Gas Chromatography Detector Gas Flow Control

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Solution Overview

Problem

Conventional gas chromatography systems using hydrogen gas generated by water electrolysis inefficiently utilize hydrogen and oxygen gases, as they are introduced as a mixed gas with a constant ratio, limiting the support for various detectors.

Innovation Solution

The system individually controls the flow rates of hydrogen and oxygen gases generated by electrolysis, allowing them to be supplied to the detector as separate gases, enabling adjustment of their ratio to suit different detectors.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If hydrogen gas and oxygen gas are introduced as mixed gas with constant ratio, then the system structure is simple, but the adaptability to various detectors is limited

Engineering Contradiction:
Improvesupport for various detectorsVSAvoidgas flow control system
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The gas flow control system is segmented into separate control paths for hydrogen gas and oxygen gas. Each gas has its own flow rate controller, allowing independent adjustment of flow rates to achieve different gas ratios suitable for various detector types.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The gas flow control system is made dynamic by allowing real-time adjustment of hydrogen and oxygen flow rates. This enables the system to adapt to different detector requirements by changing the gas ratio on demand, rather than being fixed at a constant ratio.

Inventive Principle:
Principle #15Dynamics

2Productivity

If mixed gas with constant ratio is used, then the operation is simple, but the utilization efficiency of hydrogen and oxygen gases is low

Engineering Contradiction:
Improveutilization efficiency of hydrogen and oxygen gasesVSAvoidgas flow control operation
Core Design Contradiction:
ProductivityVSEase of operation

Solution Approach 1:

The flow rate parameters of hydrogen gas and oxygen gas are made independently adjustable. This allows optimization of gas utilization efficiency by setting appropriate flow rates for each gas based on detector requirements, while the control interface maintains ease of operation through automated or semi-automated control.

Inventive Principle:
Principle #35Parameter changes

3Adaptability or versatility

If constant ratio of hydrogen to oxygen is introduced into detector, then the system is stable, but various detectors cannot be supported

Engineering Contradiction:
Improvedetector compatibilityVSAvoidgas ratio stability
Core Design Contradiction:
Adaptability or versatilityVSStability of the object's composition

Solution Approach 1:

The gas ratio is made dynamically adjustable while maintaining stability during operation. The system can switch between different stable gas ratios depending on which detector is being used, and once set, maintains stable flow rates to ensure reliable detector operation.

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach allows for efficient utilization of hydrogen and oxygen gases, supporting various detectors by controlling their ratio, thereby enhancing the flexibility and effectiveness of gas chromatography analysis.

Implementation Method 1

a gas generator configured to generate hydrogen gas and oxygen gas by electrolysis of water and to individually take out generated hydrogen gas and oxygen gas

Methodology Applied
Scientific EffectElectrolysis: Electrolysis

Data Source

PatentUS11860136B2Gas chromatography analysis method and gas chromatography analysis system
Publication Date: 2024.01.02 SHIMADZU CORP
  • US11860136B2 patent drawing
  • US11860136B2 patent drawing
  • US11860136B2 patent drawing

AI summary

A gas chromatography analysis method includes separating a component in sample gas by introducing the sample gas into a separation column (4) using carrier gas, and detecting a component in sample gas that has passed through the separation column (4) by introducing the sample gas into a detector (6). The detecting includes individually taking out hydrogen gas and oxygen gas generated by electrolysis of water, and controlling flow rates of taken-out hydrogen gas and oxygen gas and supplying the taken-out hydrogen gas and oxygen gas to the detector as detector gas.