Hydrogen Sulfide Scavenging Additives with Hydroxyl Alkylated Amine Activators

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Solution Overview

Problem

Existing hydrogen sulfide (H2S) scavenging additive compositions, particularly those using zinc compounds like zinc octoate, require high dosages and are negatively affected by the addition of polyphosphoric acid (PPA), leading to reduced scavenging efficiency and re-release of H2S, making them economically inefficient and environmentally problematic.

Innovation Solution

Incorporating hydroxyl alkylated amines as activators with zinc compounds and optionally polyphosphoric acid in the scavenging compositions to enhance H2S scavenging efficiency, either alongside or after the initial additive application, thereby reducing the negative effects of PPA and improving overall scavenging performance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If high dosage of zinc-based additives is used for H2S scavenging, then scavenging capacity is improved, but economic efficiency deteriorates

Engineering Contradiction:
ImproveH2S scavenging efficiencyVSAvoidadditive dosage
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The patent changes the chemical parameters of the additive system by introducing hydroxyl alkylated amines with specific molecular structures and functional groups. This transforms the zinc-based additive from a simple scavenger to a synergistic system where the amine component enhances the scavenging efficiency, allowing reduced dosage while maintaining or improving H2S removal capability.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite additive system combining zinc-based compounds (zinc oxide, zinc stearate, zinc octoate) with hydroxyl alkylated amines (tri-isopropanol amine, tris(2-hydroxypropyl)amine). This composite approach produces a synergistic effect where the combination of materials achieves superior H2S scavenging performance compared to individual components, reducing the total quantity of additive needed.

Inventive Principle:
Principle #40Composite materials

2Stability of the object's composition

If polyphosphoric acid (PPA) is added to enhance modification, then material properties are improved, but H2S scavenging efficiency deteriorates due to re-release

Engineering Contradiction:
Improvematerial modificationVSAvoidH2S scavenging efficiency
Core Design Contradiction:
Stability of the object's compositionVSReliability

Solution Approach 1:

The patent applies preliminary anti-action by introducing hydroxyl alkylated amines that preemptively counteract the harmful effect of PPA-induced H2S re-release. The amine components react with or sequester the H2S that would otherwise be released by PPA, neutralizing the negative effect before it can compromise scavenging efficiency. This allows PPA to be used for material modification without sacrificing H2S removal performance.

Inventive Principle:
Principle #9Preliminary anti-action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The use of hydroxyl alkylated amines significantly improves H2S scavenging efficiency of zinc-based additives, maintaining or increasing effectiveness even in the presence of PPA, thus reducing the need for high additive dosages and minimizing environmental impact.

Implementation Method 1

Incorporating hydroxyl alkylated amines as activators with zinc compounds and optionally polyphosphoric acid in the scavenging compositions to enhance H2S scavenging efficiency

Methodology Applied
Scientific EffectComplex formation: Chemical Bonding

Implementation Method 2

The prior art additive, i.e., the compound selected from the group comprising zinc compound, zinc soap, and zinc salt of organic acid

Methodology Applied
Scientific EffectPrecipitation: Precipitation

Implementation Method 3

an additive 1 comprising at least one compound selected from the group comprising zinc compound, zinc soap, and zinc salt of organic acid

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Data Source

PatentUS10493396B2Hydrogen sulfide scavenging additive compositions, and medium comprising the same
Publication Date: 2019.12.03 DORF KETAL CHEMICALS (INDIA) PRIVATE LIMITED

AI summary

The present invention relates to a hydrogen sulfide scavenging additive composition, wherein the composition comprises:a. an additive 1 comprising at least one compound selected from the group comprising zinc compound, zinc soap, and zinc salt of organic acid; andb. at least one activator comprising one or more hydroxyl alkylated amine.In one embodiment, the composition further comprises an additive 2 comprising polyphosphoric acid (PPA).In one embodiment, the present invention also relates to a method of using the hydrogen sulfide scavenging additive compositions of the present invention for scavenging the hydrogen sulfide in the medium.In one embodiment, the present invention also relates to a method of scavenging hydrogen sulphide in the medium by employing the hydrogen sulfide scavenging additive compositions of the present invention.In one embodiment, the present invention also relates to a medium comprising hydrogen sulfide (H2S) scavenging additive compositions of the present invention.