Helium Phase Separation Refrigerator for Continuous Sub-1K Cooling

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Solution Overview

Problem

There is a need for a continuous helium-3 refrigerator that is easier and cheaper to operate, as existing systems are complex and require separate gas handling circuits for helium-3 and helium-4, and helium-3 is scarce and expensive.

Innovation Solution

A cryogenic refrigerator that combines helium-3 and helium-4 pumping circuits into a single system, utilizing phase separation to achieve continuous cooling by partially liquefying the mixture and exploiting the higher vapor pressure of helium-3 to enable evaporative cooling, with a simplified design that reduces helium-3 usage.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If separate gas handling circuits are used for helium-3 and helium-4, then reliability of isotope separation is improved, but device complexity increases

Engineering Contradiction:
Improveisotope separationVSAvoidgas handling circuits
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent combines separate helium-3 and helium-4 gas handling circuits into a single unified circuit. The mixture of helium isotopes is circulated through shared components including the pulse tube cooler, heat exchangers, and pumping system. Phase separation occurs naturally in the settling chamber where liquid helium-3 and liquid helium-4 separate by density, eliminating the need for separate circulation loops while maintaining reliable isotope separation.

Inventive Principle:
Principle #5Merging (Combining)

2Loss of substance

If helium-3 is vented to atmosphere, then loss of substance is reduced, but environmental harm increases

Engineering Contradiction:
Improvehelium-3VSAvoidenvironmental impact
Core Design Contradiction:
Loss of substanceVSObject-affected harmful factors

Solution Approach 1:

The patent operates the helium-3 refrigerator in a closed-cycle configuration where the working fluid is contained within an inert, sealed system. The working fluid circulates continuously through the cooling cycle without being vented to the atmosphere, maintaining an inert environment that prevents helium-3 release while enabling continuous operation.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

3Temperature

If pumped pot method is used, then temperature below 1K is achieved, but productivity decreases due to periodic refilling

Engineering Contradiction:
Improvecooling temperatureVSAvoidcontinuous cooling
Core Design Contradiction:
TemperatureVSProductivity

Solution Approach 1:

The patent implements continuous cooling by establishing a closed-cycle system where liquid helium-3 is continuously pumped from the evaporator, vapor is condensed in the condenser, and liquid returns to the evaporator. This continuous circulation eliminates the periodic refilling requirement of pumped pot systems while maintaining temperatures below 1K, as demonstrated by the steady-state operation of the phase separation refrigerator.

Inventive Principle:
Principle #20Continuity of useful action

4Power

If helium-3 concentration is increased, then cooling power is improved, but cost increases due to scarcity

Engineering Contradiction:
Improvecooling powerVSAvoidhelium-3 amount
Core Design Contradiction:
PowerVSQuantity of substance

Solution Approach 1:

The patent exploits the phase separation transition that occurs in liquid helium mixtures at low temperatures. By controlling temperature and pressure to induce phase separation, the system concentrates helium-3 in the liquid phase while helium-4 remains in the vapor phase. This natural phase transition enables effective separation and recycling of helium-3 without requiring large quantities of the isotope, maintaining cooling power while reducing helium-3 consumption.

Inventive Principle:
Principle #36Phase transitions

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system achieves continuous cooling with lower helium-3 consumption, similar base temperatures, and reduced complexity, making it more cost-effective and user-friendly compared to existing helium-3 refrigerators.

Implementation Method 1

one or more cooling elements arranged to at least partially liquefy helium from a gas containing a mixture of helium-3 and helium-4

Methodology Applied
Scientific EffectJoule-Thomson effect: Joule-Thomson Effect

Implementation Method 2

The outgoing flow of helium from the reservoir to the pumps may be arranged to cool the incoming flow of helium to the cooling elements

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Implementation Method 3

expose a surface of the volume of the liquid helium to evaporation to cool the reservoir

Methodology Applied
Scientific EffectEvaporative cooling: Evaporative Cooler

Implementation Method 4

exploiting the higher vapor pressure of helium-3 to enable evaporative cooling

Methodology Applied
Scientific EffectVapor pressure: Vapour Pressure

Implementation Method 5

cause the liquid helium in the reservoir to separate into helium-3 rich and dilute phases

Methodology Applied
Scientific EffectPhase separation:

Data Source

PatentUS12372274B1Helium phase separation refrigerator
Publication Date: 2025.07.29 ZERO POINT CRYOGENICS INC
  • US12372274B1 patent drawing
  • US12372274B1 patent drawing
  • US12372274B1 patent drawing

AI summary

A cryogenic refrigerator uses a mixture of helium-3 and helium-4. Gaseous helium is pumped from a reservoir containing a liquid mixture of helium-3 and helium-4 to cause cooling and a phase separation into an upper helium-3 rich phase which floats at the top for further evaporation and a lower dilute phase below the helium-3 rich phase. This separation enables operation at temperatures typical of a helium-3 refrigerator while initial liquefaction of the mixture is easier than liquefaction of pure helium-3 and can use a smaller amount of helium-3. Embodiments of the refrigerator can provide continuous cooling.