Gas-Liquid Separator Feedback Control for Stable Phase Balance

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Solution Overview

Problem

Conventional gas liquid separators are prone to unbalanced states due to fixed restrictions, leading to inadequate separation and loss of samples under varying system flow conditions, as they fail to maintain the integrity of the solvent and gas phases.

Innovation Solution

Incorporating sensors to monitor solvent and gas levels within the chamber, coupled with a pressure regulator or on/off valve to adjust pressures and flows, ensuring balanced separation by regulating the solvent and gas levels dynamically.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If fixed restrictions are used in conventional gas liquid separators, then the device structure is simple, but the separation becomes unbalanced under varying system flow conditions leading to sample loss

Engineering Contradiction:
Improveseparation balance under varying flow conditionsVSAvoiddevice structure
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The patent applies dynamics by replacing fixed restrictions with adjustable flow control valves that can dynamically adapt to varying system flow conditions. The controller receives feedback from level sensors and adjusts the valve positions in real-time to maintain balanced separation between gas and solvent phases, transforming a static system into a dynamic one that responds to changing conditions.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent implements feedback control by using level sensors to continuously monitor the positions of the solvent-gas interface and gas-liquid interface in the separation chamber. The controller processes this feedback information and adjusts the flow control valves to maintain optimal separation balance, ensuring that the separator adapts to varying inlet flow conditions while preventing sample loss.

Inventive Principle:
Principle #23Feedback

2Reliability

If manual adjustment is used in conventional gas liquid separators, then the device complexity is low, but the response to varying flow conditions is slow and inadequate

Engineering Contradiction:
Improveseparation integrityVSAvoidflow regulation automation
Core Design Contradiction:
ReliabilityVSExtent of automation

Solution Approach 1:

The patent implements feedback control by using level sensors to continuously monitor the positions of the solvent-gas interface and gas-liquid interface in the separation chamber. The controller processes this feedback information and adjusts the flow control valves to maintain optimal separation balance, ensuring that the separator adapts to varying inlet flow conditions while preventing sample loss.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The system performs self-service by automatically monitoring its own operational state through level sensors and making self-adjustments via the controller and flow control valves. This eliminates the need for manual intervention while maintaining reliable separation integrity under varying flow conditions, with the system regulating its own flow distribution based on real-time feedback.

Inventive Principle:
Principle #25Self-service

3Measurement precision

If no level monitoring is implemented, then the device complexity is minimal, but the separation balance cannot be maintained under varying conditions

Engineering Contradiction:
Improvesolvent and gas level detectionVSAvoidsensor and control system
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent implements feedback control by using level sensors to continuously monitor the positions of the solvent-gas interface and gas-liquid interface in the separation chamber. The controller processes this feedback information and adjusts the flow control valves to maintain optimal separation balance, ensuring that the separator adapts to varying inlet flow conditions while preventing sample loss.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The patent replaces mechanical level indication methods with electronic level sensors that provide precise measurement of solvent and gas levels. This substitution enables accurate detection and automated control, transforming the system from a purely mechanical operation to one that incorporates electronic sensing and control for enhanced measurement precision.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This solution maintains balanced separation of fluid mixtures during changing flow conditions, preventing sample loss and ensuring accurate collection, thereby enhancing the efficiency and reliability of chromatographic processes.

Implementation Method 1

a sensor for sensing at least one of a solvent level or a gas level within a chamber

Methodology Applied
Scientific EffectLevel sensing:

Implementation Method 2

a pressure regulator for regulating a pressure within the chamber

Methodology Applied
Scientific EffectPressure regulation:

Implementation Method 3

separating the fluid mixture into a solvent and a gas

Methodology Applied
Scientific EffectGas-liquid separation:

Data Source

PatentEP3532835B1Gas liquid separator and associated methods
Publication Date: 2023.11.29 WATERS TECHNOLOGY CORP
  • EP3532835B1 patent drawingFigure 1
  • EP3532835B1 patent drawingFigure 2
  • EP3532835B1 patent drawingFigure 3

AI summary

Exemplary embodiments are directed to a gas liquid separator that includes a chamber for receiving a fluid mixture, a fluid mixture inlet, a solvent outlet, and a gas outlet. The gas liquid separator can include a sensor disposed around or within the chamber for sensing at least one of a solvent level or a gas level. The gas liquid separator can include a regulator connected to at least one of the solvent outlet or the gas outlet for regulating at least one of the solvent level or the gas level within the chamber. Exemplary methods of regulating at least one of the solvent level or the gas level within a gas liquid separator of a CO2-based chromatography flow system are also provided.