Glass Preform Manufacturing with Alkali Metal Particle Doping

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Solution Overview

Problem

Current methods for manufacturing optical fibers doped with alkali metal oxide or alkaline earth metal oxide face challenges in accurately controlling the concentration of additives and are energy-intensive, with existing techniques either being inefficient or introducing unnecessary chemical species that increase transmission loss.

Innovation Solution

An apparatus and method involving a dummy tube section with a reservoir for heating alkali metal or alkaline earth metal compounds, where the vapor is cooled and condensed into particles, which are then deposited onto a glass tube section using a second heat source, allowing for precise control of additive concentration and dispersion within the glass preform.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If conventional methods using aqueous solutions of alkali metal compounds are used, then the manufacturing process is simpler, but moisture mixing occurs which increases transmission loss

Engineering Contradiction:
Improvemanufacturing process simplicityVSAvoidtransmission loss
Core Design Contradiction:
Ease of manufactureVSObject-affected harmful factors

Solution Approach 1:

The invention changes the physical state parameter of the alkali metal compound from liquid (aqueous solution) to solid (fine particles), eliminating moisture content while maintaining ease of application through particle deposition methods

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention utilizes phase transition by converting alkali metal compounds into fine particulate form that can be deposited as solid particles, avoiding the liquid phase that introduces moisture and subsequent transmission loss

Inventive Principle:
Principle #36Phase transitions

2Quantity of substance

If composite salts with higher vapor pressure are used, then the vapor pressure increases, but unnecessary chemical species are added which increases transmission loss

Engineering Contradiction:
Improvevapor pressureVSAvoidtransmission loss
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The invention extracts only the necessary alkali metal element from composite salts, using pure alkali metal compounds or oxides directly, thereby eliminating unnecessary chemical species that would increase transmission loss while maintaining adequate vapor pressure for doping

Inventive Principle:
Principle #2Taking out (Extraction)

3Quantity of substance

If strong heating is applied to generate alkali metal vapor, then alkali metal vapor is produced, but the reaction mechanism is indefinite and energy consumption is high

Engineering Contradiction:
Improvealkali metal vaporVSAvoidenergy consumption
Core Design Contradiction:
Quantity of substanceVSUse of energy by moving object

Solution Approach 1:

The invention changes the chemical form parameter from requiring pure alkali metal vapor to using alkali metal compounds or oxides that can be introduced in solid particle form, reducing the heating temperature required and making the reaction mechanism more controllable and energy-efficient

Inventive Principle:
Principle #35Parameter changes

4Stability of the object's composition

If alkali metal salts are used as raw materials, then the salts are solid at ambient conditions, but they form very strong ionic bonds making it difficult to form gaseous compounds

Engineering Contradiction:
Improvesalt stabilityVSAvoidgaseous compound formation
Core Design Contradiction:
Stability of the object's compositionVSQuantity of substance

Solution Approach 1:

The invention uses fine particles as an intermediary carrier form, allowing alkali metal compounds to be transported and deposited without requiring them to be in gaseous state, thus maintaining salt stability while enabling effective incorporation into the glass preform

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables the stable and accurate growth of glass preforms with controlled additive concentration, reducing energy consumption and minimizing the introduction of unwanted chemical species, thereby facilitating the production of low-loss optical fibers.

Implementation Method 1

heating with a first heat source, and a cooling portion; and a glass tube section provided at the second end of the dummy tube section and having an inner wall, in which particles of the alkali metal compound or the alkaline earth metal compound which have flowed into the glass tube section from the dummy tube section are heated by a second heat source which performs traverse, and oxide of the particles being deposited on the inner wall and dispersed in the glass tube section

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 2

In the cooling portion of the dummy tube section, vapor of the alkali metal compound or the alkaline earth metal compound generated by heating with the first heat source is cooled and condensed by the dry gas flowing into the dummy tube section between the reservoir portion and the second end, and thereby the particles are generated

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 3

particles of the alkali metal compound or the alkaline earth metal compound which have flowed into the glass tube section from the dummy tube section are heated by a second heat source which performs traverse, and oxide of the particles being deposited on the inner wall and dispersed in the glass tube section

Methodology Applied
Scientific EffectDeposition: Deposition (physical)

Data Source

PatentUS9416043B2Apparatus and method for manufacturing glass preform
Publication Date: 2016.08.16 FUJIKURA LTD
  • US9416043B2 patent drawing
  • US9416043B2 patent drawing
  • US9416043B2 patent drawing

AI summary

An apparatus for manufacturing a glass perform, includes: a dummy tube section, a reservoir portion, and a cooling portion; and a glass tube section in which particles of an alkali metal compound or an alkaline earth metal compound which have flowed into the glass tube section from the dummy tube section are heated by a second heat source which performs traverse, and oxides of the particles being deposited on an inner wall and dispersed in the glass tube section. In the cooling portion of the dummy tube section, vapor of the alkali metal compound or the alkaline earth metal compound generated by heating of a first heat source is cooled and condensed by a dry gas flowing into the dummy tube section, and thereby the particles are generated.