Getter Systems with Porous Active Phase in Low Permeability Polymer

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Solution Overview

Problem

Existing getter systems face challenges such as insufficient cohesion of powder materials, hindrance of gas sorption reactions due to matrix permeability, and changes in optical properties in applications like OLEDs due to moisture absorption, which affect their performance and transparency.

Innovation Solution

A getter system with a porous material active in gas sorption is inserted inside a low permeability polymeric means, where the active phase is present within the pores of a dispersed 'guest' phase, maintaining invariant physical properties and allowing for reversible or non-reversible reactions, and potentially acting as a catalyst, while being transparent and maintaining optical consistency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Speed

If getter material is dispersed in a permeable matrix, then gas sorption speed is improved, but structural modifications of getter particles are hindered

Engineering Contradiction:
Improvegas sorption speedVSAvoidstructural modifications capability
Core Design Contradiction:
SpeedVSReliability

Solution Approach 1:

The patent applies local quality by creating distinct regions with different permeability characteristics. The matrix has controlled permeability to allow gas transport, while local zones around getter particles provide structural support. This enables gas to reach getter particles quickly while allowing particles to undergo necessary structural modifications for effective sorption.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent uses composite materials by combining matrix material with getter particles in a structured arrangement. The composite structure integrates the gas-permeable properties of the matrix with the sorption capabilities of getter particles, while the matrix provides mechanical support that allows structural modifications without compromising overall integrity.

Inventive Principle:
Principle #40Composite materials

2Reliability

If getter material is dispersed in a non-permeable matrix, then structural modifications are allowed, but gas sorption reaction is hindered

Engineering Contradiction:
Improvestructural modifications capabilityVSAvoidgas sorption reaction
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The patent creates local quality variations where the matrix provides structural support in certain regions while maintaining gas permeability in transport pathways. This allows getter particles to undergo structural modifications where needed while still enabling gas sorption reactions through controlled permeable zones.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The matrix acts as an intermediary that mediates between the conflicting requirements of structural support and gas permeability. It provides mechanical support to allow structural modifications while its controlled permeability enables gas transport to getter particles, thus facilitating sorption reactions.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Quantity of substance

If getter particles absorb moisture, then sorption capacity is improved, but optical properties change

Engineering Contradiction:
Improvemoisture absorption capacityVSAvoidoptical transparency
Core Design Contradiction:
Quantity of substanceVSIllumination intensity

Solution Approach 1:

The patent extracts the optical sensitivity issue from the sorption function by using an optical coupling medium with refractive index matching. This allows the getter particles to absorb moisture for sorption capacity while the coupling medium maintains optical transparency by compensating for refractive index changes.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent applies parameter changes by selecting materials with specific refractive index properties. The optical coupling medium is chosen to have a refractive index that remains stable or changes in a controlled manner, allowing the system to maintain optical transparency even as getter particles undergo moisture absorption and their own refractive index changes.

Inventive Principle:
Principle #35Parameter changes

4Illumination intensity

If getter particles are small, then optical transparency is maintained, but sorption efficiency decreases

Engineering Contradiction:
Improveoptical transparencyVSAvoidsorption efficiency
Core Design Contradiction:
Illumination intensityVSProductivity

Solution Approach 1:

The patent applies local quality by creating a heterogeneous structure where small getter particles are distributed throughout the matrix. The small particles maintain optical transparency, while their distributed arrangement and the matrix structure provide sufficient total surface area and pathways for effective sorption.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent transitions from considering only particle size to a multi-dimensional approach by optimizing the spatial distribution, concentration, and arrangement of particles in three-dimensional space. This allows small particles to maintain transparency while their collective distribution provides sufficient sorption efficiency.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration ensures prolonged efficacy and transparency by preventing external interaction with the matrix, allowing for effective gas sorption without altering the system's optical properties, thus enhancing the performance and lifespan of devices like OLEDs.

Implementation Method 1

Getter materials and systems are widely used in industry in all the applications wherein it is necessary to keep the vacuum, to control the composition of the gaseous atmosphere through the sorption of traces of undesired gases

Methodology Applied
Scientific EffectSorption: Sorption

Implementation Method 2

Another possible approach to the problem is to distribute the getter material inside a dispersing matrix, capable of retaining the getter particles in a fixed location while letting the gases pass towards the getter itself

Methodology Applied
Scientific EffectPermeation barrier: Permeation

Data Source

PatentEP1912734B1Getter systems comprising an active phase inserted in a porous material distributed in a low permeability means
Publication Date: 2012.05.16 SAES GETTERS SPA
  • EP1912734B1 patent drawingFigure 1~2
  • EP1912734B1 patent drawingFigure 3a~3b

AI summary

Getter systems are described, comprised of a phase (21, 21 ', 21 ", ...) active in the sorption of gas, inserted in the pores (20, 20', ...) of a porous material (12), which is in turn dispersed in a polymeric means (11) with a low permeability to the gas to be sorbed.