Graphite Powder Production Using Particulate Functional Filler

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Solution Overview

Problem

Existing graphitization processes, such as the Acheson method, face challenges in producing homogeneous graphite due to non-uniform heating, high costs, and cumbersome equipment setups, limiting productivity and flexibility.

Innovation Solution

The use of a graphitic material in particulate form as a 'functional filler' within an Acheson-type oven allows for controlled resistive heating, eliminating the need for graphite containers and enabling flexible configuration and uniform heating by adjusting the spatial arrangement of carbonaceous and graphitic materials.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Use of energy by moving object

If a solid core of graphite is used in the Acheson process, then resistive heating can be achieved, but non-uniform heating occurs leading to inhomogeneous graphite product

Engineering Contradiction:
Improveresistive heating efficiencyVSAvoidhomogeneity of graphite product
Core Design Contradiction:
Use of energy by moving objectVSManufacturing precision

Solution Approach 1:

The solid core of graphite is replaced by a plurality of graphite particles arranged in a matrix, transforming the continuous solid structure into a segmented particulate structure. This segmentation allows electrical current to flow through multiple pathways among the particles, achieving more uniform resistive heating throughout the carbonaceous material and eliminating the radial heat gradient caused by the solid core configuration.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention changes the physical state and arrangement parameters of the heating element from a continuous solid core to a particulate matrix system. By controlling parameters such as particle size distribution, particle arrangement, and matrix composition, the electrical conductivity and heat distribution are optimized to achieve uniform heating and homogeneous graphite product.

Inventive Principle:
Principle #35Parameter changes

2Manufacturing precision

If graphite containers are used to hold carbonaceous material, then heating can be controlled, but production costs increase

Engineering Contradiction:
Improveheating controlVSAvoidproduction cost
Core Design Contradiction:
Manufacturing precisionVSEase of manufacture

Solution Approach 1:

The graphite containers are completely removed from the process. Instead of using containers to hold and heat the carbonaceous material, the material is directly mixed with graphite particles in a matrix that provides both structural support and resistive heating. This elimination of intermediate containers simplifies the process and reduces production costs while maintaining heating control through the particulate matrix system.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The functions of the container (holding material) and the heating element (resistive heating) are merged into a single integrated system where graphite particles serve both as the heating source and as part of the material matrix. This consolidation eliminates the need for separate graphite containers and reduces overall material and processing costs.

Inventive Principle:
Principle #5Merging (Combining)

3Productivity

If pre-grinding of carbonaceous material is performed, then surface activity is increased, but additional processing steps and costs are required

Engineering Contradiction:
Improvesurface activity of graphiteVSAvoidprocessing steps
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The graphite particles are pre-dispersed and arranged in the matrix before the graphitization process, creating a structure that inherently provides high surface area and reactivity. This preliminary arrangement of particles eliminates the need for post-graphitization grinding to achieve the desired surface activity, as the particulate structure itself provides the necessary surface characteristics.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The graphite particles in the matrix serve multiple functions simultaneously: they provide resistive heating, act as a scaffold for the carbonaceous material, and contribute to the final surface characteristics of the product. The system is self-sufficient, requiring no additional grinding or surface treatment steps.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach results in a more homogeneous and cost-effective production of graphite with improved control over heating conditions, reducing the need for pre-grinding and enhancing the efficiency of the graphitization process.

Implementation Method 1

a functional filler consisting essentially of graphitic material in particulate form is added to the reactor for allowing electrical current to flow through the charge

Methodology Applied
Scientific EffectResistive heating (Joule effect): Joule Heating

Implementation Method 2

thermal conduction (indirect heating)

Methodology Applied
Scientific EffectThermal conduction: Conduction (thermal)

Data Source

PatentEP2373580B1Process for the production and treatment of graphite powders
Publication Date: 2018.08.08 IMERTECH SAS
  • EP2373580B1 patent drawingFigure 1
  • EP2373580B1 patent drawingFigure 2
  • EP2373580B1 patent drawingFigure 3

AI summary

The invention relates to processes for the production and thermal treatment of carbon material, in particular graphite powders, in an Acheson type oven, using a functional filler comprised essentially of graphitic material in particulate form allowing electrical current to flow through the charge. The particulate form of the filler allows greater flexibility and can be used to control the degree of direct and indirect heating, resulting in more uniform products compared to the prior art. Such graphite materials are typically employed as an additive in polymers, batteries or other applications.