On-Demand Haloamine Generation Using Solid Halogen Releasers

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Conventional methods for producing haloamine solutions, such as monochloramine, face challenges including variable active concentrations due to aging, high toxicity, equipment hazards, and inefficiencies in water usage, particularly in locations where water is scarce, and require sophisticated hardware and software for safe and effective production.

Innovation Solution

A method involving the on-site preparation of haloamine solutions using solid halogen releasers and ammonia or ammonium ions in dilute aqueous solutions, allowing for the formation of monochloramine at the site of use with controlled concentrations and reduced hazards, avoiding the need for highly concentrated solutions and minimizing water usage.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If concentrated parent solutions are used to reduce delivery costs, then manufacturing cost is reduced, but operator safety and equipment safety deteriorate due to high toxicity and exothermic reaction hazards

Engineering Contradiction:
Improvemanufacturing costVSAvoidoperator safety and equipment safety
Core Design Contradiction:
Ease of manufactureVSObject-affected harmful factors

Solution Approach 1:

The concentrated parent solutions are segmented into smaller, dilute working solutions that are prepared on-demand at the point of use. This segmentation reduces the quantity of hazardous concentrated materials handled and stored, thereby reducing toxicity risks and exothermic reaction hazards while maintaining cost-effectiveness through localized preparation.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

A generator system acts as an intermediary device that safely converts concentrated parent solutions into dilute working solutions on-demand. This intermediary process controls the mixing and reaction conditions, preventing direct handling of highly toxic concentrated materials and eliminating the risk of uncontrolled exothermic reactions.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Object-affected harmful factors

If sophisticated hardware and software are used to operate generators safely, then operator safety is improved, but device complexity increases

Engineering Contradiction:
Improveoperator safetyVSAvoidhardware and software complexity
Core Design Contradiction:
Object-affected harmful factorsVSDevice complexity

Solution Approach 1:

The generator system is designed to be self-regulating with automatic control features that monitor and adjust the mixing process without requiring complex external hardware or software. The system self-corrects potential safety issues through inherent design features such as controlled addition rates and temperature monitoring, reducing complexity while maintaining safety.

Inventive Principle:
Principle #25Self-service

3Object-affected harmful factors

If large amounts of water are used to pre-dilute parent solutions to safe levels, then operator safety is improved, but water usage efficiency deteriorates, particularly in water-scarce locations

Engineering Contradiction:
Improveoperator safetyVSAvoidwater usage
Core Design Contradiction:
Object-affected harmful factorsVSLoss of substance

Solution Approach 1:

The system performs preliminary dilution of parent solutions in controlled, small quantities immediately before use rather than pre-diluting large volumes in advance. This on-demand preparation minimizes water consumption by only diluting the necessary amount needed for current application, eliminating waste associated with storing and transporting large volumes of pre-diluted solutions.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables the safe, efficient, and economical production of haloamine solutions, such as monochloramine, on demand, reducing the risk of equipment damage and by-product formation, while maintaining biocidal efficacy and stability over time.

Implementation Method 1

dissolving at least one solid halogen releaser in a first aqueous solution to form a dilute first reactant

Methodology Applied
Scientific EffectDissolution: Solvation

Implementation Method 2

combining the dilute first reactant and the dilute second reactant to form said haloamine in solution

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Data Source

PatentEP3746399B1Methods to prepare haloamines using at least one solid reactant and products made therefrom
Publication Date: 2024.03.06 BUCKMAN LAB INT INC
  • EP3746399B1 patent drawingFigure 1
  • EP3746399B1 patent drawingFigure 2
  • EP3746399B1 patent drawing

AI summary

A method to prepare a haloamine, such as a monochloramine in solution, from a solid halogen releaser (s) is described. Also described is a process to form a haloamine in solution using solid reactants. Also, an aqueous haloamine, such as a monochloramine solution, is further described that has a haloamine in solution and a dehalogenated organic compound present. Methods of use are also described.