Halogen-Doped Garnet Oxide Solid Electrolyte

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Solution Overview

Problem

Current oxide-based solid electrolytes for lithium-ion batteries have limited ion conductivity, making it difficult to achieve high safety and performance, especially compared to sulfide-based electrolytes.

Innovation Solution

A lithium ion-conducting garnet type oxide composition comprising Li, La, Ga, Zr, and a halogen element, with specific proportions and structures, is developed to enhance ion conductivity beyond conventional levels, including a production method involving sintering at high temperatures to achieve a garnet-type crystal structure with improved lithium ion conductivity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional oxide-based solid electrolyte compositions are used, then safety is maintained, but it is extremely difficult to improve ion conductance beyond 10^-4 S/cm

Engineering Contradiction:
ImprovesafetyVSAvoidion conductance
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The invention creates a composite material system by combining the oxide-based solid electrolyte matrix with halogen elements (Cl, Br, or I). This composite approach, represented by the composition Li7-3xGaxLa3Zr2O12 containing 0.01-2.0 atom% halogen, enables simultaneous achievement of high safety (inherent to oxide-based systems) and high ion conductance (>10^-3 S/cm), resolving the contradiction between safety maintenance and conductance improvement.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The new oxide-based solid electrolyte exhibits significantly improved lithium ion conductivity at room temperature, exceeding 1.0×10−3 S/cm, suitable for high-performance battery applications, while maintaining safety and stability.

Implementation Method 1

a lithium ion-conducting garnet type oxide: that contains lithium, lanthanum, zirconium as main constituent elements and further contains a halogen element

Methodology Applied
Scientific EffectIon substitution: Dopants

Implementation Method 2

a production method involving sintering at high temperatures to achieve a garnet-type crystal structure with improved lithium ion conductivity

Methodology Applied
Scientific EffectSintering: Sintering

Data Source

PatentUS20230064947A1Lithium ion-conducting garnet type oxide
Publication Date: 2023.03.02 KANEKA CORP

AI summary

An oxide-based solid electrolyte with a high lithium ion conductance is provided. A lithium ion-conducting garnet type oxide includes Li, La, Ga, Zr, a halogen element, and oxygen. A lithium ion conductivity at room temperature is not lower than 1.0×10−3 S/cm. A proportion of Ga with respect to 1 mole of the oxide may be not larger than 0.5 moles.The halogen element may be at least one type selected from the group consisting of Cl, Br, and I, and a proportion of Li with respect to 1 mole of the oxide may be not smaller than 6.1 moles and smaller than 6.5 moles.