Process Gas Analyzer Oxygen Interference Compensation

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Solution Overview

Problem

Existing process gas analyzers face challenges in accurately measuring oxygen content in process gas mixtures due to the influence of atmospheric oxygen within the measuring heads, which requires costly oxygen-free gas flushing or additional optical components to compensate for interference.

Innovation Solution

Incorporating a temperature sensor in each measuring head to record and store ambient reference spectra at different temperatures, allowing the evaluation device to subtract the oxygen absorption from the detected absorption spectrum, thereby calculating the oxygen concentration without the need for oxygen-free gas flushing or additional optical components.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If oxygen-free gas flushing is used to prevent atmospheric oxygen interference, then measurement accuracy is improved, but operational costs increase due to consumption of expensive flushing gas

Engineering Contradiction:
Improvemeasurement accuracyVSAvoidconsumption of flushing gas
Core Design Contradiction:
Measurement precisionVSLoss of substance

Solution Approach 1:

The patent extracts and removes the atmospheric oxygen absorption component from the measured spectrum through mathematical subtraction. By recording reference spectra without process gas and subtracting them from measurement spectra, the harmful atmospheric oxygen interference is separated and eliminated, allowing accurate measurement without oxygen-free flushing gas.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent creates a copy of the atmospheric oxygen absorption spectrum through reference measurements and uses this copied spectral information to compensate for and remove the interference in actual measurements. The reference spectra serve as a template that is subtracted from measurement spectra to eliminate the atmospheric oxygen component.

Inventive Principle:
Principle #26Copying

2Measurement precision

If additional optical components are added to compensate for atmospheric oxygen interference, then measurement accuracy is improved, but device complexity increases

Engineering Contradiction:
Improvemeasurement accuracyVSAvoiddevice complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent replaces physical/optical compensation methods with a mathematical/software-based solution. Instead of adding optical components like reference cells or beam splitters, the system uses computational subtraction of reference spectra to remove atmospheric oxygen interference, thereby maintaining measurement accuracy while avoiding increased device complexity.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Measurement precision

If measuring heads are sealed to prevent ambient air ingress, then measurement accuracy is improved, but device complexity and cost increase due to additional sealing and flushing systems

Engineering Contradiction:
Improvemeasurement accuracyVSAvoiddevice complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent enables the measurement system to compensate for atmospheric oxygen interference using its own measurement capabilities. By recording reference spectra and performing mathematical subtraction, the system serves itself to remove the interference without requiring external sealing systems or additional flushing infrastructure.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method effectively compensates for the influence of atmospheric oxygen, improving measurement accuracy and reducing operational costs by eliminating the need for oxygen-free gas flushing and additional optical components, while accounting for temperature variations in the measuring heads.

Implementation Method 1

In laser absorption spectroscopy, a measurement gas mixture is irradiated with light from a wavelength-tunable laser diode and the concentration of a gas component of interest in the measurement gas mixture is determined based on the reduction in light intensity caused by the absorption of the light at the point of a selected absorption line of the gas component

Methodology Applied
Scientific EffectAbsorption spectroscopy: Absorption Spectroscopy

Implementation Method 2

a temperature sensor is arranged in at least one of the two measuring heads, which is designed to record the current temperature when measuring the absorption spectrum

Methodology Applied
Scientific EffectTemperature sensing:

Data Source

PatentEP3364169B1Process gas analyser
Publication Date: 2019.05.15 SIEMENS AG
  • EP3364169B1 patent drawingFigure 1~2
  • EP3364169B1 patent drawingFigure 3~4
  • EP3364169B1 patent drawing

AI summary

A process gas analyzer contains a wavelength-tunable laser diode (7) and a detector (8) in two separate measuring heads (5, 6), which are mounted on diametrically opposite sides of a system component (1) containing a process gas (2). To compensate for the influence of atmospheric oxygen in the measuring heads (5, 6) on the measurement of the oxygen content in the process gas mixture (2), a temperature sensor (23, 24) is arranged in at least one of the two measuring heads (5, 6). Ambient reference spectra (27, 272f) of the ambient air contained in the two measuring heads (5, 6), recorded at different temperatures and without the process gas mixture (2), are stored in a memory (26) of an evaluation unit (19).The evaluation unit (19) is further configured to select one of the stored ambient reference spectra (272f) depending on the current temperature detected by the temperature sensor (23, 24) or to calculate it from two stored ambient reference spectra (272f) and to subtract it from the currently detected absorption spectrum (182f) of the process gas mixture (2) and to determine the oxygen concentration in the process gas mixture (2) from the difference spectrum (302f).