Graphene Synthesis via Heat Conversion Unit

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Solution Overview

Problem

Current graphene synthesis methods require high-temperature environments and struggle to efficiently synthesize graphene wires due to the need for uniform heat distribution and catalyst shape compatibility.

Innovation Solution

A graphene synthesis apparatus with a chamber, a heating unit, and a heat conversion unit where a thin and long metal catalyst is placed on the heat conversion unit, allowing for efficient conductive heat transfer and graphene wire synthesis, aided by a quartz wall for maintaining a vacuum and preventing contamination.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If a heating unit is used to provide high-temperature environment for graphene synthesis, then graphene can be formed on the catalyst surface, but uniform heat distribution becomes difficult to achieve

Engineering Contradiction:
Improvecatalyst temperatureVSAvoidheat distribution uniformity
Core Design Contradiction:
TemperatureVSManufacturing precision

Solution Approach 1:

A heat conversion unit made of graphite is introduced as an intermediary between the heating unit and the catalyst. This heat conversion unit absorbs radiant heat from the heating unit and converts it to conductive heat, which is then uniformly transferred to the catalyst surface, solving the heat distribution uniformity problem while maintaining the required high temperature for graphene synthesis.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Productivity

If traditional CVD method is used for graphene synthesis, then graphene can be produced on metal catalyst surface, but synthesis of graphene wires with specific shapes is difficult

Engineering Contradiction:
Improvegraphene production efficiencyVSAvoidcatalyst shape compatibility
Core Design Contradiction:
ProductivityVSAdaptability or versatility

Solution Approach 1:

The heat conversion unit is designed to be applicable to various catalyst shapes including wires, rods, and other non-planar structures. By converting radiant heat to conductive heat that can be uniformly distributed along the catalyst surface regardless of its shape, the system achieves universal applicability for synthesizing graphene on different catalyst geometries, not just flat surfaces.

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Use of energy by moving object

If radiant heat is directly applied to the catalyst, then heating efficiency is high, but heat distribution on the catalyst surface is non-uniform

Engineering Contradiction:
Improveheating efficiencyVSAvoidheat distribution uniformity
Core Design Contradiction:
Use of energy by moving objectVSManufacturing precision

Solution Approach 1:

The heat conversion unit changes the physical parameter of heat transfer from radiant (electromagnetic radiation) to conductive (direct thermal contact). This parameter change allows the heat to be uniformly distributed through the conductive properties of the graphite material while maintaining high heating efficiency, as the conductive heat is evenly transferred from the heated graphite surface to the catalyst.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables easy synthesis of graphene wires by efficiently raising the catalyst temperature and maintaining a clean synthesis environment, facilitating large-area graphene production.

Implementation Method 1

the heat conversion unit may convert radiant heat from the heating unit to conductive heat, and the conductive heat may be directly transferred to the catalyst on a surface of the heat conversion unit

Methodology Applied
Scientific EffectRadiant heat conversion to conductive heat: Thermal Radiation

Implementation Method 2

Graphene is synthesized on a surface of a metal catalyst by a chemical vapor deposition (CVD) method by providing a gas including carbon to the surface

Methodology Applied
Scientific EffectChemical vapor deposition: Chemical Vapour Deposition

Implementation Method 3

As the gas including carbon dissociates under high-temperature conditions, graphene may form on the surface of the metal catalyst

Methodology Applied
Scientific EffectGas dissociation: Pyrolysis

Data Source

PatentUS10882748B2Graphene synthesis apparatus and graphene synthesis method using the same
Publication Date: 2021.01.05 HAESUNG CO LTD
  • US10882748B2 patent drawing
  • US10882748B2 patent drawing
  • US10882748B2 patent drawing

AI summary

Provided is a graphene synthesis apparatus including a chamber; a heating unit provided in the chamber; a heat conversion unit provided closer to a central portion of the chamber than the heating unit; and a catalyst provided on the heat conversion unit, wherein the catalyst is formed of thin and long metal.