Gas Sample Introduction Device Flow Path Switching Mechanism

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Solution Overview

Problem

Conventional gas sample introduction devices face issues with sample gas spreading to unintended pipes during switching between measurement and concentration modes, leading to reduced analytical sensitivity and precision.

Innovation Solution

A gas sample introduction device with flow path switching mechanisms that connect the measuring tube and collecting tube in series during concentration mode and short-circuit the collecting tube during measurement mode, preventing sample gas from spreading to unused pipes, and utilizing thermal desorption for concentration.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If the gas sample introduction device uses a conventional flow path switching system with parallel measuring tube and collecting tube, then it can perform both measurement mode and concentration mode, but sample gas spreads to unintended pipes during mode switching, reducing analytical sensitivity and precision

Engineering Contradiction:
Improvedual mode operation capabilityVSAvoidanalytical sensitivity and precision
Core Design Contradiction:
Adaptability or versatilityVSMeasurement precision

Solution Approach 1:

The flow path switching system is segmented into two independent switching mechanisms: a first switching mechanism that alternates between measurement mode (connecting measuring tube to exhaust) and concentration mode (connecting measuring tube to column), and a second switching mechanism that controls the collecting tube connection state. This segmentation allows precise control of gas flow paths, preventing sample gas from spreading to unintended pipes while maintaining dual mode operation capability.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The flow path configuration is made dynamic through coordinated switching of two switching mechanisms. The first switching mechanism dynamically changes the measuring tube connection between exhaust and column based on operation mode, while the second switching mechanism dynamically adjusts the collecting tube connection state. This dynamic control ensures that the collecting tube is short-circuited to exhaust during measurement mode (preventing sample gas accumulation) and connected in series during concentration mode (enabling sample concentration), thereby eliminating sample gas spreading issues.

Inventive Principle:
Principle #15Dynamics

2Device complexity

If the collecting tube is connected in parallel during measurement mode, then the device structure is simple, but sample gas may spread to the collecting tube pipe, reducing collection rate and analytical precision

Engineering Contradiction:
Improveflow path structure simplicityVSAvoidanalytical precision
Core Design Contradiction:
Device complexityVSMeasurement precision

Solution Approach 1:

The collecting tube connection is made dynamic through the second switching mechanism. During measurement mode, the second switching mechanism connects the collecting tube to exhaust (short-circuiting it), preventing sample gas from spreading into the collecting tube pipe. During concentration mode, the second switching mechanism connects the collecting tube in series between the measuring tube and the column, enabling proper sample concentration. This dynamic reconfiguration maintains analytical precision while preserving device structural simplicity.

Inventive Principle:
Principle #15Dynamics

3Ease of operation

If the measuring tube retains sample gas for later introduction, then it enables controlled sample introduction, but sample gas may spread to unused pipes during the retention period, reducing analytical reliability

Engineering Contradiction:
Improvecontrolled sample introductionVSAvoidanalytical reliability
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The flow path configuration is dynamically controlled to match the operational phase. During the sample introduction phase, the first switching mechanism connects the measuring tube to the column for controlled sample introduction. During the sample retention phase between measurements, the first switching mechanism connects the measuring tube to exhaust, and the second switching mechanism short-circuits the collecting tube to exhaust, preventing sample gas from spreading to unused pipes. This dynamic control maintains both ease of operation and analytical reliability.

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Prevents sample gas spreading, improving analytical sensitivity, precision, and reliability by ensuring accurate sample introduction and concentration, enhancing the reliability of gas analysis results.

Implementation Method 1

a collecting tube for absorbing a predetermined component in the sample gas and concentrating the sample gas by a thermal desorption method

Methodology Applied
Scientific EffectAbsorption: Absorption (physical)

Implementation Method 2

concentrating the sample gas by a thermal desorption method

Methodology Applied
Scientific EffectThermal desorption: Desorption

Data Source

PatentUS8584507B2Gas sample introduction device and a gas chromatograph using the same
Publication Date: 2013.11.19 SHIMADZU CORP
  • US8584507B2 patent drawing
  • US8584507B2 patent drawing
  • US8584507B2 patent drawing

AI summary

A gas sample introduction device for introducing sample gas to a gas analyzer includes a measuring tube, a sample gas supply flow path for introducing the sample gas to the measuring tube,a carrier gas supply flow path for introducing carrier gas to the measuring tube, an exhaust flow path for discharging the gas passing through the measuring tube to outside, and a collecting tube for absorbing a component in the sample gas. A first flow path switching device switches between a first state in which the measuring tube is inserted between the sample gas supply flow path and the exhaust flow path, and a second state in which the measuring tube is inserted between the carrier gas supply flow path and the gas analyzer. A second flow path switching device switches between a collecting-tube inserted state and a collecting-tube short-circuited state in which the collecting tube is not inserted.