Methodology Applied
Scientific EffectLight detection: Photoelectric Effect

Implementation Method 5

an optical system configured to guide the light of the wavelength of the measurement target among the light from the furnace to the detector

Methodology Applied
Scientific EffectOptical guidance: Refraction

Data Source

PatentUS10552965B1Atomic absorption spectrophotometer
Publication Date: 2020.02.04 SHIMADZU CORP
  • US10552965B1 patent drawing
  • US10552965B1 patent drawing
  • US10552965B1 patent drawing

AI summary

The atomic absorption spectrophotometer is provided with an atomization unit, a light source, a detector, an optical system, a camera, and a captured image data storage unit. The atomization unit has a tube-like furnace and atomizes the sample injected into the furnace by heating the sample. The light source emits light of a wavelength of a measurement target toward the atomization unit so that the light passes through the furnace. The detector detects the light passed through the furnace. The camera captures an image of an inside of the furnace before performing a measurement process in which a sample is atomized in the furnace and its absorbance is measured. The captured image data storage unit stores the captured image data obtained by capturing the image by the camera in association with the measurement data corresponding to the captured image data.