Heavy Oil Upgrading with Staged Catalysts for Chemical Intermediates

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Solution Overview

Problem

Existing methods struggle to efficiently convert heavy oils, such as crude oil, into valuable chemical intermediates and transportation fuels while reducing aromatic, metal, and nitrogen content effectively.

Innovation Solution

A catalytic treatment process using a series of catalysts, including hydrodemetalization, transition, hydrodenitrogenation, and hydrocracking catalysts, to upgrade heavy oils by removing metals, nitrogen, and aromatics, followed by steam cracking to produce chemical intermediates and fuels.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If traditional refining operations are used to convert heavy oils, then the process is simple, but the production of chemical intermediates is insufficient to meet rising demands

Engineering Contradiction:
Improveproduction of chemical intermediatesVSAvoidprocess complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The refining process is divided into multiple specialized catalytic stages: hydrodemetalization catalyst to remove metals, hydrodenitrogenation catalyst to remove nitrogen, and hydrocracking catalysts to reduce aromatic content. Each catalyst performs a specific function in sequence, transforming the heavy oil progressively to meet chemical intermediate production demands.

Inventive Principle:
Principle #1Segmentation

2Object-affected harmful factors

If heavy oils are processed without specialized catalytic treatment, then the process is simpler, but the aromatic, metal, and nitrogen content remains high

Engineering Contradiction:
Improvearomatic, metal, and nitrogen contentVSAvoidcatalytic treatment complexity
Core Design Contradiction:
Object-affected harmful factorsVSDevice complexity

Solution Approach 1:

The process selectively extracts and removes harmful components from heavy oil through dedicated catalytic reactions. The hydrodemetalization catalyst extracts metals, the hydrodenitrogenation catalyst extracts nitrogen, and the hydrocracking catalysts extract aromatic compounds, each targeting specific contaminants to reduce their content to acceptable levels.

Inventive Principle:
Principle #2Taking out (Extraction)

3Adaptability or versatility

If a single catalyst is used for heavy oil treatment, then the device complexity is reduced, but the catalytic functionality is insufficient to remove metals, nitrogen, and aromatics effectively

Engineering Contradiction:
Improvecatalytic functionalityVSAvoidnumber of catalysts
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The patent implements a multi-functional catalytic system where five different catalysts work in sequence, each designed for a specific transformation function. This universal approach handles multiple types of contaminants (metals, sulfur, nitrogen, aromatics) and molecular size variations through a coordinated series of catalytic reactions, providing comprehensive treatment capability.

Inventive Principle:
Principle #6Universality (Multi-functionality)

4Productivity

If conventional hydrocracking catalysts with small pores are used, then the catalyst structure is simpler, but large crude oil molecules cannot diffuse inside effectively

Engineering Contradiction:
Improvereaction activity and selectivityVSAvoidcatalyst pore structure
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent employs hydrocracking catalysts with engineered porous structures having larger pore sizes compared to conventional catalysts. This porous design enables efficient diffusion of large crude oil molecules into the catalyst interior, increasing the number of active sites accessible to reactants and thereby enhancing reaction activity and selectivity for hydrocracking processes.

Inventive Principle:
Principle #31Porous materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process significantly reduces aromatic, metal, and nitrogen content, enhancing the production of chemical intermediates and fuels with improved catalytic functionality and efficiency.

Implementation Method 1

the primary function of the first catalyst (that is, the hydrodemetalization catalyst) is to remove metals from the heavy oil

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 2

the primary function of the second catalyst (that is, the transition catalyst) is to remove metals, sulfur, and nitrogen from the heavy oil

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 3

the primary function of the third catalyst (that is, the hydrodenitrogenation catalyst) is to further remove nitrogen, sulfur, or both

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 4

the primary function of the fourth catalyst (that is, the first hydrocracking catalyst) is to reduce aromatic content in the heavy oil

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 5

the primary function of the fifth catalyst (that is, the second hydrocracking catalyst) is to further reduce aromatic content in the heavy oil

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 6

heavy oils may be upgraded and converted to at least chemical intermediates by subsequent processing, such as steam cracking

Methodology Applied
Scientific EffectPyrolysis: Pyrolysis

Data Source

PatentEP3655504B1Methods for processing heavy oils
Publication Date: 2025.08.27 SAUDI ARABIAN OIL CO
  • EP3655504B1 patent drawingFigure 1
  • EP3655504B1 patent drawingFigure 2
  • EP3655504B1 patent drawingFigure 3

AI summary

According to one embodiment, a heavy oil may be processed by a method that may include upgrading at least a portion of the heavy oil to form an upgraded oil, where the upgrading comprising contacting the heavy oil with a hydrodemetalization catalyst, a transition catalyst, a hydrodenitrogenation catalyst, a first hydrocracking catalyst, and a second hydrocracking catalyst downstream of the first hydrocracking catalyst to remove at least a portion of metals, nitrogen, or aromatics content from the heavy oil and form the upgraded oil. The final boiling point of the upgraded oil may be less than or equal to 540 C. The second hydrocracking catalyst cracks at least a portion of vacuum gas oil in the heavy oil. The first hydrocracking catalyst may comprise a greater average pore size than the second hydrocracking catalyst.