Graphene Transfer via Electrochemical Bubble Separation

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Solution Overview

Problem

Current techniques face challenges in forming high-quality graphene thin layers on insulation layers, which are essential for semiconductor devices, due to difficulties in graphene growth and transfer processes.

Innovation Solution

An apparatus and method involving a graphene structure with a metal catalyst layer, insulation layer, protection layer, and electrolyte, where a voltage is applied to separate the metal catalyst layer from the substrate, allowing for the transfer of a graphene layer onto a target insulation layer using chemical reactions and bubble generation, minimizing mechanical damage.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If graphene is grown on a metal thin layer using chemical vapor deposition or thermal decomposition, then high-quality graphene can be formed, but the graphene cannot be directly used in semiconductor devices because it requires an insulation layer

Engineering Contradiction:
Improvegraphene qualityVSAvoidgraphene transfer process
Core Design Contradiction:
Manufacturing precisionVSEase of manufacture

Solution Approach 1:

The patent introduces an insulation layer as an intermediary between the substrate and the metal catalyst layer. This insulation layer enables the graphene to be grown in a configuration that allows direct integration with semiconductor devices, eliminating the need for complex transfer processes while maintaining high graphene quality.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Manufacturing precision

If the metal catalyst layer is separated from the substrate using conventional methods, then graphene transfer is achieved, but mechanical damage occurs to the graphene layer

Engineering Contradiction:
Improvegraphene transfer qualityVSAvoidmechanical damage
Core Design Contradiction:
Manufacturing precisionVSObject-affected harmful factors

Solution Approach 1:

The patent replaces mechanical separation methods with an electrochemical approach. By applying voltage to generate bubbles that chemically separate the metal catalyst layer from the substrate, the method eliminates mechanical contact and friction that would otherwise damage the delicate graphene layer during transfer.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Productivity

If graphene is transferred using conventional techniques, then the graphene layer can be moved to the target substrate, but the process is complex and time-consuming

Engineering Contradiction:
Improvemanufacturing efficiencyVSAvoidtransfer process steps
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent merges multiple process steps into a single integrated operation. The electrochemical separation, graphene release, and transfer to the target substrate occur simultaneously in one process, eliminating the need for separate mechanical separation and transfer steps, thereby simplifying the overall manufacturing process and improving productivity.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables the transfer of high-quality graphene layers onto target substrates, facilitating the manufacturing of graphene devices with improved electrical conductivity and reduced damage, thus overcoming previous challenges in graphene growth on insulation layers.

Implementation Method 1

a power unit configured to apply a voltage between the electrode and the metal catalyst layer, and an electrolyte in which the graphene structure is at least partially submerged

Methodology Applied
Scientific EffectElectrolysis: Electrolysis

Implementation Method 2

separating the metal catalyst layer from the substrate by generating bubbles due to chemical reactions occurring in an area between the substrate and the metal catalyst layer

Methodology Applied
Scientific EffectBubble generation through chemical reactions: Bubble

Data Source

PatentEP2690198B1Apparatus and graphene device manufacturing method using the apparatus
Publication Date: 2018.10.03 SAMSUNG ELECTRONICS CO LTD
  • EP2690198B1 patent drawingFigure 1
  • EP2690198B1 patent drawingFigure 2
  • EP2690198B1 patent drawingFigure 3A~3B

AI summary

A graphene device manufacturing apparatus includes an electrode, a graphene structure including a metal catalyst layer formed on a substrate, a protection layer, and a graphene layer between the protection layer and the metal catalyst layer, a power unit configured to apply a voltage between the electrode and the metal catalyst layer, and an electrolyte in which the graphene structure is at least partially submerged.