Glass-Ceramic Solid Electrolyte for Safe Lithium-Ion Batteries

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Solution Overview

Problem

Current batteries face issues such as electrolyte leakage and thermal runaway, particularly in lithium-ion batteries, and there is a need for solid electrolytes with high lithium ion conductivity to replace traditional liquid electrolytes.

Innovation Solution

A glass-ceramic material containing lithium (Li), silicon (Si), and boron (B) with specific X-ray diffraction spectra is developed for use in batteries, enhancing ionic conductivity and stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If liquid electrolytes are used in batteries, then battery performance can be maintained, but electrolyte leakage and thermal runaway occur

Engineering Contradiction:
Improvebattery safetyVSAvoidelectrolyte leakage and thermal runaway
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent changes the physical state parameter of the electrolyte from liquid to solid by developing glass-ceramic materials with specific compositional parameters (Li2O: 40-73 mol%, SiO2: 8-40 mol%, B2O3: 10-50 mol%). This phase change eliminates leakage risks while the crystalline structure provides thermal stability against runaway

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite glass-ceramic material combining amorphous glass matrix with crystalline phases. The glass matrix provides flexibility and ion transport pathways, while the crystalline phases (indicated by XRD peaks) provide structural stability and high lithium ion conductivity, achieving both safety and performance

Inventive Principle:
Principle #40Composite materials

2Reliability

If solid electrolytes are used to eliminate leakage, then battery safety improves, but lithium ion conductivity may be reduced

Engineering Contradiction:
Improvebattery safetyVSAvoidlithium ion conductivity
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The patent optimizes compositional parameters within specific ranges to achieve high ionic conductivity in solid electrolytes. The Li2O content (40-73 mol%) provides sufficient lithium ions for conduction, while SiO2 and B2O3 form a glass network that facilitates ion transport. The resulting material achieves conductivity comparable to liquid electrolytes while maintaining solid-state safety

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent utilizes controlled phase transition from amorphous glass to crystalline glass-ceramic structure through heat treatment. This phase transition creates ordered pathways for lithium ion transport while maintaining the solid-state form, achieving high conductivity without sacrificing safety

Inventive Principle:
Principle #36Phase transitions

3Quantity of substance

If glass-ceramic material is developed with specific composition, then ionic conductivity improves, but manufacturing complexity increases

Engineering Contradiction:
Improvelithium ion conductivityVSAvoidmanufacturing process complexity
Core Design Contradiction:
Quantity of substanceVSDevice complexity

Solution Approach 1:

The patent defines specific compositional ranges for Li2O, SiO2, and B2O3 that can be achieved through conventional ceramic processing. By specifying mol% ranges rather than exact compositions, the patent allows for manufacturing tolerance while ensuring high ionic conductivity. The composition parameters are optimized to be attainable through standard mixing and firing processes

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs a two-stage thermal process: initial glass formation followed by controlled crystallization. This phase transition approach uses standard ceramic processing techniques (melting, cooling, heat treatment) rather than requiring advanced manufacturing equipment, making the complex glass-ceramic structure achievable through conventional industrial processes

Inventive Principle:
Principle #36Phase transitions

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The glass-ceramic material improves ionic conductivity and stability, reducing the risk of leakage and thermal runaway, while enabling high energy density batteries with improved charge-discharge characteristics and cycle performance.

Implementation Method 1

there has been a demand for solid electrolytes having high lithium ion conductivity

Methodology Applied
Scientific EffectIonic conduction: Conduction (electrical)

Implementation Method 2

having an X-ray diffraction spectrum with two or more peaks appearing in the range 20° ≤ 2θ ≤ 25° and with two or more peaks appearing in the range 25° ≤ 2θ ≤ 30°

Methodology Applied
Scientific EffectX-ray diffraction: Bragg Diffraction

Data Source

PatentEP3220393B1Glass ceramic, lithium-ion conductor, cell, electronic device, and method for manufacturing electrode
Publication Date: 2021.06.30 MURATA MFG CO LTD
  • EP3220393B1 patent drawingFigure 1
  • EP3220393B1 patent drawingFigure 2~4
  • EP3220393B1 patent drawingFigure 5

AI summary

A glass-ceramic includes an oxide containing lithium (Li), silicon (Si), and boron (B) and has an X-ray diffraction spectrum with two or more peaks appearing in the range 20° ≤ 2θ ≤ 25° and with two or more peaks appearing in the range 25° < 2θ ≤ 30°.