Graphene Manufacturing via Catalyst Tension

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Solution Overview

Problem

Current methods for manufacturing graphene often result in non-uniform and low-quality graphene due to limitations in catalyst metal layer grain size and orientation, which affect the electrical and mechanical properties of the final product.

Innovation Solution

Applying tension to a catalyst metal layer within a chamber during the graphene synthesis process increases the grain size and changes the orientation from (001) to (111), facilitating the growth of high-quality, uniform graphene by enhancing the diffusion of carbon atoms and improving crystalline structure.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If tension is applied to the catalyst metal layer, then the grain size increases and orientation changes to (111), but the device complexity increases due to the need for a tension unit

Engineering Contradiction:
Improvegraphene uniformityVSAvoidapparatus structure
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The catalyst metal layer is pre-treated by applying tension before the actual graphene deposition process. This preliminary action of tension application during a pre-heating stage prepares the catalyst layer with optimal grain size and (111) orientation, ensuring high-quality graphene growth without requiring complex modifications to the main deposition process

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent applies tension as a physical parameter change to the catalyst metal layer, transforming its microstructure from a random grain structure to a uniform (111) oriented structure with larger grain size. This parameter change directly improves graphene uniformity by providing a more consistent template for carbon atom deposition

Inventive Principle:
Principle #35Parameter changes

2Manufacturing precision

If tension is applied to increase grain size and change orientation, then graphene quality improves, but the manufacturing process time increases due to additional process steps

Engineering Contradiction:
Improvegraphene qualityVSAvoidmanufacturing cycle time
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

The tension application process is merged with the pre-heating stage of the chemical vapor deposition process. Instead of being a separate sequential step, the tension is applied simultaneously while the catalyst layer is being heated to deposition temperature, thus achieving grain structure optimization without adding to the total manufacturing cycle time

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The tension application maintains continuous useful action throughout the pre-heating phase. The catalyst layer remains under tension continuously from the start of heating until the deposition begins, ensuring that the grain structure optimization occurs continuously during the entire pre-heating period rather than as an intermittent or separate operation

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method achieves increased grain size and optimal orientation of the catalyst metal layer, leading to the formation of high-quality, uniform graphene with superior electrical and mechanical properties, suitable for advanced electronic devices.

Implementation Method 1

it is possible to increase the grain size of a catalyst metal layer by applying tension to the catalyst metal layer

Methodology Applied
Scientific EffectGrain growth:

Implementation Method 2

it is possible to change an orientation of the catalyst metal layer into (111) orientation by applying tension to the catalyst metal layer

Methodology Applied
Scientific EffectOrientation change:

Implementation Method 3

achieving growth of high quality uniform graphene through use of the catalyst metal layer

Methodology Applied
Scientific EffectCarbon diffusion: Diffusion

Data Source

PatentUS9764956B2Method for manufacturing graphene, said graphene, and apparatus for manufacturing same
Publication Date: 2017.09.19 LG ELECTRONICS INC
  • US9764956B2 patent drawing
  • US9764956B2 patent drawing
  • US9764956B2 patent drawing

AI summary

The present invention provides a method for manufacturing graphene, said graphene, and an apparatus for manufacturing same. The method for manufacturing graphene comprises the steps of: loading a catalytic metal layer into a chamber; applying tensile force to the catalytic metal layer; and forming graphene on the catalytic metal layer by supplying a carbon source into the chamber while the tension is applied to the catalytic metal layer. Therefore, the size of the grains on the catalytic metal layer can be increased by applying tension to the catalytic metal layer, and high quality uniform graphene can be grown through the use of the catalytic metal layer.