Hard Compact Omni-Directional Compaction Bonding

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Solution Overview

Problem

Existing hard compacts used in tools like earth boring bits face challenges in bonding superhard members, such as polycrystalline diamond, with substrates like cobalt-tungsten carbide, leading to difficulties in attachment and thermal stability, especially at high temperatures.

Innovation Solution

A rapid omni-directional compaction process is employed, involving a pre-compaction composite with a substrate, a superhard member, and a braze layer, consolidated under high pressure and temperature to form a dense, bonded hard composite body, facilitating strong attachment and thermal stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If cobalt is leached from the diamond lattice structure to gain thermal stability, then thermal stability is improved, but brittleness increases and impact resistance is reduced

Engineering Contradiction:
Improvethermal stabilityVSAvoidimpact resistance
Core Design Contradiction:
TemperatureVSStrength

Solution Approach 1:

The patent applies selective leaching where only certain portions of the diamond table are treated with acid to remove cobalt. This creates local variations in cobalt content - fully leached regions provide thermal stability while unleached or partially leached regions maintain impact resistance. The differential treatment of different zones resolves the contradiction between thermal stability and mechanical strength.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent controls the degree of leaching as a variable parameter. By adjusting leaching time, acid concentration, and temperature, the process can produce intermediate states between fully leached (thermally stable but brittle) and unleached (tough but thermally unstable). This parameter control allows optimization of both thermal stability and impact resistance simultaneously.

Inventive Principle:
Principle #35Parameter changes

2Strength

If high pressure and temperature are applied to bond superhard member to substrate, then bonding strength is improved, but thermal stability during bonding process becomes challenging

Engineering Contradiction:
Improvebonding strengthVSAvoidthermal stability during bonding
Core Design Contradiction:
StrengthVSTemperature

Solution Approach 1:

The patent introduces a braze layer as an intermediary material between the superhard diamond member and the carbide substrate. This braze layer has a melting point below the bonding temperature, allowing it to act as a flux that facilitates bonding at temperatures where the diamond remains stable. The braze layer absorbs thermal stress and enables strong bonding without requiring temperatures that would cause graphitization of the diamond.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The bonding process utilizes the phase transition of the braze layer from solid to liquid and back to solid. The braze is heated above its melting point to become liquid, enabling it to flow into bonding interfaces and create strong metallurgical bonds. Upon cooling, it solidifies to lock the superhard member to the substrate. This phase transition mechanism allows bonding at temperatures compatible with diamond thermal stability.

Inventive Principle:
Principle #36Phase transitions

3Productivity

If rapid omni-directional compaction is used to consolidate the composite, then manufacturing efficiency is improved, but achieving uniform density and bonding becomes difficult

Engineering Contradiction:
Improvemanufacturing efficiencyVSAvoiduniform density and bonding
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent employs isostatic pressing which applies pressure uniformly from all directions (omni-directional), creating a spherical stress state rather than unidirectional compression. This curved, multi-directional pressure distribution ensures uniform density throughout the compacted body and promotes even bonding across the entire interface between superhard member and substrate, resolving the issue of non-uniform density while maintaining rapid processing.

Inventive Principle:
Principle #14Spheroidality (Curvature)

Solution Approach 2:

The patent replaces traditional multi-step mechanical bonding processes with a single rapid omni-directional compaction process. Instead of sequential operations for alignment, bonding, and densification, the isostatic pressing consolidates all these functions into one rapid operation, achieving uniform density and strong bonding simultaneously while dramatically improving manufacturing efficiency.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process enhances the bonding between superhard members and substrates, improving the attachment of hard compacts to tools and extending drilling life by maintaining thermal stability up to 1200°C without graphitization issues.

Implementation Method 1

heating the isostatic die assembly to a temperature at which the pressure-transmitting material is capable of fluidic flow

Methodology Applied
Scientific EffectHeating to fluidic flow: Melting

Implementation Method 2

compressing the isostatic die assembly to consolidate the pre-compaction composite under omnidirectional pressure equal to or greater than about 60,000 psi

Methodology Applied
Scientific EffectCompression: Compression

Implementation Method 3

a layer of braze between the substrate and the superhard member

Methodology Applied
Scientific EffectBrazing: Brazing

Data Source

PatentUS8821603B2Hard compact and method for making the same
Publication Date: 2014.09.02 KENNAMETAL INC
  • US8821603B2 patent drawing
  • US8821603B2 patent drawing
  • US8821603B2 patent drawing

AI summary

A hard composite member produced by a rapid omni-directional compaction process that includes the steps of: providing a pre-compaction composite comprising a substrate, a superhard member and a layer of braze between the substrate and the superhard member; placing the pre-compaction composite in a pressure transmitting material contained within a shell to form an isostatic die assembly; heating the isostatic die assembly to a temperature at which the pressure-transmitting material is capable of fluidic flow and wherein the temperature ranges between greater than the melting point of the braze layer and less than or equal to about 1200° C.; and in a forging press, compressing the isostatic die assembly to consolidate the pre-compaction composite under omnidirectional pressure at a pressure equal to or greater than about 60,000 psi into a dense, consolidated body.