Grading Water-Absorbent Polymer Particles Using Segmented Sieves

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Solution Overview

Problem

Conventional classification processes for water-absorbing polymer particles face issues such as clogging, reduced selectivity, and product caking, leading to inefficient separation and increased downtimes, particularly when classifying post-crosslinked products.

Innovation Solution

A method involving the use of sieves with different mesh sizes to separate oversize particles before and after post-crosslinking, where the sieve with the lowest mesh size after post-crosslinking has a larger mesh size than before, allowing for higher throughput and reduced incorrect discharge, and incorporating a gas stream and temperature control during classification.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional sieving is used to classify water-absorbing polymer particles, then particle size separation is achieved, but sieve clogging and product caking occur leading to reduced classification efficiency and increased downtimes

Engineering Contradiction:
Improveparticle size separation efficiencyVSAvoidcontinuous operation capability
Core Design Contradiction:
Manufacturing precisionVSReliability

Solution Approach 1:

The classification process is divided into multiple stages with different sieve mesh sizes. First classification uses a coarse sieve (e.g., 850 μm) to remove large oversize particles, while second classification uses a fine sieve (e.g., 200 μm) to separate undersize particles. This segmentation prevents clogging by handling different particle size ranges separately, maintaining continuous operation capability.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Oversize particles are removed from the polymer powder before the main classification process. By performing preliminary removal of large particles that would cause clogging, the subsequent classification can proceed continuously without interruptions, resolving the reliability issue.

Inventive Principle:
Principle #10Preliminary action

2Manufacturing precision

If sieve mesh size is reduced to improve separation precision, then classification accuracy increases, but throughput decreases due to increased clogging tendency

Engineering Contradiction:
Improveparticle size classification accuracyVSAvoidmaterial throughput
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The classification is segmented into multiple passes with different sieve mesh sizes. Coarse sieving is performed first to remove large particles that would clog fine sieves, allowing the fine sieve to operate at high throughput without clogging, thus achieving both precision and productivity.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Large oversize particles are removed in advance before the fine classification step. This preliminary action prevents clogging of the fine sieve during high-throughput operation, enabling both accurate separation and high productivity to coexist.

Inventive Principle:
Principle #10Preliminary action

3Reliability

If post-crosslinking is performed before classification, then particle properties are optimized, but agglomerate formation increases leading to classification disruptions

Engineering Contradiction:
Improveproduct properties consistencyVSAvoidcontinuous classification capability
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

Classification is performed before post-crosslinking treatment. By classifying the particles while they are still in a more separable state, the process avoids the agglomerate formation that occurs after crosslinking, maintaining continuous classification capability while still achieving consistent product properties through subsequent crosslinking.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The process is segmented into classification step followed by post-crosslinking step. This temporal separation allows classification to be performed on particles before agglomerate formation, maintaining productivity, while post-crosslinking is then applied to optimize particle properties without disrupting the classification process.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enhances the selectivity and efficiency of the classification process, reducing the proportion of undersize particles in the oversize fraction and maintaining high classifying performance even at increased throughputs, thereby minimizing disruptions and improving product quality.

Implementation Method 1

sieves with different mesh sizes are used to separate the oversize material before and after post-crosslinking

Methodology Applied
Scientific EffectMechanical filtration: Filter (physical)

Implementation Method 2

Suitable crosslinkers for this purpose are compounds containing at least two groups that can form covalent bonds with the carboxylate groups of the hydrophilic polymer

Methodology Applied
Scientific EffectCovalent bonding: Chemical Bonding

Implementation Method 3

incorporating a gas stream and temperature control during classification

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentEP2073943B2Method for grading water-absorbent polymer particles
Publication Date: 2020.09.02 BASF SE
  • EP2073943B2 patent drawing

AI summary

The invention relates to a method for grading water-absorbent polymer particles. The invention is characterized by using sieves having different mesh sizes before and after secondary crosslinking to separate oversize particles.