Replicated Mirror Curing With Gamma Radiation for Low Residual Stress

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Elevated temperature curing techniques for mirror replication result in residual stress and surface figure errors due to thermal expansion variations, while low temperature UV curing limits the achievable cure state, leading to inadequate mechanical properties and dimensional stability.

Innovation Solution

A low temperature curing process using Gamma radiation in conjunction with UV radiation to achieve a high cure state with low residual stress, optimizing the dosage based on the material substrate composition, and potentially incorporating nano-particles to enhance cross-linking and reduce chain scission.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If elevated temperature curing techniques are used to achieve high cure state, then the material substrate reaches high cure state with increased density and mechanical properties, but residual stress and surface figure errors occur due to thermal expansion variations

Engineering Contradiction:
Improvecure stateVSAvoidsurface figure error
Core Design Contradiction:
StrengthVSManufacturing precision

Solution Approach 1:

The patent changes the curing parameter from thermal energy to gamma radiation energy. This fundamental parameter change allows achieving high cure state without the thermal expansion issues that cause surface figure errors and residual stress in conventional thermal curing processes.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces the thermal curing mechanism with a radiation-based curing mechanism. Gamma radiation penetrates the material substrate and initiates cross-linking reactions directly, substituting the thermal field with a radiation field to eliminate temperature-related defects.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Manufacturing precision

If low temperature UV curing techniques are used to avoid thermal stress, then surface figure error is reduced, but the achievable cure state is limited due to low energy and low penetration depth of UV rays

Engineering Contradiction:
Improvesurface figure errorVSAvoidcure state
Core Design Contradiction:
Manufacturing precisionVSStrength

Solution Approach 1:

The patent changes the radiation parameter from UV to gamma radiation. Gamma rays have significantly higher energy and penetration depth compared to UV rays, enabling them to cure thick material substrates thoroughly while maintaining low temperature conditions that prevent thermal stress and surface figure errors.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent substitutes UV radiation with gamma radiation for the curing process. This substitution provides sufficient energy penetration through the material substrate to achieve high cure state while maintaining the advantage of low temperature curing that prevents thermal expansion issues.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Stability of the object's composition

If gamma radiation is used to achieve high cure state with low residual stress, then dimensional stability and mechanical properties are improved, but chain scission and fragmentation may occur in the polymer backbone

Engineering Contradiction:
Improvedimensional stabilityVSAvoidmechanical capability
Core Design Contradiction:
Stability of the object's compositionVSStrength

Solution Approach 1:

The patent optimizes the gamma radiation dosage parameter to achieve the desired cure state while minimizing chain scission. By carefully controlling the radiation dose and using appropriate resin formulations with cross-linking dominance, the process achieves high dimensional stability without significant mechanical degradation.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables high dimensional stability, increased glass transition temperature, higher modulus, and reduced moisture absorption, overcoming the limitations of existing curing methods by achieving a high cure state without warping or significant degradation.

Implementation Method 1

expose the portion of the material substrate layer to Gamma radiation such that a relatively high cure state and a low residual stress are achieved

Methodology Applied
Scientific EffectGamma radiation: Radiation

Implementation Method 2

Resin formulations in which cross-linking dominates over chain scission result in net increase in cure state while reducing residual stress

Methodology Applied
Scientific EffectCross-linking: Chemical Bonding

Implementation Method 3

a dosage level of the Gamma radiation is based, at least in part, on at least one composition of the material substrate layer

Methodology Applied
Scientific EffectRadiation absorption: Absorption (EM radiation)

Data Source

PatentUS11762301B2Systems and methods for gamma radiation based stabilization of replicated mirror structures at the nanometer-scale
Publication Date: 2023.09.19 AEROSPACE CORP
  • US11762301B2 patent drawing
  • US11762301B2 patent drawing
  • US11762301B2 patent drawing

AI summary

An assembly comprises an exposure chamber configured to receive a structure and identify at least one portion of the structure for further processing. The exposure chamber is further configured to expose the at least one portion of the structure to radiation such that a high cure state and a low residual stress are achieved for the structure. A dosage level of the radiation is determined based, at least in part, on the composition of the structure.