Guayule Rubber Extraction via Hammer and Roller Milling

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Solution Overview

Problem

Non-Hevea plants store natural rubber within their cells, making it inaccessible for extraction through tapping, and existing methods do not effectively increase extractable rubber content without also increasing resin content.

Innovation Solution

The use of hammer milling and/or roller milling with specific parameters, such as screen sizes and moisture content, to process chopped non-Hevea plant matter, resulting in increased extractable rubber content through organic or aqueous extraction without significantly increasing resin content.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If conventional physical means are used to break down cell walls of non-Hevea plants, then rubber becomes accessible for extraction, but resin content increases unduly

Engineering Contradiction:
Improveextractable rubber contentVSAvoidresin content
Core Design Contradiction:
Quantity of substanceVSObject-generated harmful factors

Solution Approach 1:

The patent applies parameter changes by controlling moisture content at 10-15% and using specific screen sizes (less than 1/2 inch) in hammer milling, along with corrugated rolls having no more than 12 grooves per inch in roller milling. These specific parameter ranges optimize cell wall breakdown while minimizing resin release, resolving the contradiction between increasing rubber accessibility and controlling resin content.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs dynamic milling processes where hammer mills and roller mills with corrugated rolls create varying mechanical forces during processing. The combination of hammer impact and rolling compression with specific groove configurations creates dynamic stress patterns that selectively rupture rubber-containing cells while preserving resin-containing structures, thereby increasing extractable rubber without unduly increasing resin content.

Inventive Principle:
Principle #15Dynamics

2Quantity of substance

If hammer milling with small screen size is used, then extractable rubber content increases by at least 30%, but processing complexity increases

Engineering Contradiction:
Improveextractable rubber contentVSAvoidmilling process complexity
Core Design Contradiction:
Quantity of substanceVSDevice complexity

Solution Approach 1:

The patent merges hammer milling and roller milling with corrugated rolls into a single integrated processing step. By combining these two milling mechanisms in one operation rather than using them separately, the patent achieves the 30% increase in extractable rubber content while minimizing the increase in processing complexity. The combined process handles both size reduction and cell wall breakdown in one pass through the milling equipment.

Inventive Principle:
Principle #5Merging (Combining)

3Productivity

If moisture content is kept at maximum 15 weight %, then rubber extraction efficiency increases, but processing conditions become more restrictive

Engineering Contradiction:
Improverubber extraction efficiencyVSAvoidprocessing condition flexibility
Core Design Contradiction:
ProductivityVSAdaptability or versatility

Solution Approach 1:

The patent establishes a specific moisture content parameter range of 10-15 weight % as an optimal processing condition. By defining this narrow range, the patent maximizes rubber extraction efficiency through controlled cell wall permeability while accepting reduced flexibility in processing conditions. This parameter optimization ensures consistent extraction efficiency across different non-Hevea plant materials.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method achieves a 30-100% increase in extractable rubber content while keeping resin content within acceptable limits, making it a more efficient process for extracting rubber from non-Hevea plant matter.

Implementation Method 1

subjecting the chopped non-Hevea plant matter to at least one of hammer milling utilizing a screen size of less than 1⁄2′′ and roller milling with corrugated rolls

Methodology Applied
Scientific EffectMechanical force: Mechanical Force

Implementation Method 2

the resulting plant matter such as by organic solvent extraction or aqueous extraction

Methodology Applied
Scientific EffectSolvent extraction: Solvation

Data Source

PatentUS10138304B2Methods for increasing the extractable rubber content of non-<i>Hevea </i>plant matter
Publication Date: 2018.11.27 BRIDGESTONE CORP

AI summary

Methods for increasing the extractable rubber content of non-Hevea plant matter that entail the use of particular forms of hammer milling and/or roller milling in an increase in the amount of rubber that can be extracted from the resulting plant matter such as by organic solvent extraction or aqueous extraction are provided. In certain embodiments, the methods are for increasing the extractable rubber content of guayule plant matter, and entail the use of particular forms of hammer milling in combination with roller milling and flaking to increase the amount of rubber that can be extracted from the guayule plant matter such as by organic solvent extraction or aqueous extraction.