Glass Formation in Reduced Gravity via Parameter Changes

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Solution Overview

Problem

Existing methods for glass formation are limited by the constraints of normal gravity acceleration on Earth, which affects the critical cooling rate required to prevent crystallization and form glass.

Innovation Solution

A method for forming glass or amorphous materials by processing a liquid in an environment with a gravity acceleration less than that on Earth, utilizing a critical cooling rate that is lower in reduced gravity, allowing for glass formation without crystallization.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If glass formation is performed under normal gravity acceleration on Earth, then the critical cooling rate must be very high to prevent crystallization, but this high cooling rate limits the types of materials that can be processed and the quality of glass products

Engineering Contradiction:
Improvecooling rateVSAvoidglass formation process
Core Design Contradiction:
TemperatureVSEase of manufacture

Solution Approach 1:

The patent changes the gravitational acceleration parameter from normal Earth gravity to reduced gravity (microgravity) environment. This parameter change fundamentally alters the cooling behavior of liquids, allowing glass formation at much lower cooling rates and enabling processing of materials that would crystallize under normal gravity conditions.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a microgravity environment where gravitational potential differences are minimized throughout the liquid. This equipotential condition prevents gravity-driven convection and density-driven flow, allowing uniform cooling and glass formation without the complications of natural convection that occur under normal gravity.

Inventive Principle:
Principle #12Equipotentiality

2Reliability

If high cooling rates are used to form glass under normal gravity, then crystallization can be prevented, but the process becomes more difficult and limits material selection

Engineering Contradiction:
Improvecrystallization preventionVSAvoidcooling system
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

By changing the gravitational acceleration parameter to reduced gravity, the patent enables reliable crystallization prevention at much lower cooling rates. This parameter change transforms a difficult process requiring complex rapid cooling systems into a more manageable process with simpler cooling requirements.

Inventive Principle:
Principle #35Parameter changes

3Ease of manufacture

If normal gravity processing is used, then standard manufacturing equipment can be employed, but unique product structures such as uniformly distributed bubbles and multiple glass phases cannot be achieved

Engineering Contradiction:
Improvestandard equipmentVSAvoidproduct structure uniformity
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The patent changes the gravitational parameter to enable unique product structures. In microgravity, bubbles remain uniformly suspended in the liquid rather than rising to the surface, and multiple glass phases can be evenly distributed. This parameter change enables manufacturing precision in terms of structural uniformity that cannot be achieved under normal gravity.

Inventive Principle:
Principle #35Parameter changes

4Temperature

If glass formation is attempted under normal gravity with slow cooling, then crystallization occurs, but in reduced gravity slow cooling enables glass formation

Engineering Contradiction:
Improvecooling rateVSAvoidamorphous structure
Core Design Contradiction:
TemperatureVSStability of the object's composition

Solution Approach 1:

The patent changes the gravitational acceleration parameter, which fundamentally alters the phase transformation behavior of cooling liquids. In reduced gravity, slow cooling maintains the liquid's amorphous structure and prevents crystallization, whereas under normal gravity the same slow cooling rate would result in crystal formation.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method enables the formation of glass products with unique properties, such as the distribution of bubbles and voids, and multiple glass phases, which can be achieved without the limitations of normal gravity, resulting in novel material structures and properties.

Implementation Method 1

pieces of the material used are heated with a laser beam to increase their temperature to above the equilibrium melting point of the crystalline starting material

Methodology Applied
Scientific EffectLaser heating: Laser

Implementation Method 2

When they are completely molten, the liquid is cooled by turning the heating laser beam off

Methodology Applied
Scientific EffectCooling: Cooling

Implementation Method 3

Liquids that cool without crystallizing and form a glass or amorphous material do not show a thermal arrest

Methodology Applied
Scientific EffectVitrification: Vitrification

Data Source

PatentUS20250145513A1Method for glass formation and morphology of products made from non-equilibrium liquids by processing in reduced gravity
Publication Date: 2025.05.08 MATERIALS DEVELOPMENT INC
  • US20250145513A1 patent drawing
  • US20250145513A1 patent drawing
  • US20250145513A1 patent drawing

AI summary

Methods of making a product of glass or other amorphous material by processing a liquid in an environment with a gravity acceleration less than the normal gravity acceleration on Earth. Methods of forming glass at different gravity levels control the distribution of second phases, such as bubbles, voids or additional glassy phases of similar or different composition.