FWA Formulation Brightness and Yellowing in Papermaking

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Solution Overview

Problem

Conventional optical brightening agents (OBA) face limitations in brightness gain and yellowing due to overdosing, especially in paper products with significant mechanical pulp content, and existing fluorescent whitening agents (FWA) suffer from low solubility and retention issues in papermaking processes.

Innovation Solution

The combination of FWA formulation FB #351 and FB #71, which have different molecular structures and improved solubility, is used in the wet-end papermaking process to achieve higher brightness and retention rates without yellowing, utilizing their unique light re-emission properties and interactions with paper fibers.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Illumination intensity

If conventional FWA is overdosed to increase brightness, then brightness gain is improved, but yellowing occurs due to the natural appearance of conventional FWA

Engineering Contradiction:
ImprovebrightnessVSAvoidyellowing
Core Design Contradiction:
Illumination intensityVSObject-generated harmful factors

Solution Approach 1:

The patent changes the molecular structure parameters of the FWA from conventional types to new generation FB #351 and FB 71, which have different emission characteristics. This structural parameter change allows achieving higher brightness without the yellowing effect that plagues conventional FWA overdosing

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite FWA formulation combining FB #351 and FB 71 in specific ratios (30:70 to 70:30). This composite approach leverages the complementary properties of both dyes to achieve superior brightness enhancement without yellowing, overcoming the limitations of single-component conventional FWAs

Inventive Principle:
Principle #40Composite materials

2Illumination intensity

If FWA formulation is used to achieve high brightness, then brightness gain is improved, but solubility and retention issues occur in papermaking processes

Engineering Contradiction:
ImprovebrightnessVSAvoidsolubility and retention
Core Design Contradiction:
Illumination intensityVSReliability

Solution Approach 1:

The patent modifies the chemical parameters of the FWA by selecting FB #351 and FB 71 which possess superior solubility characteristics compared to conventional FWAs. This parameter change ensures reliable dissolution and retention in the papermaking process while maintaining high brightness performance

Inventive Principle:
Principle #35Parameter changes

3Illumination intensity

If FWA is used in mechanical pulp papermaking, then brightness is improved, but brightness reversion occurs due to limitations in brightness gain

Engineering Contradiction:
ImprovebrightnessVSAvoidbrightness reversion
Core Design Contradiction:
Illumination intensityVSStability of the object's composition

Solution Approach 1:

The patent changes the FWA molecular structure to FB #351 and FB 71 which exhibit superior stability characteristics. These new generation dyes maintain their brightness-enhancing properties over time in mechanical pulp papermaking applications, preventing the brightness reversion that occurs with conventional FWAs

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach allows for increased brightness and retention rates at lower costs, overcoming the limitations of conventional OBAs and FWAs by maintaining high ISO brightness values and preventing brightness reversion, thus expanding market applications and reducing costs.

Implementation Method 1

Optical brightening agents (OBA's) or fluorescent whitening agent (FWA's) have chemical properties that absorb light in the ultraviolet region (340-370 nm) and then re-emitting it back into the visible spectrum

Methodology Applied
Scientific EffectFluorescence: Fluorescence

Data Source

PatentUS9181656B2FWA formulation used for the papermaking process
Publication Date: 2015.11.10 LI MENG JUN

AI summary

A new fluorescent whitening agent (FWA) formulation containing 0.1%-99.9% fluorescent brightener #351 (FB #351) 4,4″-bis(2-sulfostyryl)biphenyl disodium salt (CAS #27344-41-8) and 0.1%-99.9% fluorescent brightener #71 (FB #71) 4,4′-bis[4-anilino-6-morpholino-1,3,5-triazin-2-yl]amino-2,2′-stilbene disodium salt (CAS #16090-02-1) is used on the wet-end papermaking process and coating papermaking process to increase the brightness of paper.