Guayusa Antioxidant Extraction via Multi-Stage Filtration and Drying

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Solution Overview

Problem

Current methods for utilizing guayusa plant extracts are inefficient in producing a concentrated, effective nutritional formulation for inflammatory disease prevention and cognitive enhancement, with limitations in shelf life and sensory profile, and lack a specific active ratio for enhanced health benefits.

Innovation Solution

A process involving multiple solvent contacts and filtrations to extract and combine antioxidant, xanthine, and amino acid-rich extracts from guayusa plant material, using ethanol:hot water solutions and nanofiltration to achieve a nutrient-rich extract with enhanced stability and taste.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If guayusa leaves are steeped to form a beverage substrate, then the product contains antioxidants, catechins, vitamins and amino acids, but the levels of these beneficial compounds are relatively low

Engineering Contradiction:
Improveantioxidant contentVSAvoidextraction efficiency
Core Design Contradiction:
Quantity of substanceVSProductivity

Solution Approach 1:

The extraction process is divided into multiple sequential steps including initial steeping, filtration, concentration, and drying. The plant material is processed in stages to progressively extract and concentrate the desired compounds, transforming the low-yield single-steep method into a multi-stage extraction system that achieves high concentration of antioxidants and other beneficial compounds.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention transitions from a liquid beverage form to a concentrated powder extract, adding a new dimension of concentration and versatility. This dimensional change allows the same plant material to provide both immediate beverage consumption and long-term stored concentrated extract, significantly increasing the effective quantity of active compounds available per unit of plant material.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Reliability

If the beverage is produced with natural ingredients, then the product has health benefits, but the shelf life is limited and oxidative damage occurs

Engineering Contradiction:
Improveshelf lifeVSAvoidoxidative damage
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The antioxidant extract is prepared in advance and concentrated before use, removing moisture that would facilitate oxidative degradation. By pre-concentrating the extract and controlling the drying process, the system eliminates the water activity that enables oxidation during storage, thereby extending shelf life while preserving the health benefits of the natural compounds.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The invention changes the physical state and concentration parameters of the extract through controlled drying and concentration processes. By adjusting moisture content, temperature, and concentration levels during processing, the system creates a stable, low-moisture final product that resists oxidative damage while maintaining the bioactive compounds responsible for health benefits.

Inventive Principle:
Principle #35Parameter changes

3Quantity of substance

If the extract is concentrated to increase antioxidant content, then the health benefits are enhanced, but the sensory profile deteriorates with bitterness

Engineering Contradiction:
Improveantioxidant concentrationVSAvoidbitterness
Core Design Contradiction:
Quantity of substanceVSObject-generated harmful factors

Solution Approach 1:

The invention selectively extracts the desired antioxidant compounds and other beneficial substances from the plant material while leaving behind unwanted bitter-tasting compounds in the discarded solid residue. Through controlled extraction and filtration, the system separates the beneficial antioxidants from the bitter components, achieving high concentration of desirable compounds without the accompanying bitterness.

Inventive Principle:
Principle #2Taking out (Extraction)

4Quantity of substance

If multiple extraction steps are performed to increase concentration, then the nutrient content is enhanced, but the process complexity increases

Engineering Contradiction:
Improvenutrient concentrationVSAvoidprocess steps
Core Design Contradiction:
Quantity of substanceVSDevice complexity

Solution Approach 1:

The extraction system uses a universal solvent system (water and/or alcohol) that can extract multiple types of compounds (antioxidants, catechins, vitamins, amino acids) simultaneously in a single contact. This multi-functional extraction approach achieves high nutrient concentration without requiring separate extraction processes for each compound type, thereby reducing overall process complexity while maintaining high concentration of all beneficial nutrients.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process results in a concentrated extract with increased antioxidant and nutrient content, improved shelf stability, and a balanced active ratio providing enhanced health benefits, including inflammation reduction and cognitive enhancement.

Implementation Method 1

contacting a plant material from a guayusa plant for a first time with a solvent, thereby obtaining a first slurry, filtering said first slurry, thereby obtaining a first extract

Methodology Applied
Scientific EffectExtraction: Liquid-Liquid Extraction

Implementation Method 2

contacting a plant material from a guayusa plant for a first time with a solvent, thereby obtaining a first slurry

Methodology Applied
Scientific EffectDiffusion: Diffusion

Implementation Method 3

filtering said first slurry, thereby obtaining a first extract, contacting said plant material for a second time with said solvent, thereby obtaining a second slurry, filtering said second slurry, thereby obtaining a second extract

Methodology Applied
Scientific EffectFiltration: Filter (physical)

Implementation Method 4

substantially drying said third extract

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentUS10792319B2Process for the production of an enriched natural antioxidant mixture from a single source plant
Publication Date: 2020.10.06 APPLIED FOOD SCI
  • US10792319B2 patent drawing

AI summary

A process for extracting antioxidants from a plant, including contacting a plant material from a guayusa plant for a first time with a solvent, thereby obtaining a first slurry, filtering said first slurry, thereby obtaining a first extract, contacting said plant material for a second time with said solvent, thereby obtaining a second slurry, filtering said second slurry, thereby obtaining a second extract, combining said first extract and said second extract, thereby generating an third extract containing at least antioxidants, xanthines, and amino acids, and substantially drying said third extract.