Tar and Water Removal in Gas Sampling Lines

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Solution Overview

Problem

Current methods for online analysis of gas composition, particularly in syngas from biomass pyrolysis or gasification, face challenges in removing tars, water, and solid particles, which can condense and block filters or capture target compounds like HCl, leading to inefficient analysis and high costs due to the need for heating the sampling line above 400°C.

Innovation Solution

A device with a container and multiple filters, where a tar-absorbing material like cotton or nylon filters out tars without capturing target compounds, and a water adsorbent material like zeolite removes moisture without reacting with acidic gases, ensuring efficient tar and water removal while maintaining the target compounds in the gas stream.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If organic solvents like acetone or isopropanol are used to remove tars from syngas, then tar removal is achieved, but hydrogen chloride (HCl) is captured in the gas sampling line and accumulates in the bubbler headspace

Engineering Contradiction:
Improvetar removal efficiencyVSAvoidHCl loss
Core Design Contradiction:
Quantity of substanceVSLoss of substance

Solution Approach 1:

The patent extracts the tar removal function from the gas sampling line by introducing a separate cleaning device with a dedicated cleaning gas flow. This separates the tar removal process from the HCl sampling process, allowing tars to be removed without capturing HCl in the sampling line or bubbler headspace.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent introduces a cleaning gas as an intermediary substance that carries tars away from the sampling line without interfering with HCl sampling. The cleaning gas acts as a mediator between the tar-laden syngas and the HCl analysis system, removing tars while leaving HCl intact for analysis.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If the pipeline is heated to above 400°C to prevent tar condensation, then tar condensation is prevented, but the cost of material and heating increases significantly

Engineering Contradiction:
Improvetar condensation preventionVSAvoidheating cost
Core Design Contradiction:
ReliabilityVSUse of energy by stationary object

Solution Approach 1:

The patent applies preliminary action by introducing a cleaning gas flow that proactively removes tars before they can condense in the sampling line. This preventive cleaning approach eliminates the need for high-temperature heating to prevent condensation, reducing energy consumption and material costs.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent replaces the thermal field (high-temperature heating) with a fluid field (cleaning gas flow) to achieve tar removal. Instead of using heat to prevent condensation, the system uses a flowing cleaning gas to physically carry tars away, substituting a mechanical/fluid approach for a thermal approach.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Quantity of substance

If a solid filter like deactivated fused silica wool is used in the gas sampling probe, then solid particles are removed, but tar condensation on the filter blocks it

Engineering Contradiction:
Improvesolid particle removalVSAvoidfilter blockage
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent extracts the tar removal function from the solid filter by introducing a cleaning gas flow that removes tars upstream of the filter. This separates the tar removal function from the particle filtration function, preventing tar condensation on the filter while maintaining solid particle removal capability.

Inventive Principle:
Principle #2Taking out (Extraction)

4Productivity

If the gas flow rate in the sampling line is kept low, then the analysis system operates efficiently, but hydrogen chloride (HCl) accumulates in the bubbler headspace because it is denser than syngas

Engineering Contradiction:
Improveanalysis efficiencyVSAvoidHCl accumulation
Core Design Contradiction:
ProductivityVSQuantity of substance

Solution Approach 1:

The patent extracts HCl from the bubbler headspace by introducing a cleaning gas flow that actively removes accumulated HCl. This prevents HCl buildup while maintaining low sampling flow rates for efficient analysis, separating the HCl removal function from the sampling function.

Inventive Principle:
Principle #2Taking out (Extraction)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This solution allows for effective online monitoring of gas composition by preventing tar and water condensation, avoiding filter blockages and chemical reactions, and maintaining the target compounds in the gas stream, thus enhancing the accuracy and cost-effectiveness of gas analysis.

Implementation Method 1

a first filter positioned between the inlet and the outlet of the container, through which the gas flows, intended to filter the tar, and the first filter comprising a tar-absorbing material

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

a second filter positioned between the inlet and the outlet of the container, upstream or downstream of the first filter, through which the gas circulates and intended to remove water from the gas, and the second filter comprising a water adsorbent material

Methodology Applied
Scientific EffectAdsorption: Adsorption

Data Source

PatentEP3658255B1Device for cleaning a gas for on-line analysis
Publication Date: 2024.07.24 SUEZ INTERNATIONAL
  • EP3658255B1 patent drawingFigure 1~2
  • EP3658255B1 patent drawingFigure 3~4
  • EP3658255B1 patent drawingFigure 5~6

AI summary

The invention relates to a device (60) for cleaning a gas (12) comprising a plurality of compounds, a first compound from the plurality of compounds being tar, said device comprising: a container (13) with an inlet (14) and an outlet (15), the gas (12) circulating through the container (13) from the inlet (14) to the outlet (15); and a first filter (11) positioned between the inlet (14) and the outlet (15) of the container (13), through which the gas (12) circulates, for filtering the tar, said first filter (11) comprising an absorbent material. The cleaning device (60) can also comprise a second filter (17) positioned between the inlet (14) and the outlet (15) of the container (13), upstream or downstream of the first filter (11), through which the gas circulates (12), for removing the water from the gas (12), said second filter comprising a water-adsorbent material.