Graphene Preparation via 55-65 Hz Vibration Exfoliation

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Solution Overview

Problem

Existing methods for preparing graphene using graphite and a dispersant result in low process yield and high manufacturing costs due to excessive grinding and the need for optimal dispersant adjustments, limiting the flexibility and efficiency of the process.

Innovation Solution

A method involving the preparation of graphite and applying vibration at a frequency of 55 Hz to 65 Hz to a vessel without using a dispersant, allowing for exfoliation and formation of graphene with improved yield and reduced costs.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If a dispersant is used to prepare graphene by grinding graphite, then the graphene can be exfoliated and dispersed, but the graphene is excessively ground and the process yield is low

Engineering Contradiction:
Improvegraphene size and shape controlVSAvoidprocess yield
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The invention extracts and removes the dispersant from the preparation process, using only vibration to achieve graphene exfoliation without the harmful grinding effect that dispersants cause, thereby preventing excessive ground and improving process yield

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention applies mechanical vibration at a specific frequency (55-65 Hz) to the vessel containing graphite to achieve exfoliation and formation of graphene, replacing the chemical/mechanical action of dispersants with controlled vibration that prevents excessive grinding

Inventive Principle:
Principle #18Mechanical vibration

2Reliability

If a dispersant is used to prepare graphene, then the graphene can be prepared, but the process becomes complex and manufacturing cost increases

Engineering Contradiction:
Improvegraphene preparation effectivenessVSAvoidprocess complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The invention removes the dispersant component from the preparation system, simplifying the process to only require vibration while maintaining effective graphene preparation, thereby reducing process complexity and manufacturing cost

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The vibration process itself performs both the exfoliation and dispersion functions that previously required separate dispersant addition and optimization, allowing the system to prepare graphene through self-contained mechanical action

Inventive Principle:
Principle #25Self-service

3Manufacturing precision

If a dispersant is used to prepare graphene, then the graphene can be formed, but the process flexibility is reduced due to optimal adjustment requirements

Engineering Contradiction:
Improvegraphene formation qualityVSAvoidprocess flexibility
Core Design Contradiction:
Manufacturing precisionVSAdaptability or versatility

Solution Approach 1:

By removing the dispersant variable from the process, the invention eliminates the need to optimize dispersant type and ratio for different raw materials, thereby restoring process flexibility while maintaining graphene formation quality through vibration control

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention changes the control parameter from chemical composition (dispersant type and ratio) to physical parameter (vibration frequency 55-65 Hz), which is easier to control and adjust, thereby improving process flexibility and adaptability

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach prevents excessive grinding, simplifies the process, and enables the production of high-quality graphene with desired size and shape, reducing manufacturing costs and enhancing process efficiency.

Implementation Method 1

applying vibration at a frequency of 55 Hz to 65 Hz to the vessel

Methodology Applied
Scientific EffectVibration: Vibration

Data Source

PatentUS11254576B2Method of preparing graphene
Publication Date: 2022.02.22 LG ENERGY SOLUTION LTD
  • US11254576B2 patent drawing
  • US11254576B2 patent drawing
  • US11254576B2 patent drawing

AI summary

A method of preparing graphene, including preparing graphite; and putting the graphite in the inside of a vessel and applying vibration at a frequency of 55 Hz to 65 Hz to the vessel.