Ge-core Waveguide Low-Temperature Shell Deposition

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Solution Overview

Problem

Conventional industrial production methods for infrared medium spectrum optical waveguides result in degraded performance due to core alterations, such as deformation and faceting, which affect the integrity and optical index contrast of the waveguides.

Innovation Solution

A method involving the deposition of a germanium-based core followed by a low-temperature shell and a high-temperature encapsulation layer, with specific temperature and composition controls to maintain core integrity and enhance optical index contrast, allowing for industrial-scale production without performance degradation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If high-temperature deposition is used to deposit thick encapsulation layers, then industrial productivity and deposition speed are improved, but core deformation and alteration occur leading to degraded waveguide performance

Engineering Contradiction:
Improvedeposition speedVSAvoidcore shape precision
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The encapsulation layer is divided into two distinct parts: a first encapsulation layer deposited at low temperature (≤780°C) to protect the core, and a second encapsulation layer deposited at high temperature for thick layer formation. This segmentation allows each layer to serve different functions - the first layer prevents core deformation while the second layer provides the necessary thickness for effective encapsulation, thus resolving the contradiction between productivity and precision.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The first encapsulation layer is deposited at low temperature before the second high-temperature encapsulation layer. This preliminary action creates a protective barrier that prevents core deformation and alteration during the subsequent high-temperature deposition process, enabling the second layer to be deposited at high temperature without harming the core, thus achieving both high productivity and core shape precision.

Inventive Principle:
Principle #10Preliminary action

2Speed

If high-temperature deposition is used, then growth speed of encapsulation layer is increased, but atomic mobility increases causing core material redistribution and deformation

Engineering Contradiction:
Improvegrowth speedVSAvoidcore composition stability
Core Design Contradiction:
SpeedVSStability of the object's composition

Solution Approach 1:

The encapsulation process is segmented into two stages with different temperature conditions. The first stage uses low temperature (≤780°C) to minimize atomic mobility and preserve core composition stability. The second stage uses high temperature for rapid growth of the remaining encapsulation layer. This segmentation allows the system to achieve high overall growth speed while maintaining core composition stability during the critical initial phase.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The low-temperature deposition of the first encapsulation layer is performed as a preliminary action before high-temperature deposition. This preliminary layer is deposited when atomic mobility is low, preventing core material redistribution. Subsequently, the high-temperature deposition can proceed rapidly to complete the encapsulation, achieving both fast growth speed and core composition stability.

Inventive Principle:
Principle #10Preliminary action

3Reliability

If thick encapsulation layers are deposited to ensure proper cladding, then waveguide performance is improved, but deposition time increases reducing industrial yield

Engineering Contradiction:
Improvewaveguide performanceVSAvoiddeposition time
Core Design Contradiction:
ReliabilityVSLoss of time

Solution Approach 1:

The thick encapsulation layer is segmented into two deposition stages. The first stage deposits a portion of the required thickness at low temperature, ensuring core protection and performance. The second stage deposits the remaining thickness at high temperature, significantly reducing deposition time. This segmentation allows the waveguide to achieve proper cladding thickness for reliable performance while minimizing total deposition time through the use of high-temperature rapid deposition for the majority of the layer.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The deposition temperature parameter is changed between two stages: first stage at low temperature (≤780°C) for core-protection-critical initial layer, and second stage at high temperature for rapid thick layer deposition. This parameter change enables the system to balance between ensuring adequate encapsulation thickness for waveguide performance and reducing overall deposition time to improve industrial yield.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method preserves the rectangular cross-section of the core and maintains high optical index contrast, ensuring effective confinement and propagation of infrared light fluxes, thus achieving compatible industrial yields with preserved waveguide performance.

Implementation Method 1

The encapsulation layer is advantageously deposited by epitaxy at a temperature Tencapsulation epitaxy such that: Tencapsulation epitaxy≥1.08*Tshell epitaxy

Methodology Applied
Scientific EffectEpitaxy: Epitaxy

Implementation Method 2

the deposition by epitaxy of the shell being done at a temperature: Tshell epitaxy≤780° C.

Methodology Applied
Scientific EffectEpitaxy: Epitaxy

Data Source

PatentUS11236417B2Method for producing Ge-core based waveguides
Publication Date: 2022.02.01 COMMISSARIAT A LENERGIE ATOMIQUE ET AUX ENERGIES ALTERNATIVES
  • US11236417B2 patent drawing
  • US11236417B2 patent drawing
  • US11236417B2 patent drawing

AI summary

A method for producing a waveguide including a germanium-based core and a cladding is provided, the method including a step of “low temperature” depositing of a shell after forming the core by engraving, such that the deposition temperature is less than 780° C., followed by a step of “high temperature” depositing of a thick encapsulation layer. The shell and the encapsulation layer at least partially form the cladding of the waveguide. Optionally, a step of annealing under hydrogen at a “low temperature”, less than 750° C., precedes the deposition of the shell. These “low temperature” annealing and depositing steps advantageously make it possible to avoid a post-engraving alteration of the free surfaces of the core during the forming of the cladding which is less germanium-rich.