Gas Separation System Using Temperature-Controlled Adsorbent Collection

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Solution Overview

Problem

Existing gas separation systems face challenges in efficiently and stably fractionating target components due to the risk of system blockage and instability when liquefying components for collection.

Innovation Solution

A gas separation system incorporating a separation column, a sample gas supplier, a detector, a collection tube filled with adsorbent, a temperature adjuster, and a switching mechanism that adsorbs and desorbs the target component at specific temperatures to facilitate efficient and stable fractionation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If a target component is liquefied and collected in a container, then the target component can be collected, but the system may be blocked by the liquefied substance and the target component cannot be stably fractionated

Engineering Contradiction:
Improvetarget component collectionVSAvoidsystem stability
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The invention changes the temperature parameter of the collection tube, switching between a first temperature (for adsorption) and a second temperature higher than the first (for desorption). This temperature parameter change allows the adsorbent to alternately adsorb and desorb the target component, preventing system blockage while enabling stable fractionation and collection of the target component.

Inventive Principle:
Principle #35Parameter changes

2Manufacturing precision

If precision distillation apparatus is used to extract target component with high purity, then purification quality is improved, but the amount of purified gas is limited to 1 g or less

Engineering Contradiction:
Improvepurification qualityVSAvoidamount of purified gas
Core Design Contradiction:
Manufacturing precisionVSQuantity of substance

Solution Approach 1:

The invention uses an adsorbent material with porous structure in the collection tube. The adsorbent can adsorb large amounts of target component from the gas phase, enabling collection of quantities exceeding 1 g while maintaining high purification quality. The porous structure provides large surface area for adsorption, resolving the contradiction between purification quality and quantity.

Inventive Principle:
Principle #31Porous materials

3Quantity of substance

If gas is handled for purification, then target component can be extracted, but highly accurate purification is difficult to realize

Engineering Contradiction:
Improvetarget component extractionVSAvoidpurification accuracy
Core Design Contradiction:
Quantity of substanceVSManufacturing precision

Solution Approach 1:

The invention introduces an adsorbent as an intermediary substance between the gas phase and collection container. The adsorbent mediates the purification process by selectively adsorbing the target component from the gas stream, enabling highly accurate purification that is difficult to achieve through direct gas handling alone.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system enables highly efficient and stable fractionation of target components by controlling temperature and switching mechanisms to adsorb and collect the target component effectively, preventing system blockage and ensuring consistent purification.

Implementation Method 1

a collection tube filled with an adsorbent having a property of adsorbing a target component in the sample gas under a condition of a first temperature or less and desorbing the adsorbed target component under a condition of a second temperature or more higher than the first temperature

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

a temperature adjuster for adjusting a temperature of the collection tube by cooling and heating the collection tube

Methodology Applied
Scientific EffectCooling: Cooling

Implementation Method 3

a temperature adjuster for adjusting a temperature of the collection tube by cooling and heating the collection tube

Methodology Applied
Scientific EffectHeating: Heating

Data Source

PatentUS11879878B2Gas separation system
Publication Date: 2024.01.23 SHIMADZU CORP
  • US11879878B2 patent drawing
  • US11879878B2 patent drawing
  • US11879878B2 patent drawing

AI summary

A gas separation system includes a separation column for separating components contained in sample gas, a sample gas supplier fluidly connected to an inlet of the separation column for supplying sample gas to the separation column, a detector fluidly connected to an outlet of the separation column, a collection tube filled with an adsorbent having a property of adsorbing a target component in the sample gas under a condition of a first temperature or less and desorbing the adsorbed target component under a condition of a second temperature or more higher than the first temperature, a temperature adjuster for adjusting a temperature of the collection tube, a collection container for collecting the target component, and a switching mechanism for switching between a state in which the collection tube is connected to an outlet of the detector and a state in which the collection tube is connected to the collection container.