Cryogenic Leaf Embrittlement for Guayule Latex Extraction

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Conventional methods for removing leaves from rubber-producing plants, such as Guayule, often result in environmental and health concerns, as well as undesirable dehydration and coagulation of latex, particularly due to the use of chemical defoliants and hormonal treatments, which are not suitable for plants lacking a leaf abscission zone.

Innovation Solution

The method involves contacting harvested plant material with a cryogenic liquid to embrittle the leaves, followed by applying a mechanical force to separate them from the branches, while avoiding embrittlement of the branches, and optionally using rapid defrosting to prevent latex coagulation, utilizing techniques like agitation, vibration, or density separation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If conventional chemical defoliants or hormonal treatments are used to remove leaves, then leaf removal is achieved, but environmental and health concerns arise, and latex coagulation occurs

Engineering Contradiction:
Improveleaf removalVSAvoidenvironmental and health concerns, latex coagulation
Core Design Contradiction:
Ease of manufactureVSObject-affected harmful factors

Solution Approach 1:

The invention changes the physical state parameter of the leaves by exposing them to cryogenic temperatures, transforming them from a flexible state to an embrittled state. This physical parameter change enables mechanical removal without chemical agents, eliminating the harmful effects of chemical defoliants and hormonal treatments while preventing latex coagulation.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention replaces chemical and hormonal systems with a physical cryogenic system. Instead of using chemicals to soften leaves for removal, the system uses cold temperatures to embrittle leaves, making them susceptible to mechanical fracture. This substitution eliminates the harmful chemical effects while achieving the same functional goal of leaf removal.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Ease of manufacture

If conventional chemical and hormonal defoliants are used on plants lacking a leaf abscission zone, then leaf removal is attempted, but dehydration and irreversible coagulation of latex occur

Engineering Contradiction:
Improveleaf removalVSAvoidlatex integrity
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The invention applies a cryogenic temperature parameter change that selectively embrittles leaves without affecting the plant's latex content. By controlling the temperature exposure, the system achieves leaf embrittlement while maintaining latex fluidity, thus removing leaves without causing dehydration or coagulation of the valuable latex product.

Inventive Principle:
Principle #35Parameter changes

3Ease of manufacture

If cryogenic liquid is applied for extended time to embrittle leaves, then leaf separation is improved, but branches may become embrittled and damaged

Engineering Contradiction:
Improveleaf separationVSAvoidbranch integrity
Core Design Contradiction:
Ease of manufactureVSStrength

Solution Approach 1:

The invention applies partial action by controlling the cryogenic exposure time to be sufficient for leaf embrittlement but insufficient for branch embrittlement. This partial application of the cryogenic effect achieves the desired leaf separation while preserving branch strength and integrity for subsequent processing.

Inventive Principle:
Principle #16Partial or excessive action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This process effectively separates leaves from branches without coagulating the latex, reducing contamination and dehydration, and can be scaled for industrial use, enhancing the quality and yield of natural rubber latex for medical and industrial applications.

Implementation Method 1

contacting at least a portion of harvested plant material having a leaves and branches with at least one cryogenic liquid for at least an amount of time sufficient to produce embrittled leaves

Methodology Applied
Scientific EffectCryogenic embrittlement: Freezing

Data Source

PatentUS9873813B2Bioprocessing of harvested plant materials for extraction of biopolymers and related materials and methods
Publication Date: 2018.01.23 OHIO STATE INNOVATION FOUND
  • US9873813B2 patent drawing
  • US9873813B2 patent drawing
  • US9873813B2 patent drawing

AI summary

Methods are provided for rapid and efficient removal and separation of leaves and bark from harvested plant material for use in extraction and purification of plant products, and in particular, the removal of leaves and bark from Guayule for the extraction of latex for use in latex and rubber products.